OBSP Determination:
4-HEPTANONE, 2,6-DIMETHYL-
METHOD: 4437 , TESTIDCODE: 77419GM016

Analysis Date = 06/29/16 SpikeMix = NSI 041516: 40 µl & ChemService 5082800: 40 µl Pct Recovery = 101% Analysis Date = 10/21/16 SpikeMix = ChemService 5082800: 40 µl & Supelco LC20145V: 40 µl & NSI 041416HVOC: 40 µl Pct Recovery = 88% Analysis Date = 01/24/17 SpikeMix = ChemService 5082800: 40 µl & Supelco LC20145V: 40 µl Pct Recovery = 85% Analysis Date = 02/02/17 SpikeMix = Abs 060916HVOC: 40 µl & ChemService 5082800: 40 µl & Accu 216041225: 40 µl Pct Recovery = 87% Analysis Date = 09/23/16 SpikeMix = Phenova B20160303: 40 µl & Accu 216041354: 40 µl Pct Recovery = 89% Analysis Date = 12/05/16 SpikeMix = Abs 060916HVOC: 40 µl & Phenova B20160303: 40 µl Pct Recovery = 87% Analysis Date = 03/09/17 SpikeMix = NSI 110916: 40 µl & Phenova B20160303: 40 µl Pct Recovery = 88% Analysis Date = 07/14/16 SpikeMix = NSI 041516: 25 µl & ChemService 5082800: 25 µl & NSI 041416HVOC: 25 µl Pct Recovery = 88% Analysis Date = 08/31/16 SpikeMix = ChemService 5082800: 25 µl & Accu 216041354: 25 µl Pct Recovery = 92% Analysis Date = 12/23/16 SpikeMix = ChemService 5082800: 25 µl & Accu 216041354: 25 µl & NSI 041416HVOC: 25 µl Pct Recovery = 99% Analysis Date = 06/13/17 SpikeMix = Abs 060916HVOC: 25 µl & ChemService 5082800: 25 µl Pct Recovery = 87% Analysis Date = 08/11/16 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl Pct Recovery = 88% Analysis Date = 09/08/16 SpikeMix = Abs 060916HVOC: 25 µl & Phenova B20160303: 25 µl & NSI 041416HVOC: 25 µl Pct Recovery = 83% Analysis Date = 11/10/16 SpikeMix = NSI 041516: 25 µl & Phenova B20160303: 25 µl & Accu 216041225: 25 µl Pct Recovery = 86% Analysis Date = 03/10/17 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & Accu 216041225: 25 µl Pct Recovery = 91% Analysis Date = 08/16/17 SpikeMix = ChemService 6441300: 15 µl & Spex Organics BW170726021: 15 µl & ChemService 6424 Pct Recovery = 106% Analysis Date = 06/23/16 SpikeMix = . Pct Recovery = 96% Analysis Date = 07/27/16 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl Pct Recovery = 92% Analysis Date = 08/18/16 SpikeMix = Abs 060916HVOC: 15 µl & ChemService 5082800: 15 µl Pct Recovery = 97% Analysis Date = 10/07/16 SpikeMix = Abs 060916HVOC: 15 µl & ChemService 5082800: 15 µl Pct Recovery = 98% Analysis Date = 11/18/16 SpikeMix = NSI 110916: 15 µl & ChemService 5082800: 15 µl & Accu 216041225: 15 µl Pct Recovery = 94% Analysis Date = 04/27/17 SpikeMix = Abs 060916HVOC: 15 µl & ChemService 5082800: 15 µl & NSI 041416HVOC: 15 µl Pct Recovery = 92% Analysis Date = 07/14/17 SpikeMix = Accu 216041354: 15 µl & ChemService 5082800: 15 µl & Accu 216041225: 15 µl Pct Recovery = 110% Analysis Date = 07/06/16 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl Pct Recovery = 89% Analysis Date = 01/14/17 SpikeMix = Phenova B20160303: 15 µl & Supelco LC20145V: 15 µl Pct Recovery = 84% Analysis Date = 02/24/17 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & Accu 216041225: 15 µl Pct Recovery = 83% Analysis Date = 03/24/17 SpikeMix = Abs 060916HVOC: 15 µl & Phenova B20160303: 15 µl & Accu 216041225: 15 µl Pct Recovery = 102% Analysis Date = 08/01/17 SpikeMix = Abs 062917: 15 µl & Phenova B20160303: 15 µl Pct Recovery = 97% Analysis Date = 06/03/16 SpikeMix = NSI 041516: 15 µl & Phenova B20160303: 15 µl & NSI 041416HVOC: 15 µl Pct Recovery = 91% Analysis Date = 04/28/16 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl Pct Recovery = 99% Analysis Date = 03/22/16 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl Pct Recovery = 108% Analysis Date = 02/12/16 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl Pct Recovery = 86% Analysis Date = 08/16/17 Pct Recovery = 103% Analysis Date = 08/13/17 Pct Recovery = 102% Analysis Date = 08/13/17 Pct Recovery = 102% Analysis Date = 08/10/17 Pct Recovery = 102% Analysis Date = 08/10/17 Pct Recovery = 102% Analysis Date = 08/07/17 Pct Recovery = 102% Analysis Date = 08/07/17 Pct Recovery = 102% Analysis Date = 08/04/17 Pct Recovery = 102% Analysis Date = 08/04/17 Pct Recovery = 102% Analysis Date = 08/02/17 Pct Recovery = 102% Analysis Date = 08/02/17 Pct Recovery = 102% Analysis Date = 07/30/17 Pct Recovery = 101% Analysis Date = 07/30/17 Pct Recovery = 101% Analysis Date = 07/27/17 Pct Recovery = 101% Analysis Date = 07/27/17 Pct Recovery = 101% Analysis Date = 07/24/17 Pct Recovery = 101% Analysis Date = 07/24/17 Pct Recovery = 101% Analysis Date = 07/22/17 Pct Recovery = 101% Analysis Date = 07/22/17 Pct Recovery = 101% Analysis Date = 07/19/17 Pct Recovery = 101% Analysis Date = 07/19/17 Pct Recovery = 101% Analysis Date = 07/16/17 Pct Recovery = 100% Analysis Date = 07/16/17 Pct Recovery = 100% Analysis Date = 07/13/17 Pct Recovery = 100% Analysis Date = 07/13/17 Pct Recovery = 100% Analysis Date = 07/11/17 Pct Recovery = 100% Analysis Date = 07/11/17 Pct Recovery = 100% Analysis Date = 07/08/17 Pct Recovery = 100% Analysis Date = 07/08/17 Pct Recovery = 100% Analysis Date = 07/05/17 Pct Recovery = 100% Analysis Date = 07/05/17 Pct Recovery = 100% Analysis Date = 07/02/17 Pct Recovery = 99% Analysis Date = 07/02/17 Pct Recovery = 99% Analysis Date = 06/30/17 Pct Recovery = 99% Analysis Date = 06/30/17 Pct Recovery = 99% Analysis Date = 06/27/17 Pct Recovery = 99% Analysis Date = 06/27/17 Pct Recovery = 99% Analysis Date = 06/24/17 Pct Recovery = 99% Analysis Date = 06/24/17 Pct Recovery = 99% Analysis Date = 06/21/17 Pct Recovery = 99% Analysis Date = 06/21/17 Pct Recovery = 99% Analysis Date = 06/19/17 Pct Recovery = 98% Analysis Date = 06/19/17 Pct Recovery = 98% Analysis Date = 06/16/17 Pct Recovery = 98% Analysis Date = 06/16/17 Pct Recovery = 98% Analysis Date = 06/13/17 Pct Recovery = 98% Analysis Date = 06/13/17 Pct Recovery = 98% Analysis Date = 06/10/17 Pct Recovery = 98% Analysis Date = 06/10/17 Pct Recovery = 98% Analysis Date = 06/08/17 Pct Recovery = 98% Analysis Date = 06/08/17 Pct Recovery = 98% Analysis Date = 06/05/17 Pct Recovery = 97% Analysis Date = 06/05/17 Pct Recovery = 97% Analysis Date = 06/02/17 Pct Recovery = 97% Analysis Date = 06/02/17 Pct Recovery = 97% Analysis Date = 05/30/17 Pct Recovery = 97% Analysis Date = 05/30/17 Pct Recovery = 97% Analysis Date = 05/28/17 Pct Recovery = 97% Analysis Date = 05/28/17 Pct Recovery = 97% Analysis Date = 05/25/17 Pct Recovery = 97% Analysis Date = 05/25/17 Pct Recovery = 97% Analysis Date = 05/22/17 Pct Recovery = 96% Analysis Date = 05/22/17 Pct Recovery = 96% Analysis Date = 05/19/17 Pct Recovery = 96% Analysis Date = 05/19/17 Pct Recovery = 96% Analysis Date = 05/17/17 Pct Recovery = 96% Analysis Date = 05/17/17 Pct Recovery = 96% Analysis Date = 05/14/17 Pct Recovery = 96% Analysis Date = 05/14/17 Pct Recovery = 96% Analysis Date = 05/11/17 Pct Recovery = 95% Analysis Date = 05/11/17 Pct Recovery = 95% Analysis Date = 05/08/17 Pct Recovery = 95% Analysis Date = 05/08/17 Pct Recovery = 95% Analysis Date = 05/06/17 Pct Recovery = 95% Analysis Date = 05/06/17 Pct Recovery = 95% Analysis Date = 05/03/17 Pct Recovery = 95% Analysis Date = 05/03/17 Pct Recovery = 95% Analysis Date = 04/30/17 Pct Recovery = 95% Analysis Date = 04/30/17 Pct Recovery = 95% Analysis Date = 04/27/17 Pct Recovery = 94% Analysis Date = 04/27/17 Pct Recovery = 94% Analysis Date = 04/25/17 Pct Recovery = 94% Analysis Date = 04/25/17 Pct Recovery = 94% Analysis Date = 04/22/17 Pct Recovery = 94% Analysis Date = 04/22/17 Pct Recovery = 94% Analysis Date = 04/19/17 Pct Recovery = 94% Analysis Date = 04/19/17 Pct Recovery = 94% Analysis Date = 04/16/17 Pct Recovery = 94% Analysis Date = 04/16/17 Pct Recovery = 94% Analysis Date = 04/14/17 Pct Recovery = 93% Analysis Date = 04/14/17 Pct Recovery = 93% Analysis Date = 04/11/17 Pct Recovery = 93% Analysis Date = 04/11/17 Pct Recovery = 93% Analysis Date = 04/08/17 Pct Recovery = 93% Analysis Date = 04/08/17 Pct Recovery = 93% Analysis Date = 04/05/17 Pct Recovery = 93% Analysis Date = 04/05/17 Pct Recovery = 93% Analysis Date = 04/03/17 Pct Recovery = 93% Analysis Date = 04/03/17 Pct Recovery = 93% Analysis Date = 03/31/17 Pct Recovery = 92% Analysis Date = 03/31/17 Pct Recovery = 92% Analysis Date = 03/28/17 Pct Recovery = 92% Analysis Date = 03/28/17 Pct Recovery = 92% Analysis Date = 03/25/17 Pct Recovery = 92% Analysis Date = 03/25/17 Pct Recovery = 92% Analysis Date = 03/22/17 Pct Recovery = 92% Analysis Date = 03/22/17 Pct Recovery = 92% Analysis Date = 03/20/17 Pct Recovery = 91% Analysis Date = 03/20/17 Pct Recovery = 91% Analysis Date = 03/17/17 Pct Recovery = 91% Analysis Date = 03/17/17 Pct Recovery = 91% Analysis Date = 03/14/17 Pct Recovery = 91% Analysis Date = 03/14/17 Pct Recovery = 91% Analysis Date = 03/11/17 Pct Recovery = 91% Analysis Date = 03/11/17 Pct Recovery = 91% Analysis Date = 03/09/17 Pct Recovery = 91% Analysis Date = 03/09/17 Pct Recovery = 91% Analysis Date = 03/06/17 Pct Recovery = 91% Analysis Date = 03/06/17 Pct Recovery = 91% Analysis Date = 03/03/17 Pct Recovery = 90% Analysis Date = 03/03/17 Pct Recovery = 90% Analysis Date = 02/28/17 Pct Recovery = 90% Analysis Date = 02/28/17 Pct Recovery = 90% Analysis Date = 02/26/17 Pct Recovery = 90% Analysis Date = 02/26/17 Pct Recovery = 90% Analysis Date = 02/23/17 Pct Recovery = 90% Analysis Date = 02/23/17 Pct Recovery = 90% Analysis Date = 02/20/17 Pct Recovery = 90% Analysis Date = 02/20/17 Pct Recovery = 90% Analysis Date = 02/17/17 Pct Recovery = 90% Analysis Date = 02/17/17 Pct Recovery = 90% Analysis Date = 02/15/17 Pct Recovery = 90% Analysis Date = 02/15/17 Pct Recovery = 90% Analysis Date = 02/12/17 Pct Recovery = 90% Analysis Date = 02/12/17 Pct Recovery = 90% Analysis Date = 02/09/17 Pct Recovery = 90% Analysis Date = 02/09/17 Pct Recovery = 90% Analysis Date = 02/06/17 Pct Recovery = 90% Analysis Date = 02/06/17 Pct Recovery = 90% Analysis Date = 02/04/17 Pct Recovery = 90% Analysis Date = 02/04/17 Pct Recovery = 90% Analysis Date = 02/01/17 Pct Recovery = 90% Analysis Date = 02/01/17 Pct Recovery = 90% Analysis Date = 01/29/17 Pct Recovery = 90% Analysis Date = 01/29/17 Pct Recovery = 90% Analysis Date = 01/26/17 Pct Recovery = 90% Analysis Date = 01/26/17 Pct Recovery = 90% Analysis Date = 01/24/17 Pct Recovery = 90% Analysis Date = 01/24/17 Pct Recovery = 90% Analysis Date = 01/21/17 Pct Recovery = 90% Analysis Date = 01/21/17 Pct Recovery = 90% Analysis Date = 01/18/17 Pct Recovery = 90% Analysis Date = 01/18/17 Pct Recovery = 90% Analysis Date = 01/15/17 Pct Recovery = 90% Analysis Date = 01/15/17 Pct Recovery = 90% Analysis Date = 01/13/17 Pct Recovery = 90% Analysis Date = 01/13/17 Pct Recovery = 90% Analysis Date = 01/10/17 Pct Recovery = 90% Analysis Date = 01/10/17 Pct Recovery = 90% Analysis Date = 01/07/17 Pct Recovery = 90% Analysis Date = 01/07/17 Pct Recovery = 90% Analysis Date = 01/04/17 Pct Recovery = 89% Analysis Date = 01/04/17 Pct Recovery = 89% Analysis Date = 01/02/17 Pct Recovery = 89% Analysis Date = 01/02/17 Pct Recovery = 89% Analysis Date = 12/30/16 Pct Recovery = 89% Analysis Date = 12/30/16 Pct Recovery = 89% Analysis Date = 12/27/16 Pct Recovery = 89% Analysis Date = 12/27/16 Pct Recovery = 89% Analysis Date = 12/24/16 Pct Recovery = 89% Analysis Date = 12/24/16 Pct Recovery = 89% Analysis Date = 12/22/16 Pct Recovery = 89% Analysis Date = 12/22/16 Pct Recovery = 89% Analysis Date = 12/19/16 Pct Recovery = 89% Analysis Date = 12/19/16 Pct Recovery = 89% Analysis Date = 12/16/16 Pct Recovery = 89% Analysis Date = 12/16/16 Pct Recovery = 89% Analysis Date = 12/13/16 Pct Recovery = 89% Analysis Date = 12/13/16 Pct Recovery = 89% Analysis Date = 12/11/16 Pct Recovery = 89% Analysis Date = 12/11/16 Pct Recovery = 89% Analysis Date = 12/08/16 Pct Recovery = 89% Analysis Date = 12/08/16 Pct Recovery = 89% Analysis Date = 12/05/16 Pct Recovery = 89% Analysis Date = 12/05/16 Pct Recovery = 89% Analysis Date = 12/02/16 Pct Recovery = 90% Analysis Date = 12/02/16 Pct Recovery = 90% Analysis Date = 11/30/16 Pct Recovery = 90% Analysis Date = 11/30/16 Pct Recovery = 90% Analysis Date = 11/27/16 Pct Recovery = 90% Analysis Date = 11/27/16 Pct Recovery = 90% Analysis Date = 11/24/16 Pct Recovery = 90% Analysis Date = 11/24/16 Pct Recovery = 90% Analysis Date = 11/21/16 Pct Recovery = 90% Analysis Date = 11/21/16 Pct Recovery = 90% Analysis Date = 11/19/16 Pct Recovery = 90% Analysis Date = 11/19/16 Pct Recovery = 90% Analysis Date = 11/16/16 Pct Recovery = 90% Analysis Date = 11/16/16 Pct Recovery = 90% Analysis Date = 11/13/16 Pct Recovery = 90% Analysis Date = 11/13/16 Pct Recovery = 90% Analysis Date = 11/10/16 Pct Recovery = 90% Analysis Date = 11/10/16 Pct Recovery = 90% Analysis Date = 11/07/16 Pct Recovery = 90% Analysis Date = 11/07/16 Pct Recovery = 90% Analysis Date = 11/05/16 Pct Recovery = 90% Analysis Date = 11/05/16 Pct Recovery = 90% Analysis Date = 11/02/16 Pct Recovery = 90% Analysis Date = 11/02/16 Pct Recovery = 90% Analysis Date = 10/30/16 Pct Recovery = 90% Analysis Date = 10/30/16 Pct Recovery = 90% Analysis Date = 10/27/16 Pct Recovery = 90% Analysis Date = 10/27/16 Pct Recovery = 90% Analysis Date = 10/25/16 Pct Recovery = 90% Analysis Date = 10/25/16 Pct Recovery = 90% Analysis Date = 10/22/16 Pct Recovery = 90% Analysis Date = 10/22/16 Pct Recovery = 90% Analysis Date = 10/19/16 Pct Recovery = 90% Analysis Date = 10/19/16 Pct Recovery = 90% Analysis Date = 10/16/16 Pct Recovery = 90% Analysis Date = 10/16/16 Pct Recovery = 90% Analysis Date = 10/14/16 Pct Recovery = 90% Analysis Date = 10/14/16 Pct Recovery = 90% Analysis Date = 10/11/16 Pct Recovery = 91% Analysis Date = 10/11/16 Pct Recovery = 91% Analysis Date = 10/08/16 Pct Recovery = 91% Analysis Date = 10/08/16 Pct Recovery = 91% Analysis Date = 10/05/16 Pct Recovery = 91% Analysis Date = 10/05/16 Pct Recovery = 91% Analysis Date = 10/03/16 Pct Recovery = 91% Analysis Date = 10/03/16 Pct Recovery = 91% Analysis Date = 09/30/16 Pct Recovery = 91% Analysis Date = 09/30/16 Pct Recovery = 91% Analysis Date = 09/27/16 Pct Recovery = 91% Analysis Date = 09/27/16 Pct Recovery = 91% Analysis Date = 09/24/16 Pct Recovery = 91% Analysis Date = 09/24/16 Pct Recovery = 91% Analysis Date = 09/22/16 Pct Recovery = 91% Analysis Date = 09/22/16 Pct Recovery = 91% Analysis Date = 09/19/16 Pct Recovery = 91% Analysis Date = 09/19/16 Pct Recovery = 91% Analysis Date = 09/16/16 Pct Recovery = 91% Analysis Date = 09/16/16 Pct Recovery = 91% Analysis Date = 09/13/16 Pct Recovery = 91% Analysis Date = 09/13/16 Pct Recovery = 91% Analysis Date = 09/11/16 Pct Recovery = 91% Analysis Date = 09/11/16 Pct Recovery = 91% Analysis Date = 09/08/16 Pct Recovery = 91% Analysis Date = 09/08/16 Pct Recovery = 91% Analysis Date = 09/05/16 Pct Recovery = 91% Analysis Date = 09/05/16 Pct Recovery = 91% Analysis Date = 09/02/16 Pct Recovery = 91% Analysis Date = 09/02/16 Pct Recovery = 91% Analysis Date = 08/31/16 Pct Recovery = 91% Analysis Date = 08/31/16 Pct Recovery = 91% Analysis Date = 08/28/16 Pct Recovery = 91% Analysis Date = 08/28/16 Pct Recovery = 91% Analysis Date = 08/25/16 Pct Recovery = 91% Analysis Date = 08/25/16 Pct Recovery = 91% Analysis Date = 08/22/16 Pct Recovery = 91% Analysis Date = 08/22/16 Pct Recovery = 91% Analysis Date = 08/20/16 Pct Recovery = 91% Analysis Date = 08/20/16 Pct Recovery = 91% Analysis Date = 08/17/16 Pct Recovery = 92% Analysis Date = 08/17/16 Pct Recovery = 92% Analysis Date = 08/14/16 Pct Recovery = 92% Analysis Date = 08/14/16 Pct Recovery = 92% Analysis Date = 08/11/16 Pct Recovery = 92% Analysis Date = 08/11/16 Pct Recovery = 92% Analysis Date = 08/09/16 Pct Recovery = 92% Analysis Date = 08/09/16 Pct Recovery = 92% Analysis Date = 08/06/16 Pct Recovery = 92% Analysis Date = 08/06/16 Pct Recovery = 92% Analysis Date = 08/03/16 Pct Recovery = 92% Analysis Date = 08/03/16 Pct Recovery = 92% Analysis Date = 07/31/16 Pct Recovery = 92% Analysis Date = 07/31/16 Pct Recovery = 92% Analysis Date = 07/29/16 Pct Recovery = 92% Analysis Date = 07/29/16 Pct Recovery = 92% Analysis Date = 07/26/16 Pct Recovery = 93% Analysis Date = 07/26/16 Pct Recovery = 93% Analysis Date = 07/23/16 Pct Recovery = 93% Analysis Date = 07/23/16 Pct Recovery = 93% Analysis Date = 07/20/16 Pct Recovery = 93% Analysis Date = 07/20/16 Pct Recovery = 93% Analysis Date = 07/18/16 Pct Recovery = 93% Analysis Date = 07/18/16 Pct Recovery = 93% Analysis Date = 07/15/16 Pct Recovery = 93% Analysis Date = 07/15/16 Pct Recovery = 93% Analysis Date = 07/12/16 Pct Recovery = 93% Analysis Date = 07/12/16 Pct Recovery = 93% Analysis Date = 07/09/16 Pct Recovery = 93% Analysis Date = 07/09/16 Pct Recovery = 93% Analysis Date = 07/07/16 Pct Recovery = 94% Analysis Date = 07/07/16 Pct Recovery = 94% Analysis Date = 07/04/16 Pct Recovery = 94% Analysis Date = 07/04/16 Pct Recovery = 94% Analysis Date = 07/01/16 Pct Recovery = 94% Analysis Date = 07/01/16 Pct Recovery = 94% Analysis Date = 06/28/16 Pct Recovery = 94% Analysis Date = 06/28/16 Pct Recovery = 94% Analysis Date = 06/25/16 Pct Recovery = 94% Analysis Date = 06/25/16 Pct Recovery = 94% Analysis Date = 06/23/16 Pct Recovery = 94% Analysis Date = 06/23/16 Pct Recovery = 94% Analysis Date = 06/20/16 Pct Recovery = 94% Analysis Date = 06/20/16 Pct Recovery = 94% Analysis Date = 06/17/16 Pct Recovery = 94% Analysis Date = 06/17/16 Pct Recovery = 94% Analysis Date = 06/14/16 Pct Recovery = 95% Analysis Date = 06/14/16 Pct Recovery = 95% Analysis Date = 06/12/16 Pct Recovery = 95% Analysis Date = 06/12/16 Pct Recovery = 95% Analysis Date = 06/09/16 Pct Recovery = 95% Analysis Date = 06/09/16 Pct Recovery = 95% Analysis Date = 06/06/16 Pct Recovery = 95% Analysis Date = 06/06/16 Pct Recovery = 95% Analysis Date = 06/03/16 Pct Recovery = 95% Analysis Date = 06/03/16 Pct Recovery = 95% Analysis Date = 06/01/16 Pct Recovery = 95% Analysis Date = 06/01/16 Pct Recovery = 95% Analysis Date = 05/29/16 Pct Recovery = 95% Analysis Date = 05/29/16 Pct Recovery = 95% Analysis Date = 05/26/16 Pct Recovery = 95% Analysis Date = 05/26/16 Pct Recovery = 95% Analysis Date = 05/23/16 Pct Recovery = 95% Analysis Date = 05/23/16 Pct Recovery = 95% Analysis Date = 05/21/16 Pct Recovery = 95% Analysis Date = 05/21/16 Pct Recovery = 95% Analysis Date = 05/18/16 Pct Recovery = 95% Analysis Date = 05/18/16 Pct Recovery = 95% Analysis Date = 05/15/16 Pct Recovery = 95% Analysis Date = 05/15/16 Pct Recovery = 95% Analysis Date = 05/12/16 Pct Recovery = 95% Analysis Date = 05/12/16 Pct Recovery = 95% Analysis Date = 05/10/16 Pct Recovery = 95% Analysis Date = 05/10/16 Pct Recovery = 95% Analysis Date = 05/07/16 Pct Recovery = 95% Analysis Date = 05/07/16 Pct Recovery = 95% Analysis Date = 05/04/16 Pct Recovery = 95% Analysis Date = 05/04/16 Pct Recovery = 95% Analysis Date = 05/01/16 Pct Recovery = 95% Analysis Date = 05/01/16 Pct Recovery = 95% Analysis Date = 04/29/16 Pct Recovery = 95% Analysis Date = 04/29/16 Pct Recovery = 95% Analysis Date = 04/26/16 Pct Recovery = 96% Analysis Date = 04/26/16 Pct Recovery = 96% Analysis Date = 04/23/16 Pct Recovery = 96% Analysis Date = 04/23/16 Pct Recovery = 96% Analysis Date = 04/20/16 Pct Recovery = 96% Analysis Date = 04/20/16 Pct Recovery = 96% Analysis Date = 04/18/16 Pct Recovery = 96% Analysis Date = 04/18/16 Pct Recovery = 96% Analysis Date = 04/15/16 Pct Recovery = 96% Analysis Date = 04/15/16 Pct Recovery = 96% Analysis Date = 04/12/16 Pct Recovery = 96% Analysis Date = 04/12/16 Pct Recovery = 96% Analysis Date = 04/09/16 Pct Recovery = 96% Analysis Date = 04/09/16 Pct Recovery = 96% Analysis Date = 04/07/16 Pct Recovery = 96% Analysis Date = 04/07/16 Pct Recovery = 96% Analysis Date = 04/04/16 Pct Recovery = 96% Analysis Date = 04/04/16 Pct Recovery = 96% Analysis Date = 04/01/16 Pct Recovery = 96% Analysis Date = 04/01/16 Pct Recovery = 96% Analysis Date = 03/29/16 Pct Recovery = 96% Analysis Date = 03/29/16 Pct Recovery = 96% Analysis Date = 03/27/16 Pct Recovery = 96% Analysis Date = 03/27/16 Pct Recovery = 96% Analysis Date = 03/24/16 Pct Recovery = 96% Analysis Date = 03/24/16 Pct Recovery = 96% Analysis Date = 03/21/16 Pct Recovery = 96% Analysis Date = 03/21/16 Pct Recovery = 96% Analysis Date = 03/18/16 Pct Recovery = 96% Analysis Date = 03/18/16 Pct Recovery = 96% Analysis Date = 03/16/16 Pct Recovery = 96% Analysis Date = 03/16/16 Pct Recovery = 96% Analysis Date = 03/13/16 Pct Recovery = 96% Analysis Date = 03/13/16 Pct Recovery = 96% Analysis Date = 03/10/16 Pct Recovery = 96% Analysis Date = 03/10/16 Pct Recovery = 96% Analysis Date = 03/07/16 Pct Recovery = 96% Analysis Date = 03/07/16 Pct Recovery = 96% Analysis Date = 03/05/16 Pct Recovery = 97% Analysis Date = 03/05/16 Pct Recovery = 97% Analysis Date = 03/02/16 Pct Recovery = 97% Analysis Date = 03/02/16 Pct Recovery = 97% Analysis Date = 02/28/16 Pct Recovery = 97% Analysis Date = 02/28/16 Pct Recovery = 97% Analysis Date = 02/25/16 Pct Recovery = 97% Analysis Date = 02/25/16 Pct Recovery = 97% Analysis Date = 02/23/16 Pct Recovery = 97% Analysis Date = 02/23/16 Pct Recovery = 97% Analysis Date = 02/20/16 Pct Recovery = 97% Analysis Date = 02/20/16 Pct Recovery = 97% Analysis Date = 02/17/16 Pct Recovery = 97% Analysis Date = 02/17/16 Pct Recovery = 97% Analysis Date = 02/14/16 Pct Recovery = 97% Analysis Date = 02/14/16 Pct Recovery = 97% Analysis Date = 02/12/16 Pct Recovery = 97% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
4-HEPTANONE, 2,6-DIMETHYL-

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 32 93% 7% 91% 8%
Total 32 93% 7% 91% 8%

Sample Statistics
4-HEPTANONE, 2,6-DIMETHYL-

Characteristic N % % Basis
Plotted 32 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 32 .  
False Negatives 0 0% 0 out of 32
Not Spiked 17 .  
False Positives 3 18% 3 out of 17