OBSP Determination:
PIPERONYL BUTOXIDE
METHOD: 2440 , TESTIDCODE: 67435LCM56

Analysis Date = 10/22/17 SpikeMix = ERA 06281703: 20 µl & ERA 06281704: 20 µl Pct Recovery = 249% Analysis Date = 03/14/17 SpikeMix = Crescent EN160610015: 40 µl & ERA 04281604: 40 µl Pct Recovery = 1387% Analysis Date = 03/14/17 SpikeMix = Crescent EN160610015: 40 µl & ERA 04281604: 40 µl Pct Recovery = 1427% Analysis Date = 09/21/17 SpikeMix = Abs 072517Pharm2: 80 µl & Abs 071817Pharm: 80 µl Pct Recovery = 59% Analysis Date = 09/09/17 SpikeMix = Abs 071817Pharm: 80 µl & Abs 072517Pharm1: 80 µl Pct Recovery = 40% Analysis Date = 09/21/17 SpikeMix = Abs 071817Pharm: 50 µl & Abs 072517Pharm1: 50 µl Pct Recovery = 53% Analysis Date = 08/26/17 SpikeMix = Abs 072517Pharm1: 50 µl & Abs 071817Pharm: 50 µl Pct Recovery = 40% Analysis Date = 08/25/17 SpikeMix = Abs 072517Pharm2: 50 µl & Abs 071817Pharm: 50 µl Pct Recovery = 53% Analysis Date = 08/11/17 SpikeMix = Abs 060916PHARM: 20 µl & Abs 071817Pharm: 20 µl Pct Recovery = 23% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 37% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 29% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 70% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 80% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 99% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 109% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 39% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 38% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 35% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 36% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 26% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 46% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 37% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 41% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 88% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 22% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 42% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 35% Analysis Date = 02/07/17 SpikeMix = Abs 061416: 100 µl & ERA 04281603: 100 µl Pct Recovery = 45% Analysis Date = 02/07/17 SpikeMix = Abs 061416: 100 µl & ERA 04281603: 100 µl Pct Recovery = 42% Analysis Date = 06/17/17 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 73% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 32% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 41% Analysis Date = 07/15/17 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 13% Analysis Date = 06/17/17 SpikeMix = Abs 061416: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 42% Analysis Date = 06/08/17 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 49% Analysis Date = 06/07/17 SpikeMix = Crescent EN160610015: 40 µl & ERA 04281604: 40 µl Pct Recovery = 65% Analysis Date = 04/06/17 SpikeMix = ERA 04281604: 40 µl & ERA 04281603: 40 µl Pct Recovery = 71% Analysis Date = 04/06/17 SpikeMix = ERA 04281603: 40 µl & ERA 04281604: 40 µl Pct Recovery = 72% Analysis Date = 02/07/17 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 52% Analysis Date = 02/07/17 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 69% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 93% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 71% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 65% Analysis Date = 05/11/17 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 72% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 17% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 24% Analysis Date = 10/19/17 Pct Recovery = ( 3%) Analysis Date = 10/19/17 Pct Recovery = ( 3%) Analysis Date = 10/16/17 Pct Recovery = 1% Analysis Date = 10/16/17 Pct Recovery = 1% Analysis Date = 10/13/17 Pct Recovery = 5% Analysis Date = 10/13/17 Pct Recovery = 5% Analysis Date = 10/10/17 Pct Recovery = 8% Analysis Date = 10/10/17 Pct Recovery = 8% Analysis Date = 10/07/17 Pct Recovery = 12% Analysis Date = 10/07/17 Pct Recovery = 12% Analysis Date = 10/05/17 Pct Recovery = 16% Analysis Date = 10/05/17 Pct Recovery = 16% Analysis Date = 10/02/17 Pct Recovery = 19% Analysis Date = 10/02/17 Pct Recovery = 19% Analysis Date = 09/29/17 Pct Recovery = 23% Analysis Date = 09/29/17 Pct Recovery = 23% Analysis Date = 09/26/17 Pct Recovery = 27% Analysis Date = 09/26/17 Pct Recovery = 27% Analysis Date = 09/23/17 Pct Recovery = 30% Analysis Date = 09/23/17 Pct Recovery = 30% Analysis Date = 09/21/17 Pct Recovery = 34% Analysis Date = 09/21/17 Pct Recovery = 34% Analysis Date = 09/18/17 Pct Recovery = 38% Analysis Date = 09/18/17 Pct Recovery = 38% Analysis Date = 09/15/17 Pct Recovery = 41% Analysis Date = 09/15/17 Pct Recovery = 41% Analysis Date = 09/12/17 Pct Recovery = 45% Analysis Date = 09/12/17 Pct Recovery = 45% Analysis Date = 09/09/17 Pct Recovery = 49% Analysis Date = 09/09/17 Pct Recovery = 49% Analysis Date = 09/07/17 Pct Recovery = 52% Analysis Date = 09/07/17 Pct Recovery = 52% Analysis Date = 09/04/17 Pct Recovery = 56% Analysis Date = 09/04/17 Pct Recovery = 56% Analysis Date = 09/01/17 Pct Recovery = 60% Analysis Date = 09/01/17 Pct Recovery = 60% Analysis Date = 08/29/17 Pct Recovery = 63% Analysis Date = 08/29/17 Pct Recovery = 63% Analysis Date = 08/26/17 Pct Recovery = 67% Analysis Date = 08/26/17 Pct Recovery = 67% Analysis Date = 08/24/17 Pct Recovery = 71% Analysis Date = 08/24/17 Pct Recovery = 71% Analysis Date = 08/21/17 Pct Recovery = 75% Analysis Date = 08/21/17 Pct Recovery = 75% Analysis Date = 08/18/17 Pct Recovery = 78% Analysis Date = 08/18/17 Pct Recovery = 78% Analysis Date = 08/15/17 Pct Recovery = 82% Analysis Date = 08/15/17 Pct Recovery = 82% Analysis Date = 08/12/17 Pct Recovery = 86% Analysis Date = 08/12/17 Pct Recovery = 86% Analysis Date = 08/10/17 Pct Recovery = 90% Analysis Date = 08/10/17 Pct Recovery = 90% Analysis Date = 08/07/17 Pct Recovery = 94% Analysis Date = 08/07/17 Pct Recovery = 94% Analysis Date = 08/04/17 Pct Recovery = 97% Analysis Date = 08/04/17 Pct Recovery = 97% Analysis Date = 08/01/17 Pct Recovery = 101% Analysis Date = 08/01/17 Pct Recovery = 101% Analysis Date = 07/29/17 Pct Recovery = 105% Analysis Date = 07/29/17 Pct Recovery = 105% Analysis Date = 07/27/17 Pct Recovery = 109% Analysis Date = 07/27/17 Pct Recovery = 109% Analysis Date = 07/24/17 Pct Recovery = 113% Analysis Date = 07/24/17 Pct Recovery = 113% Analysis Date = 07/21/17 Pct Recovery = 116% Analysis Date = 07/21/17 Pct Recovery = 116% Analysis Date = 07/18/17 Pct Recovery = 120% Analysis Date = 07/18/17 Pct Recovery = 120% Analysis Date = 07/15/17 Pct Recovery = 124% Analysis Date = 07/15/17 Pct Recovery = 124% Analysis Date = 07/13/17 Pct Recovery = 128% Analysis Date = 07/13/17 Pct Recovery = 128% Analysis Date = 07/10/17 Pct Recovery = 132% Analysis Date = 07/10/17 Pct Recovery = 132% Analysis Date = 07/07/17 Pct Recovery = 135% Analysis Date = 07/07/17 Pct Recovery = 135% Analysis Date = 07/04/17 Pct Recovery = 139% Analysis Date = 07/04/17 Pct Recovery = 139% Analysis Date = 07/01/17 Pct Recovery = 143% Analysis Date = 07/01/17 Pct Recovery = 143% Analysis Date = 06/28/17 Pct Recovery = 147% Analysis Date = 06/28/17 Pct Recovery = 147% Analysis Date = 06/26/17 Pct Recovery = 151% Analysis Date = 06/26/17 Pct Recovery = 151% Analysis Date = 06/23/17 Pct Recovery = 154% Analysis Date = 06/23/17 Pct Recovery = 154% Analysis Date = 06/20/17 Pct Recovery = 158% Analysis Date = 06/20/17 Pct Recovery = 158% Analysis Date = 06/17/17 Pct Recovery = 162% Analysis Date = 06/17/17 Pct Recovery = 162% Analysis Date = 06/14/17 Pct Recovery = 166% Analysis Date = 06/14/17 Pct Recovery = 166% Analysis Date = 06/12/17 Pct Recovery = 169% Analysis Date = 06/12/17 Pct Recovery = 169% Analysis Date = 06/09/17 Pct Recovery = 173% Analysis Date = 06/09/17 Pct Recovery = 173% Analysis Date = 06/06/17 Pct Recovery = 176% Analysis Date = 06/06/17 Pct Recovery = 176% Analysis Date = 06/03/17 Pct Recovery = 179% Analysis Date = 06/03/17 Pct Recovery = 179% Analysis Date = 05/31/17 Pct Recovery = 183% Analysis Date = 05/31/17 Pct Recovery = 183% Analysis Date = 05/29/17 Pct Recovery = 186% Analysis Date = 05/29/17 Pct Recovery = 186% Analysis Date = 05/26/17 Pct Recovery = 190% Analysis Date = 05/26/17 Pct Recovery = 190% Analysis Date = 05/23/17 Pct Recovery = 193% Analysis Date = 05/23/17 Pct Recovery = 193% Analysis Date = 05/20/17 Pct Recovery = 197% Analysis Date = 05/20/17 Pct Recovery = 197% Analysis Date = 05/17/17 Pct Recovery = 200% Analysis Date = 05/17/17 Pct Recovery = 200% Analysis Date = 05/15/17 Pct Recovery = 204% Analysis Date = 05/15/17 Pct Recovery = 204% Analysis Date = 01/17/17 Pct Recovery = 207% Analysis Date = 01/14/17 Pct Recovery = 198% Analysis Date = 01/14/17 Pct Recovery = 198% Analysis Date = 01/11/17 Pct Recovery = 190% Analysis Date = 01/11/17 Pct Recovery = 190% Analysis Date = 01/08/17 Pct Recovery = 182% Analysis Date = 01/08/17 Pct Recovery = 182% Analysis Date = 01/06/17 Pct Recovery = 174% Analysis Date = 01/06/17 Pct Recovery = 174% Analysis Date = 01/03/17 Pct Recovery = 165% Analysis Date = 01/03/17 Pct Recovery = 165% Analysis Date = 12/31/16 Pct Recovery = 157% Analysis Date = 12/31/16 Pct Recovery = 157% Analysis Date = 12/28/16 Pct Recovery = 149% Analysis Date = 12/28/16 Pct Recovery = 149% Analysis Date = 12/25/16 Pct Recovery = 141% Analysis Date = 12/25/16 Pct Recovery = 141% Analysis Date = 12/23/16 Pct Recovery = 132% Analysis Date = 12/23/16 Pct Recovery = 132% Analysis Date = 12/20/16 Pct Recovery = 124% Analysis Date = 12/20/16 Pct Recovery = 124% Analysis Date = 12/17/16 Pct Recovery = 116% Analysis Date = 12/17/16 Pct Recovery = 116% Analysis Date = 12/14/16 Pct Recovery = 110% Analysis Date = 12/14/16 Pct Recovery = 110% Analysis Date = 12/11/16 Pct Recovery = 106% Analysis Date = 12/11/16 Pct Recovery = 106% Analysis Date = 12/09/16 Pct Recovery = 102% Analysis Date = 12/09/16 Pct Recovery = 102% Analysis Date = 12/06/16 Pct Recovery = 98% Analysis Date = 12/06/16 Pct Recovery = 98% Analysis Date = 12/03/16 Pct Recovery = 94% Analysis Date = 12/03/16 Pct Recovery = 94% Analysis Date = 11/30/16 Pct Recovery = 90% Analysis Date = 11/30/16 Pct Recovery = 90% Analysis Date = 11/27/16 Pct Recovery = 85% Analysis Date = 11/27/16 Pct Recovery = 85% Analysis Date = 11/25/16 Pct Recovery = 81% Analysis Date = 11/25/16 Pct Recovery = 81% Analysis Date = 11/22/16 Pct Recovery = 77% Analysis Date = 11/22/16 Pct Recovery = 77% Analysis Date = 11/19/16 Pct Recovery = 73% Analysis Date = 11/19/16 Pct Recovery = 73% Analysis Date = 11/16/16 Pct Recovery = 69% Analysis Date = 11/16/16 Pct Recovery = 69% Analysis Date = 11/13/16 Pct Recovery = 65% Analysis Date = 11/13/16 Pct Recovery = 65% Analysis Date = 11/10/16 Pct Recovery = 61% Analysis Date = 11/10/16 Pct Recovery = 61% Analysis Date = 11/08/16 Pct Recovery = 57% Analysis Date = 11/08/16 Pct Recovery = 57% Analysis Date = 11/05/16 Pct Recovery = 53% Analysis Date = 11/05/16 Pct Recovery = 53% Analysis Date = 11/02/16 Pct Recovery = 49% Analysis Date = 11/02/16 Pct Recovery = 49% Analysis Date = 10/30/16 Pct Recovery = 45% Analysis Date = 10/30/16 Pct Recovery = 45% Analysis Date = 10/27/16 Pct Recovery = 41% Analysis Date = 10/27/16 Pct Recovery = 41% Analysis Date = 10/25/16 Pct Recovery = 42% Analysis Date = 10/25/16 Pct Recovery = 42% Analysis Date = 10/22/16 Pct Recovery = 42% Analysis Date = 10/22/16 Pct Recovery = 42% Analysis Date = 10/19/16 Pct Recovery = 43% Analysis Date = 10/19/16 Pct Recovery = 43% Analysis Date = 10/16/16 Pct Recovery = 43% Analysis Date = 10/16/16 Pct Recovery = 43% Analysis Date = 10/13/16 Pct Recovery = 44% Analysis Date = 10/13/16 Pct Recovery = 44% Analysis Date = 10/11/16 Pct Recovery = 44% Analysis Date = 10/11/16 Pct Recovery = 44% Analysis Date = 10/08/16 Pct Recovery = 45% Analysis Date = 10/08/16 Pct Recovery = 45% Analysis Date = 10/05/16 Pct Recovery = 45% Analysis Date = 10/05/16 Pct Recovery = 45% Analysis Date = 10/02/16 Pct Recovery = 46% Analysis Date = 10/02/16 Pct Recovery = 46% Analysis Date = 09/29/16 Pct Recovery = 46% Analysis Date = 09/29/16 Pct Recovery = 46% Analysis Date = 09/27/16 Pct Recovery = 46% Analysis Date = 09/27/16 Pct Recovery = 46% Analysis Date = 09/24/16 Pct Recovery = 47% Analysis Date = 09/24/16 Pct Recovery = 47% Analysis Date = 09/21/16 Pct Recovery = 48% Analysis Date = 09/21/16 Pct Recovery = 48% Analysis Date = 09/18/16 Pct Recovery = 48% Analysis Date = 09/18/16 Pct Recovery = 48% Analysis Date = 09/15/16 Pct Recovery = 49% Analysis Date = 09/15/16 Pct Recovery = 49% Analysis Date = 09/13/16 Pct Recovery = 50% Analysis Date = 09/13/16 Pct Recovery = 50% Analysis Date = 09/10/16 Pct Recovery = 51% Analysis Date = 09/10/16 Pct Recovery = 51% Analysis Date = 09/07/16 Pct Recovery = 51% Analysis Date = 09/07/16 Pct Recovery = 51% Analysis Date = 09/04/16 Pct Recovery = 52% Analysis Date = 09/04/16 Pct Recovery = 52% Analysis Date = 09/01/16 Pct Recovery = 52% Analysis Date = 09/01/16 Pct Recovery = 52% Analysis Date = 08/30/16 Pct Recovery = 53% Analysis Date = 08/30/16 Pct Recovery = 53% Analysis Date = 08/27/16 Pct Recovery = 53% Analysis Date = 08/27/16 Pct Recovery = 53% Analysis Date = 08/24/16 Pct Recovery = 54% Analysis Date = 08/24/16 Pct Recovery = 54% Analysis Date = 08/21/16 Pct Recovery = 55% Analysis Date = 08/21/16 Pct Recovery = 55% Analysis Date = 08/18/16 Pct Recovery = 55% Analysis Date = 08/18/16 Pct Recovery = 55% Analysis Date = 08/16/16 Pct Recovery = 56% Analysis Date = 08/16/16 Pct Recovery = 56% Analysis Date = 08/13/16 Pct Recovery = 56% Analysis Date = 08/13/16 Pct Recovery = 56% Analysis Date = 08/10/16 Pct Recovery = 56% Analysis Date = 08/10/16 Pct Recovery = 56% Analysis Date = 08/07/16 Pct Recovery = 56% Analysis Date = 08/07/16 Pct Recovery = 56% Analysis Date = 08/04/16 Pct Recovery = 56% Analysis Date = 08/04/16 Pct Recovery = 56% Analysis Date = 08/02/16 Pct Recovery = 57% Analysis Date = 08/02/16 Pct Recovery = 57% Analysis Date = 07/30/16 Pct Recovery = 57% Analysis Date = 07/30/16 Pct Recovery = 57% Analysis Date = 07/27/16 Pct Recovery = 57% Analysis Date = 07/27/16 Pct Recovery = 57% Analysis Date = 07/24/16 Pct Recovery = 57% Analysis Date = 07/24/16 Pct Recovery = 57% Analysis Date = 07/21/16 Pct Recovery = 58% Analysis Date = 07/21/16 Pct Recovery = 58% Analysis Date = 07/18/16 Pct Recovery = 58% Analysis Date = 07/18/16 Pct Recovery = 58% Analysis Date = 07/16/16 Pct Recovery = 58% Analysis Date = 07/16/16 Pct Recovery = 58% Analysis Date = 07/13/16 Pct Recovery = 59% Analysis Date = 07/13/16 Pct Recovery = 59% Analysis Date = 07/10/16 Pct Recovery = 59% Analysis Date = 07/10/16 Pct Recovery = 59% Analysis Date = 07/07/16 Pct Recovery = 59% Analysis Date = 07/07/16 Pct Recovery = 59% Analysis Date = 07/04/16 Pct Recovery = 60% Analysis Date = 07/04/16 Pct Recovery = 60% Analysis Date = 07/02/16 Pct Recovery = 60% Analysis Date = 07/02/16 Pct Recovery = 60% Analysis Date = 06/29/16 Pct Recovery = 60% Analysis Date = 06/29/16 Pct Recovery = 60% Analysis Date = 06/26/16 Pct Recovery = 61% Analysis Date = 06/26/16 Pct Recovery = 61% Analysis Date = 06/23/16 Pct Recovery = 61% Analysis Date = 06/23/16 Pct Recovery = 61% Analysis Date = 06/20/16 Pct Recovery = 61% Analysis Date = 06/20/16 Pct Recovery = 61% Analysis Date = 06/18/16 Pct Recovery = 62% Analysis Date = 06/18/16 Pct Recovery = 62% Analysis Date = 06/15/16 Pct Recovery = 62% Analysis Date = 06/15/16 Pct Recovery = 62% Analysis Date = 06/12/16 Pct Recovery = 62% Analysis Date = 06/12/16 Pct Recovery = 62% Analysis Date = 06/09/16 Pct Recovery = 63% Analysis Date = 06/09/16 Pct Recovery = 63% Analysis Date = 06/06/16 Pct Recovery = 63% Analysis Date = 06/06/16 Pct Recovery = 63% Analysis Date = 06/04/16 Pct Recovery = 63% Analysis Date = 06/04/16 Pct Recovery = 63% Analysis Date = 06/01/16 Pct Recovery = 64% Analysis Date = 06/01/16 Pct Recovery = 64% Analysis Date = 05/29/16 Pct Recovery = 64% Analysis Date = 05/29/16 Pct Recovery = 64% Analysis Date = 05/26/16 Pct Recovery = 64% Analysis Date = 05/26/16 Pct Recovery = 64% Analysis Date = 05/23/16 Pct Recovery = 65% Analysis Date = 05/23/16 Pct Recovery = 65% Analysis Date = 05/21/16 Pct Recovery = 65% Analysis Date = 05/21/16 Pct Recovery = 65% Analysis Date = 05/18/16 Pct Recovery = 65% Analysis Date = 05/18/16 Pct Recovery = 65% Analysis Date = 05/15/16 Pct Recovery = 66% Analysis Date = 05/15/16 Pct Recovery = 66% Analysis Date = 05/12/16 Pct Recovery = 66% Analysis Date = 05/12/16 Pct Recovery = 66% Analysis Date = 05/09/16 Pct Recovery = 66% Analysis Date = 05/09/16 Pct Recovery = 66% Analysis Date = 05/07/16 Pct Recovery = 67% Analysis Date = 05/07/16 Pct Recovery = 67% Analysis Date = 05/04/16 Pct Recovery = 67% Analysis Date = 05/04/16 Pct Recovery = 67% Analysis Date = 05/01/16 Pct Recovery = 67% Analysis Date = 05/01/16 Pct Recovery = 67% Analysis Date = 04/28/16 Pct Recovery = 68% Analysis Date = 04/28/16 Pct Recovery = 68% Analysis Date = 04/25/16 Pct Recovery = 68% Analysis Date = 04/25/16 Pct Recovery = 68% Analysis Date = 04/23/16 Pct Recovery = 68% Analysis Date = 04/23/16 Pct Recovery = 68% Analysis Date = 04/20/16 Pct Recovery = 69% Analysis Date = 04/20/16 Pct Recovery = 69% Analysis Date = 04/17/16 Pct Recovery = 69% Analysis Date = 04/17/16 Pct Recovery = 69% Analysis Date = 04/14/16 Pct Recovery = 69% Analysis Date = 04/14/16 Pct Recovery = 69% Analysis Date = 04/11/16 Pct Recovery = 70% Analysis Date = 04/11/16 Pct Recovery = 70% Analysis Date = 04/09/16 Pct Recovery = 70% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PIPERONYL BUTOXIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 23 170% 391% 52% 23%
>= Reporting Level 23 59% 48% 40% 25%
Total 46 114% 281% 46% 25%

Sample Statistics
PIPERONYL BUTOXIDE

Characteristic N % % Basis
Plotted 46 81% Spiked
Estimated Values 39 68% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 9 16% Spiked
Spiked 57 .  
False Negatives 2 4% 2 out of 57
Not Spiked 29 .  
False Positives 0 0% 0 out of 29