OBSP Determination:
SULFAMETHIZOLE
METHOD: 2440 , TESTIDCODE: 67476LCM56

Analysis Date = 09/21/17 SpikeMix = Abs 072517Pharm2: 80 µl & Abs 071817Pharm: 80 µl Pct Recovery = 95% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 88% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 85% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 80% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 74% Analysis Date = 08/10/17 SpikeMix = Crescent EN160610015: 80 µl & ERA 04281603: 80 µl Pct Recovery = 89% Analysis Date = 07/14/17 SpikeMix = Crescent EN160610015: 80 µl & ERA 04281603: 80 µl Pct Recovery = 75% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 75% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 74% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 75% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 71% Analysis Date = 07/15/17 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 104% Analysis Date = 06/17/17 SpikeMix = Abs 061416: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 86% Analysis Date = 06/08/17 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 77% Analysis Date = 04/20/17 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 81% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 78% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 78% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 87% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 80% Analysis Date = 10/21/17 SpikeMix = ERA 06281702: 50 µl & ERA 06281703: 50 µl Pct Recovery = 75% Analysis Date = 08/28/17 SpikeMix = Abs 072517Pharm1: 50 µl & Abs 072517Pharm2: 50 µl Pct Recovery = 82% Analysis Date = 08/25/17 SpikeMix = Abs 072517Pharm2: 50 µl & Abs 071817Pharm: 50 µl Pct Recovery = 74% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 77% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 67% Analysis Date = 06/18/17 SpikeMix = Crescent EN160610015: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 87% Analysis Date = 06/07/17 SpikeMix = Crescent EN160610015: 40 µl & ERA 04281604: 40 µl Pct Recovery = 73% Analysis Date = 04/07/17 SpikeMix = ERA 04281603: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 77% Analysis Date = 04/07/17 SpikeMix = ERA 04281603: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 65% Analysis Date = 03/14/17 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 80% Analysis Date = 03/14/17 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 80% Analysis Date = 03/14/17 SpikeMix = Crescent EN160610015: 40 µl & ERA 04281604: 40 µl Pct Recovery = 89% Analysis Date = 03/14/17 SpikeMix = Crescent EN160610015: 40 µl & ERA 04281604: 40 µl Pct Recovery = 81% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 67% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 75% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 73% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 77% Analysis Date = 02/07/17 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 74% Analysis Date = 02/07/17 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 78% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 76% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 73% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 81% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 76% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 68% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 65% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 64% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 57% Analysis Date = 11/09/17 SpikeMix = ERA 06281702: 20 µl & Abs 072517Pharm2: 20 µl Pct Recovery = 76% Analysis Date = 11/08/17 SpikeMix = Abs 072517Pharm2: 20 µl & ERA 06281704: 20 µl Pct Recovery = 105% Analysis Date = 10/22/17 SpikeMix = ERA 06281703: 20 µl & ERA 06281704: 20 µl Pct Recovery = 72% Analysis Date = 09/23/17 SpikeMix = Abs 072517Pharm1: 20 µl & Abs 072517Pharm2: 20 µl Pct Recovery = 87% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 47% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 51% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 104% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 75% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 81% Analysis Date = 08/11/17 SpikeMix = Abs 060916PHARM: 20 µl & Abs 071817Pharm: 20 µl Pct Recovery = 52% Analysis Date = 11/09/17 Pct Recovery = 83% Analysis Date = 11/06/17 Pct Recovery = 83% Analysis Date = 11/06/17 Pct Recovery = 83% Analysis Date = 11/03/17 Pct Recovery = 83% Analysis Date = 11/03/17 Pct Recovery = 83% Analysis Date = 10/31/17 Pct Recovery = 83% Analysis Date = 10/31/17 Pct Recovery = 83% Analysis Date = 10/28/17 Pct Recovery = 83% Analysis Date = 10/28/17 Pct Recovery = 83% Analysis Date = 10/25/17 Pct Recovery = 83% Analysis Date = 10/25/17 Pct Recovery = 83% Analysis Date = 10/22/17 Pct Recovery = 83% Analysis Date = 10/22/17 Pct Recovery = 83% Analysis Date = 10/19/17 Pct Recovery = 83% Analysis Date = 10/19/17 Pct Recovery = 83% Analysis Date = 10/16/17 Pct Recovery = 83% Analysis Date = 10/16/17 Pct Recovery = 83% Analysis Date = 10/13/17 Pct Recovery = 83% Analysis Date = 10/13/17 Pct Recovery = 83% Analysis Date = 10/11/17 Pct Recovery = 83% Analysis Date = 10/11/17 Pct Recovery = 83% Analysis Date = 10/08/17 Pct Recovery = 83% Analysis Date = 10/08/17 Pct Recovery = 83% Analysis Date = 10/05/17 Pct Recovery = 83% Analysis Date = 10/05/17 Pct Recovery = 83% Analysis Date = 10/02/17 Pct Recovery = 83% Analysis Date = 10/02/17 Pct Recovery = 83% Analysis Date = 09/29/17 Pct Recovery = 83% Analysis Date = 09/29/17 Pct Recovery = 83% Analysis Date = 09/26/17 Pct Recovery = 83% Analysis Date = 09/26/17 Pct Recovery = 83% Analysis Date = 09/23/17 Pct Recovery = 82% Analysis Date = 09/23/17 Pct Recovery = 82% Analysis Date = 09/20/17 Pct Recovery = 82% Analysis Date = 09/20/17 Pct Recovery = 82% Analysis Date = 09/17/17 Pct Recovery = 82% Analysis Date = 09/17/17 Pct Recovery = 82% Analysis Date = 09/14/17 Pct Recovery = 82% Analysis Date = 09/14/17 Pct Recovery = 82% Analysis Date = 09/12/17 Pct Recovery = 82% Analysis Date = 09/12/17 Pct Recovery = 82% Analysis Date = 09/09/17 Pct Recovery = 82% Analysis Date = 09/09/17 Pct Recovery = 82% Analysis Date = 09/06/17 Pct Recovery = 82% Analysis Date = 09/06/17 Pct Recovery = 82% Analysis Date = 09/03/17 Pct Recovery = 82% Analysis Date = 09/03/17 Pct Recovery = 82% Analysis Date = 08/31/17 Pct Recovery = 82% Analysis Date = 08/31/17 Pct Recovery = 82% Analysis Date = 08/28/17 Pct Recovery = 82% Analysis Date = 08/28/17 Pct Recovery = 82% Analysis Date = 08/25/17 Pct Recovery = 82% Analysis Date = 08/25/17 Pct Recovery = 82% Analysis Date = 08/22/17 Pct Recovery = 82% Analysis Date = 08/22/17 Pct Recovery = 82% Analysis Date = 08/19/17 Pct Recovery = 82% Analysis Date = 08/19/17 Pct Recovery = 82% Analysis Date = 08/17/17 Pct Recovery = 82% Analysis Date = 08/17/17 Pct Recovery = 82% Analysis Date = 08/14/17 Pct Recovery = 82% Analysis Date = 08/14/17 Pct Recovery = 82% Analysis Date = 08/11/17 Pct Recovery = 81% Analysis Date = 08/11/17 Pct Recovery = 81% Analysis Date = 08/08/17 Pct Recovery = 81% Analysis Date = 08/08/17 Pct Recovery = 81% Analysis Date = 08/05/17 Pct Recovery = 81% Analysis Date = 08/05/17 Pct Recovery = 81% Analysis Date = 08/02/17 Pct Recovery = 81% Analysis Date = 08/02/17 Pct Recovery = 81% Analysis Date = 07/30/17 Pct Recovery = 81% Analysis Date = 07/30/17 Pct Recovery = 81% Analysis Date = 07/27/17 Pct Recovery = 81% Analysis Date = 07/27/17 Pct Recovery = 81% Analysis Date = 07/24/17 Pct Recovery = 81% Analysis Date = 07/24/17 Pct Recovery = 81% Analysis Date = 07/21/17 Pct Recovery = 81% Analysis Date = 07/21/17 Pct Recovery = 81% Analysis Date = 07/19/17 Pct Recovery = 81% Analysis Date = 07/19/17 Pct Recovery = 81% Analysis Date = 07/16/17 Pct Recovery = 81% Analysis Date = 07/16/17 Pct Recovery = 81% Analysis Date = 07/13/17 Pct Recovery = 81% Analysis Date = 07/13/17 Pct Recovery = 81% Analysis Date = 07/10/17 Pct Recovery = 81% Analysis Date = 07/10/17 Pct Recovery = 81% Analysis Date = 07/07/17 Pct Recovery = 81% Analysis Date = 07/07/17 Pct Recovery = 81% Analysis Date = 07/04/17 Pct Recovery = 81% Analysis Date = 07/04/17 Pct Recovery = 81% Analysis Date = 07/01/17 Pct Recovery = 81% Analysis Date = 07/01/17 Pct Recovery = 81% Analysis Date = 06/28/17 Pct Recovery = 80% Analysis Date = 06/28/17 Pct Recovery = 80% Analysis Date = 06/25/17 Pct Recovery = 80% Analysis Date = 06/25/17 Pct Recovery = 80% Analysis Date = 06/23/17 Pct Recovery = 80% Analysis Date = 06/23/17 Pct Recovery = 80% Analysis Date = 06/20/17 Pct Recovery = 80% Analysis Date = 06/20/17 Pct Recovery = 80% Analysis Date = 06/17/17 Pct Recovery = 80% Analysis Date = 06/17/17 Pct Recovery = 80% Analysis Date = 06/14/17 Pct Recovery = 80% Analysis Date = 06/14/17 Pct Recovery = 80% Analysis Date = 06/11/17 Pct Recovery = 80% Analysis Date = 06/11/17 Pct Recovery = 80% Analysis Date = 06/08/17 Pct Recovery = 80% Analysis Date = 06/08/17 Pct Recovery = 80% Analysis Date = 06/05/17 Pct Recovery = 80% Analysis Date = 06/05/17 Pct Recovery = 80% Analysis Date = 06/02/17 Pct Recovery = 80% Analysis Date = 06/02/17 Pct Recovery = 80% Analysis Date = 05/30/17 Pct Recovery = 80% Analysis Date = 05/30/17 Pct Recovery = 80% Analysis Date = 05/27/17 Pct Recovery = 80% Analysis Date = 05/27/17 Pct Recovery = 80% Analysis Date = 05/25/17 Pct Recovery = 80% Analysis Date = 05/25/17 Pct Recovery = 80% Analysis Date = 05/22/17 Pct Recovery = 80% Analysis Date = 05/22/17 Pct Recovery = 80% Analysis Date = 05/19/17 Pct Recovery = 80% Analysis Date = 05/19/17 Pct Recovery = 80% Analysis Date = 05/16/17 Pct Recovery = 80% Analysis Date = 05/16/17 Pct Recovery = 80% Analysis Date = 05/13/17 Pct Recovery = 79% Analysis Date = 05/13/17 Pct Recovery = 79% Analysis Date = 05/10/17 Pct Recovery = 79% Analysis Date = 05/10/17 Pct Recovery = 79% Analysis Date = 05/07/17 Pct Recovery = 79% Analysis Date = 05/07/17 Pct Recovery = 79% Analysis Date = 05/04/17 Pct Recovery = 79% Analysis Date = 05/04/17 Pct Recovery = 79% Analysis Date = 05/01/17 Pct Recovery = 79% Analysis Date = 05/01/17 Pct Recovery = 79% Analysis Date = 04/29/17 Pct Recovery = 79% Analysis Date = 04/29/17 Pct Recovery = 79% Analysis Date = 04/26/17 Pct Recovery = 79% Analysis Date = 04/26/17 Pct Recovery = 79% Analysis Date = 04/23/17 Pct Recovery = 79% Analysis Date = 04/23/17 Pct Recovery = 79% Analysis Date = 04/20/17 Pct Recovery = 79% Analysis Date = 04/20/17 Pct Recovery = 79% Analysis Date = 04/17/17 Pct Recovery = 79% Analysis Date = 04/17/17 Pct Recovery = 79% Analysis Date = 04/14/17 Pct Recovery = 79% Analysis Date = 04/14/17 Pct Recovery = 79% Analysis Date = 04/11/17 Pct Recovery = 79% Analysis Date = 04/11/17 Pct Recovery = 79% Analysis Date = 04/08/17 Pct Recovery = 79% Analysis Date = 04/08/17 Pct Recovery = 79% Analysis Date = 04/05/17 Pct Recovery = 79% Analysis Date = 04/05/17 Pct Recovery = 79% Analysis Date = 04/02/17 Pct Recovery = 79% Analysis Date = 04/02/17 Pct Recovery = 79% Analysis Date = 03/31/17 Pct Recovery = 79% Analysis Date = 03/31/17 Pct Recovery = 79% Analysis Date = 03/28/17 Pct Recovery = 79% Analysis Date = 03/28/17 Pct Recovery = 79% Analysis Date = 03/25/17 Pct Recovery = 78% Analysis Date = 03/25/17 Pct Recovery = 78% Analysis Date = 03/22/17 Pct Recovery = 78% Analysis Date = 03/22/17 Pct Recovery = 78% Analysis Date = 03/19/17 Pct Recovery = 78% Analysis Date = 03/19/17 Pct Recovery = 78% Analysis Date = 03/16/17 Pct Recovery = 78% Analysis Date = 03/16/17 Pct Recovery = 78% Analysis Date = 03/13/17 Pct Recovery = 78% Analysis Date = 03/13/17 Pct Recovery = 78% Analysis Date = 03/10/17 Pct Recovery = 78% Analysis Date = 03/10/17 Pct Recovery = 78% Analysis Date = 03/07/17 Pct Recovery = 78% Analysis Date = 03/07/17 Pct Recovery = 78% Analysis Date = 03/05/17 Pct Recovery = 78% Analysis Date = 03/05/17 Pct Recovery = 78% Analysis Date = 03/02/17 Pct Recovery = 78% Analysis Date = 03/02/17 Pct Recovery = 78% Analysis Date = 02/27/17 Pct Recovery = 78% Analysis Date = 02/27/17 Pct Recovery = 78% Analysis Date = 02/24/17 Pct Recovery = 78% Analysis Date = 02/24/17 Pct Recovery = 78% Analysis Date = 02/21/17 Pct Recovery = 78% Analysis Date = 02/21/17 Pct Recovery = 78% Analysis Date = 02/18/17 Pct Recovery = 78% Analysis Date = 02/18/17 Pct Recovery = 78% Analysis Date = 02/15/17 Pct Recovery = 78% Analysis Date = 02/15/17 Pct Recovery = 78% Analysis Date = 02/12/17 Pct Recovery = 78% Analysis Date = 02/12/17 Pct Recovery = 78% Analysis Date = 02/09/17 Pct Recovery = 77% Analysis Date = 02/09/17 Pct Recovery = 77% Analysis Date = 02/06/17 Pct Recovery = 77% Analysis Date = 02/06/17 Pct Recovery = 77% Analysis Date = 02/04/17 Pct Recovery = 77% Analysis Date = 02/04/17 Pct Recovery = 77% Analysis Date = 02/01/17 Pct Recovery = 77% Analysis Date = 02/01/17 Pct Recovery = 77% Analysis Date = 01/29/17 Pct Recovery = 77% Analysis Date = 01/29/17 Pct Recovery = 77% Analysis Date = 01/26/17 Pct Recovery = 77% Analysis Date = 01/26/17 Pct Recovery = 77% Analysis Date = 01/23/17 Pct Recovery = 77% Analysis Date = 01/23/17 Pct Recovery = 77% Analysis Date = 01/20/17 Pct Recovery = 77% Analysis Date = 01/20/17 Pct Recovery = 77% Analysis Date = 01/17/17 Pct Recovery = 77% Analysis Date = 01/17/17 Pct Recovery = 77% Analysis Date = 01/14/17 Pct Recovery = 77% Analysis Date = 01/14/17 Pct Recovery = 77% Analysis Date = 01/11/17 Pct Recovery = 77% Analysis Date = 01/11/17 Pct Recovery = 77% Analysis Date = 01/09/17 Pct Recovery = 77% Analysis Date = 01/09/17 Pct Recovery = 77% Analysis Date = 01/06/17 Pct Recovery = 77% Analysis Date = 01/06/17 Pct Recovery = 77% Analysis Date = 01/03/17 Pct Recovery = 77% Analysis Date = 01/03/17 Pct Recovery = 77% Analysis Date = 12/31/16 Pct Recovery = 77% Analysis Date = 12/31/16 Pct Recovery = 77% Analysis Date = 12/28/16 Pct Recovery = 77% Analysis Date = 12/28/16 Pct Recovery = 77% Analysis Date = 12/25/16 Pct Recovery = 77% Analysis Date = 12/25/16 Pct Recovery = 77% Analysis Date = 12/22/16 Pct Recovery = 77% Analysis Date = 12/22/16 Pct Recovery = 77% Analysis Date = 12/19/16 Pct Recovery = 77% Analysis Date = 12/19/16 Pct Recovery = 77% Analysis Date = 12/16/16 Pct Recovery = 77% Analysis Date = 12/16/16 Pct Recovery = 77% Analysis Date = 12/13/16 Pct Recovery = 77% Analysis Date = 12/13/16 Pct Recovery = 77% Analysis Date = 12/11/16 Pct Recovery = 77% Analysis Date = 12/11/16 Pct Recovery = 77% Analysis Date = 12/08/16 Pct Recovery = 77% Analysis Date = 12/08/16 Pct Recovery = 77% Analysis Date = 12/05/16 Pct Recovery = 77% Analysis Date = 12/05/16 Pct Recovery = 77% Analysis Date = 12/02/16 Pct Recovery = 76% Analysis Date = 12/02/16 Pct Recovery = 76% Analysis Date = 11/29/16 Pct Recovery = 76% Analysis Date = 11/29/16 Pct Recovery = 76% Analysis Date = 11/26/16 Pct Recovery = 76% Analysis Date = 11/26/16 Pct Recovery = 76% Analysis Date = 11/23/16 Pct Recovery = 76% Analysis Date = 11/23/16 Pct Recovery = 76% Analysis Date = 11/20/16 Pct Recovery = 76% Analysis Date = 11/20/16 Pct Recovery = 76% Analysis Date = 11/17/16 Pct Recovery = 76% Analysis Date = 11/17/16 Pct Recovery = 76% Analysis Date = 11/15/16 Pct Recovery = 76% Analysis Date = 11/15/16 Pct Recovery = 76% Analysis Date = 11/12/16 Pct Recovery = 76% Analysis Date = 11/12/16 Pct Recovery = 76% Analysis Date = 11/09/16 Pct Recovery = 76% Analysis Date = 11/09/16 Pct Recovery = 76% Analysis Date = 11/06/16 Pct Recovery = 76% Analysis Date = 11/06/16 Pct Recovery = 76% Analysis Date = 11/03/16 Pct Recovery = 76% Analysis Date = 11/03/16 Pct Recovery = 76% Analysis Date = 10/31/16 Pct Recovery = 76% Analysis Date = 10/31/16 Pct Recovery = 76% Analysis Date = 10/28/16 Pct Recovery = 75% Analysis Date = 10/28/16 Pct Recovery = 75% Analysis Date = 10/25/16 Pct Recovery = 75% Analysis Date = 10/25/16 Pct Recovery = 75% Analysis Date = 10/22/16 Pct Recovery = 75% Analysis Date = 10/22/16 Pct Recovery = 75% Analysis Date = 10/19/16 Pct Recovery = 75% Analysis Date = 10/19/16 Pct Recovery = 75% Analysis Date = 10/17/16 Pct Recovery = 75% Analysis Date = 10/17/16 Pct Recovery = 75% Analysis Date = 10/14/16 Pct Recovery = 75% Analysis Date = 10/14/16 Pct Recovery = 75% Analysis Date = 10/11/16 Pct Recovery = 75% Analysis Date = 10/11/16 Pct Recovery = 75% Analysis Date = 10/08/16 Pct Recovery = 75% Analysis Date = 10/08/16 Pct Recovery = 75% Analysis Date = 10/05/16 Pct Recovery = 75% Analysis Date = 10/05/16 Pct Recovery = 75% Analysis Date = 10/02/16 Pct Recovery = 75% Analysis Date = 10/02/16 Pct Recovery = 75% Analysis Date = 09/29/16 Pct Recovery = 75% Analysis Date = 09/29/16 Pct Recovery = 75% Analysis Date = 09/26/16 Pct Recovery = 75% Analysis Date = 09/26/16 Pct Recovery = 75% Analysis Date = 09/23/16 Pct Recovery = 74% Analysis Date = 09/23/16 Pct Recovery = 74% Analysis Date = 09/21/16 Pct Recovery = 74% Analysis Date = 09/21/16 Pct Recovery = 74% Analysis Date = 09/18/16 Pct Recovery = 74% Analysis Date = 09/18/16 Pct Recovery = 74% Analysis Date = 09/15/16 Pct Recovery = 74% Analysis Date = 09/15/16 Pct Recovery = 74% Analysis Date = 09/12/16 Pct Recovery = 74% Analysis Date = 09/12/16 Pct Recovery = 74% Analysis Date = 09/09/16 Pct Recovery = 74% Analysis Date = 09/09/16 Pct Recovery = 74% Analysis Date = 09/06/16 Pct Recovery = 74% Analysis Date = 09/06/16 Pct Recovery = 74% Analysis Date = 09/03/16 Pct Recovery = 74% Analysis Date = 09/03/16 Pct Recovery = 74% Analysis Date = 08/31/16 Pct Recovery = 74% Analysis Date = 08/31/16 Pct Recovery = 74% Analysis Date = 08/28/16 Pct Recovery = 74% Analysis Date = 08/28/16 Pct Recovery = 74% Analysis Date = 08/25/16 Pct Recovery = 74% Analysis Date = 08/25/16 Pct Recovery = 74% Analysis Date = 08/23/16 Pct Recovery = 74% Analysis Date = 08/23/16 Pct Recovery = 74% Analysis Date = 08/20/16 Pct Recovery = 73% Analysis Date = 08/20/16 Pct Recovery = 73% Analysis Date = 08/17/16 Pct Recovery = 73% Analysis Date = 08/17/16 Pct Recovery = 73% Analysis Date = 08/14/16 Pct Recovery = 73% Analysis Date = 08/14/16 Pct Recovery = 73% Analysis Date = 08/11/16 Pct Recovery = 73% Analysis Date = 08/11/16 Pct Recovery = 73% Analysis Date = 08/08/16 Pct Recovery = 73% Analysis Date = 08/08/16 Pct Recovery = 73% Analysis Date = 08/05/16 Pct Recovery = 73% Analysis Date = 08/05/16 Pct Recovery = 73% Analysis Date = 08/02/16 Pct Recovery = 73% Analysis Date = 08/02/16 Pct Recovery = 73% Analysis Date = 07/30/16 Pct Recovery = 73% Analysis Date = 07/30/16 Pct Recovery = 73% Analysis Date = 07/28/16 Pct Recovery = 73% Analysis Date = 07/28/16 Pct Recovery = 73% Analysis Date = 07/25/16 Pct Recovery = 73% Analysis Date = 07/25/16 Pct Recovery = 73% Analysis Date = 07/22/16 Pct Recovery = 73% Analysis Date = 07/22/16 Pct Recovery = 73% Analysis Date = 07/19/16 Pct Recovery = 73% Analysis Date = 07/19/16 Pct Recovery = 73% Analysis Date = 07/16/16 Pct Recovery = 73% Analysis Date = 07/16/16 Pct Recovery = 73% Analysis Date = 07/13/16 Pct Recovery = 73% Analysis Date = 07/13/16 Pct Recovery = 73% Analysis Date = 07/10/16 Pct Recovery = 73% Analysis Date = 07/10/16 Pct Recovery = 73% Analysis Date = 07/07/16 Pct Recovery = 73% Analysis Date = 07/07/16 Pct Recovery = 73% Analysis Date = 07/04/16 Pct Recovery = 73% Analysis Date = 07/04/16 Pct Recovery = 73% Analysis Date = 07/01/16 Pct Recovery = 73% Analysis Date = 07/01/16 Pct Recovery = 73% Analysis Date = 06/29/16 Pct Recovery = 73% Analysis Date = 06/29/16 Pct Recovery = 73% Analysis Date = 06/26/16 Pct Recovery = 73% Analysis Date = 06/26/16 Pct Recovery = 73% Analysis Date = 06/23/16 Pct Recovery = 73% Analysis Date = 06/23/16 Pct Recovery = 73% Analysis Date = 06/20/16 Pct Recovery = 73% Analysis Date = 06/20/16 Pct Recovery = 73% Analysis Date = 06/17/16 Pct Recovery = 73% Analysis Date = 06/17/16 Pct Recovery = 73% Analysis Date = 06/14/16 Pct Recovery = 73% Analysis Date = 06/14/16 Pct Recovery = 73% Analysis Date = 06/11/16 Pct Recovery = 73% Analysis Date = 06/11/16 Pct Recovery = 73% Analysis Date = 06/08/16 Pct Recovery = 73% Analysis Date = 06/08/16 Pct Recovery = 73% Analysis Date = 06/05/16 Pct Recovery = 73% Analysis Date = 06/05/16 Pct Recovery = 73% Analysis Date = 06/03/16 Pct Recovery = 73% Analysis Date = 06/03/16 Pct Recovery = 73% Analysis Date = 05/31/16 Pct Recovery = 73% Analysis Date = 05/31/16 Pct Recovery = 73% Analysis Date = 05/28/16 Pct Recovery = 72% Analysis Date = 05/28/16 Pct Recovery = 72% Analysis Date = 05/25/16 Pct Recovery = 72% Analysis Date = 05/25/16 Pct Recovery = 72% Analysis Date = 05/22/16 Pct Recovery = 72% Analysis Date = 05/22/16 Pct Recovery = 72% Analysis Date = 05/19/16 Pct Recovery = 72% Analysis Date = 05/19/16 Pct Recovery = 72% Analysis Date = 05/16/16 Pct Recovery = 72% Analysis Date = 05/16/16 Pct Recovery = 72% Analysis Date = 05/13/16 Pct Recovery = 72% Analysis Date = 05/13/16 Pct Recovery = 72% Analysis Date = 05/10/16 Pct Recovery = 72% Analysis Date = 05/10/16 Pct Recovery = 72% Analysis Date = 05/07/16 Pct Recovery = 72% Analysis Date = 05/07/16 Pct Recovery = 72% Analysis Date = 05/05/16 Pct Recovery = 72% Analysis Date = 05/05/16 Pct Recovery = 72% Analysis Date = 05/02/16 Pct Recovery = 72% Analysis Date = 05/02/16 Pct Recovery = 72% Analysis Date = 04/29/16 Pct Recovery = 72% Analysis Date = 04/29/16 Pct Recovery = 72% Analysis Date = 04/26/16 Pct Recovery = 72% Analysis Date = 04/26/16 Pct Recovery = 72% Analysis Date = 04/23/16 Pct Recovery = 72% Analysis Date = 04/23/16 Pct Recovery = 72% Analysis Date = 04/20/16 Pct Recovery = 72% Analysis Date = 04/20/16 Pct Recovery = 72% Analysis Date = 04/17/16 Pct Recovery = 72% Analysis Date = 04/17/16 Pct Recovery = 72% Analysis Date = 04/14/16 Pct Recovery = 72% Analysis Date = 04/14/16 Pct Recovery = 72% Analysis Date = 04/11/16 Pct Recovery = 72% Analysis Date = 04/11/16 Pct Recovery = 72% Analysis Date = 04/09/16 Pct Recovery = 72% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
SULFAMETHIZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 56 77% 11% 77% 6%
Total 56 77% 11% 77% 6%

Sample Statistics
SULFAMETHIZOLE

Characteristic N % % Basis
Plotted 56 100% Spiked
Estimated Values 2 4% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 56 .  
False Negatives 0 0% 0 out of 56
Not Spiked 30 .  
False Positives 0 0% 0 out of 30