OBSP Determination:
FAMOTIDINE
METHOD: 2440 , TESTIDCODE: 68000LCM56

Analysis Date = 09/09/17 SpikeMix = Abs 071817Pharm: 80 µl & Abs 072517Pharm1: 80 µl Pct Recovery = 69% Analysis Date = 11/09/17 SpikeMix = ERA 06281704: 50 µl & ERA 06281702: 50 µl Pct Recovery = 14% Analysis Date = 10/21/17 SpikeMix = ERA 06281702: 50 µl & ERA 06281703: 50 µl Pct Recovery = 56% Analysis Date = 08/28/17 SpikeMix = Abs 072517Pharm1: 50 µl & Abs 072517Pharm2: 50 µl Pct Recovery = 34% Analysis Date = 08/26/17 SpikeMix = Abs 072517Pharm1: 50 µl & Abs 071817Pharm: 50 µl Pct Recovery = 68% Analysis Date = 11/09/17 SpikeMix = ERA 06281702: 20 µl & Abs 072517Pharm2: 20 µl Pct Recovery = 12% Analysis Date = 11/08/17 SpikeMix = ERA 06281704: 20 µl & Abs 072517Pharm1: 20 µl Pct Recovery = 26% Analysis Date = 09/23/17 SpikeMix = Abs 072517Pharm1: 20 µl & Abs 072517Pharm2: 20 µl Pct Recovery = 65% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 23% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 19% Analysis Date = 08/10/17 SpikeMix = Crescent EN160610015: 80 µl & ERA 04281603: 80 µl Pct Recovery = 82% Analysis Date = 07/14/17 SpikeMix = Crescent EN160610015: 80 µl & ERA 04281603: 80 µl Pct Recovery = 71% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 39% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 39% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 45% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 45% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 6% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 5% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 12% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 15% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 17% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 15% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 10% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 8% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 17% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 19% Analysis Date = 06/18/17 SpikeMix = Crescent EN160610015: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 34% Analysis Date = 06/07/17 SpikeMix = Crescent EN160610015: 40 µl & ERA 04281604: 40 µl Pct Recovery = 102% Analysis Date = 04/07/17 SpikeMix = ERA 04281603: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 56% Analysis Date = 04/07/17 SpikeMix = ERA 04281603: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 64% Analysis Date = 03/14/17 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 44% Analysis Date = 03/14/17 SpikeMix = Crescent EN160610015: 40 µl & ERA 04281604: 40 µl Pct Recovery = 57% Analysis Date = 03/14/17 SpikeMix = Crescent EN160610015: 40 µl & ERA 04281604: 40 µl Pct Recovery = 56% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 59% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 65% Analysis Date = 11/09/17 Pct Recovery = 39% Analysis Date = 11/06/17 Pct Recovery = 40% Analysis Date = 11/06/17 Pct Recovery = 40% Analysis Date = 11/04/17 Pct Recovery = 40% Analysis Date = 11/04/17 Pct Recovery = 40% Analysis Date = 11/01/17 Pct Recovery = 41% Analysis Date = 11/01/17 Pct Recovery = 41% Analysis Date = 10/30/17 Pct Recovery = 41% Analysis Date = 10/30/17 Pct Recovery = 41% Analysis Date = 10/28/17 Pct Recovery = 41% Analysis Date = 10/28/17 Pct Recovery = 41% Analysis Date = 10/25/17 Pct Recovery = 42% Analysis Date = 10/25/17 Pct Recovery = 42% Analysis Date = 10/23/17 Pct Recovery = 42% Analysis Date = 10/23/17 Pct Recovery = 42% Analysis Date = 10/21/17 Pct Recovery = 42% Analysis Date = 10/21/17 Pct Recovery = 42% Analysis Date = 10/18/17 Pct Recovery = 43% Analysis Date = 10/18/17 Pct Recovery = 43% Analysis Date = 10/16/17 Pct Recovery = 43% Analysis Date = 10/16/17 Pct Recovery = 43% Analysis Date = 10/13/17 Pct Recovery = 44% Analysis Date = 10/13/17 Pct Recovery = 44% Analysis Date = 10/11/17 Pct Recovery = 44% Analysis Date = 10/11/17 Pct Recovery = 44% Analysis Date = 10/09/17 Pct Recovery = 44% Analysis Date = 10/09/17 Pct Recovery = 44% Analysis Date = 10/06/17 Pct Recovery = 45% Analysis Date = 10/06/17 Pct Recovery = 45% Analysis Date = 10/04/17 Pct Recovery = 45% Analysis Date = 10/04/17 Pct Recovery = 45% Analysis Date = 10/02/17 Pct Recovery = 45% Analysis Date = 10/02/17 Pct Recovery = 45% Analysis Date = 09/29/17 Pct Recovery = 46% Analysis Date = 09/29/17 Pct Recovery = 46% Analysis Date = 09/27/17 Pct Recovery = 46% Analysis Date = 09/27/17 Pct Recovery = 46% Analysis Date = 09/24/17 Pct Recovery = 47% Analysis Date = 09/24/17 Pct Recovery = 47% Analysis Date = 09/22/17 Pct Recovery = 47% Analysis Date = 09/22/17 Pct Recovery = 47% Analysis Date = 09/20/17 Pct Recovery = 47% Analysis Date = 09/20/17 Pct Recovery = 47% Analysis Date = 09/17/17 Pct Recovery = 48% Analysis Date = 09/17/17 Pct Recovery = 48% Analysis Date = 09/15/17 Pct Recovery = 48% Analysis Date = 09/15/17 Pct Recovery = 48% Analysis Date = 09/13/17 Pct Recovery = 48% Analysis Date = 09/13/17 Pct Recovery = 48% Analysis Date = 09/10/17 Pct Recovery = 48% Analysis Date = 09/10/17 Pct Recovery = 48% Analysis Date = 09/08/17 Pct Recovery = 49% Analysis Date = 09/08/17 Pct Recovery = 49% Analysis Date = 09/05/17 Pct Recovery = 49% Analysis Date = 09/05/17 Pct Recovery = 49% Analysis Date = 09/03/17 Pct Recovery = 49% Analysis Date = 09/03/17 Pct Recovery = 49% Analysis Date = 09/01/17 Pct Recovery = 50% Analysis Date = 09/01/17 Pct Recovery = 50% Analysis Date = 08/29/17 Pct Recovery = 50% Analysis Date = 08/29/17 Pct Recovery = 50% Analysis Date = 08/27/17 Pct Recovery = 50% Analysis Date = 08/27/17 Pct Recovery = 50% Analysis Date = 08/25/17 Pct Recovery = 51% Analysis Date = 08/25/17 Pct Recovery = 51% Analysis Date = 08/22/17 Pct Recovery = 51% Analysis Date = 08/22/17 Pct Recovery = 51% Analysis Date = 08/20/17 Pct Recovery = 51% Analysis Date = 08/20/17 Pct Recovery = 51% Analysis Date = 08/17/17 Pct Recovery = 52% Analysis Date = 08/17/17 Pct Recovery = 52% Analysis Date = 08/15/17 Pct Recovery = 52% Analysis Date = 08/15/17 Pct Recovery = 52% Analysis Date = 08/13/17 Pct Recovery = 52% Analysis Date = 08/13/17 Pct Recovery = 52% Analysis Date = 08/10/17 Pct Recovery = 53% Analysis Date = 08/10/17 Pct Recovery = 53% Analysis Date = 08/08/17 Pct Recovery = 53% Analysis Date = 08/08/17 Pct Recovery = 53% Analysis Date = 08/06/17 Pct Recovery = 53% Analysis Date = 08/06/17 Pct Recovery = 53% Analysis Date = 08/03/17 Pct Recovery = 53% Analysis Date = 08/03/17 Pct Recovery = 53% Analysis Date = 08/01/17 Pct Recovery = 53% Analysis Date = 08/01/17 Pct Recovery = 53% Analysis Date = 07/29/17 Pct Recovery = 53% Analysis Date = 07/29/17 Pct Recovery = 53% Analysis Date = 07/27/17 Pct Recovery = 53% Analysis Date = 07/27/17 Pct Recovery = 53% Analysis Date = 07/25/17 Pct Recovery = 54% Analysis Date = 07/25/17 Pct Recovery = 54% Analysis Date = 07/22/17 Pct Recovery = 54% Analysis Date = 07/22/17 Pct Recovery = 54% Analysis Date = 07/20/17 Pct Recovery = 54% Analysis Date = 07/20/17 Pct Recovery = 54% Analysis Date = 07/18/17 Pct Recovery = 54% Analysis Date = 07/18/17 Pct Recovery = 54% Analysis Date = 07/15/17 Pct Recovery = 54% Analysis Date = 07/15/17 Pct Recovery = 54% Analysis Date = 07/13/17 Pct Recovery = 54% Analysis Date = 07/13/17 Pct Recovery = 54% Analysis Date = 07/10/17 Pct Recovery = 54% Analysis Date = 07/10/17 Pct Recovery = 54% Analysis Date = 07/08/17 Pct Recovery = 54% Analysis Date = 07/08/17 Pct Recovery = 54% Analysis Date = 07/06/17 Pct Recovery = 54% Analysis Date = 07/06/17 Pct Recovery = 54% Analysis Date = 07/03/17 Pct Recovery = 55% Analysis Date = 07/03/17 Pct Recovery = 55% Analysis Date = 07/01/17 Pct Recovery = 55% Analysis Date = 07/01/17 Pct Recovery = 55% Analysis Date = 06/29/17 Pct Recovery = 55% Analysis Date = 06/29/17 Pct Recovery = 55% Analysis Date = 06/26/17 Pct Recovery = 55% Analysis Date = 06/26/17 Pct Recovery = 55% Analysis Date = 06/24/17 Pct Recovery = 55% Analysis Date = 06/24/17 Pct Recovery = 55% Analysis Date = 06/21/17 Pct Recovery = 55% Analysis Date = 06/21/17 Pct Recovery = 55% Analysis Date = 06/19/17 Pct Recovery = 55% Analysis Date = 06/19/17 Pct Recovery = 55% Analysis Date = 06/17/17 Pct Recovery = 55% Analysis Date = 06/17/17 Pct Recovery = 55% Analysis Date = 06/14/17 Pct Recovery = 56% Analysis Date = 06/14/17 Pct Recovery = 56% Analysis Date = 06/12/17 Pct Recovery = 56% Analysis Date = 06/12/17 Pct Recovery = 56% Analysis Date = 06/10/17 Pct Recovery = 56% Analysis Date = 06/10/17 Pct Recovery = 56% Analysis Date = 06/07/17 Pct Recovery = 56% Analysis Date = 06/07/17 Pct Recovery = 56% Analysis Date = 06/05/17 Pct Recovery = 56% Analysis Date = 06/05/17 Pct Recovery = 56% Analysis Date = 06/02/17 Pct Recovery = 56% Analysis Date = 06/02/17 Pct Recovery = 56% Analysis Date = 05/31/17 Pct Recovery = 56% Analysis Date = 05/31/17 Pct Recovery = 56% Analysis Date = 05/29/17 Pct Recovery = 56% Analysis Date = 05/29/17 Pct Recovery = 56% Analysis Date = 05/26/17 Pct Recovery = 56% Analysis Date = 05/26/17 Pct Recovery = 56% Analysis Date = 05/24/17 Pct Recovery = 57% Analysis Date = 05/24/17 Pct Recovery = 57% Analysis Date = 05/22/17 Pct Recovery = 57% Analysis Date = 05/22/17 Pct Recovery = 57% Analysis Date = 05/19/17 Pct Recovery = 57% Analysis Date = 05/19/17 Pct Recovery = 57% Analysis Date = 05/17/17 Pct Recovery = 57% Analysis Date = 05/17/17 Pct Recovery = 57% Analysis Date = 05/14/17 Pct Recovery = 57% Analysis Date = 05/14/17 Pct Recovery = 57% Analysis Date = 05/12/17 Pct Recovery = 57% Analysis Date = 05/12/17 Pct Recovery = 57% Analysis Date = 05/10/17 Pct Recovery = 57% Analysis Date = 05/10/17 Pct Recovery = 57% Analysis Date = 05/07/17 Pct Recovery = 57% Analysis Date = 05/07/17 Pct Recovery = 57% Analysis Date = 05/05/17 Pct Recovery = 57% Analysis Date = 05/05/17 Pct Recovery = 57% Analysis Date = 05/03/17 Pct Recovery = 58% Analysis Date = 05/03/17 Pct Recovery = 58% Analysis Date = 04/30/17 Pct Recovery = 58% Analysis Date = 04/30/17 Pct Recovery = 58% Analysis Date = 04/28/17 Pct Recovery = 58% Analysis Date = 04/28/17 Pct Recovery = 58% Analysis Date = 04/25/17 Pct Recovery = 58% Analysis Date = 04/25/17 Pct Recovery = 58% Analysis Date = 04/23/17 Pct Recovery = 58% Analysis Date = 04/23/17 Pct Recovery = 58% Analysis Date = 04/21/17 Pct Recovery = 58% Analysis Date = 04/21/17 Pct Recovery = 58% Analysis Date = 04/18/17 Pct Recovery = 58% Analysis Date = 04/18/17 Pct Recovery = 58% Analysis Date = 04/16/17 Pct Recovery = 58% Analysis Date = 04/16/17 Pct Recovery = 58% Analysis Date = 04/14/17 Pct Recovery = 58% Analysis Date = 04/14/17 Pct Recovery = 58% Analysis Date = 04/11/17 Pct Recovery = 59% Analysis Date = 04/11/17 Pct Recovery = 59% Analysis Date = 04/09/17 Pct Recovery = 59% Analysis Date = 04/09/17 Pct Recovery = 59% Analysis Date = 04/06/17 Pct Recovery = 59% Analysis Date = 04/06/17 Pct Recovery = 59% Analysis Date = 04/04/17 Pct Recovery = 59% Analysis Date = 04/04/17 Pct Recovery = 59% Analysis Date = 04/02/17 Pct Recovery = 58% Analysis Date = 04/02/17 Pct Recovery = 58% Analysis Date = 03/30/17 Pct Recovery = 58% Analysis Date = 03/30/17 Pct Recovery = 58% Analysis Date = 03/28/17 Pct Recovery = 58% Analysis Date = 03/28/17 Pct Recovery = 58% Analysis Date = 03/26/17 Pct Recovery = 58% Analysis Date = 03/26/17 Pct Recovery = 58% Analysis Date = 03/23/17 Pct Recovery = 58% Analysis Date = 03/23/17 Pct Recovery = 58% Analysis Date = 03/21/17 Pct Recovery = 58% Analysis Date = 03/21/17 Pct Recovery = 58% Analysis Date = 03/18/17 Pct Recovery = 58% Analysis Date = 03/18/17 Pct Recovery = 58% Analysis Date = 03/16/17 Pct Recovery = 57% Analysis Date = 03/16/17 Pct Recovery = 57% Analysis Date = 03/14/17 Pct Recovery = 57% Analysis Date = 03/14/17 Pct Recovery = 57% Analysis Date = 03/11/17 Pct Recovery = 57% Analysis Date = 03/11/17 Pct Recovery = 57% Analysis Date = 03/09/17 Pct Recovery = 57% Analysis Date = 03/09/17 Pct Recovery = 57% Analysis Date = 03/07/17 Pct Recovery = 56% Analysis Date = 03/07/17 Pct Recovery = 56% Analysis Date = 03/04/17 Pct Recovery = 56% Analysis Date = 03/04/17 Pct Recovery = 56% Analysis Date = 03/02/17 Pct Recovery = 56% Analysis Date = 03/02/17 Pct Recovery = 56% Analysis Date = 02/27/17 Pct Recovery = 55% Analysis Date = 02/27/17 Pct Recovery = 55% Analysis Date = 02/25/17 Pct Recovery = 55% Analysis Date = 02/25/17 Pct Recovery = 55% Analysis Date = 02/23/17 Pct Recovery = 55% Analysis Date = 02/23/17 Pct Recovery = 55% Analysis Date = 02/20/17 Pct Recovery = 54% Analysis Date = 02/20/17 Pct Recovery = 54% Analysis Date = 02/18/17 Pct Recovery = 54% Analysis Date = 02/18/17 Pct Recovery = 54% Analysis Date = 02/16/17 Pct Recovery = 54% Analysis Date = 02/16/17 Pct Recovery = 54% Analysis Date = 02/13/17 Pct Recovery = 53% Analysis Date = 02/13/17 Pct Recovery = 53% Analysis Date = 02/11/17 Pct Recovery = 53% Analysis Date = 02/11/17 Pct Recovery = 53% Analysis Date = 02/08/17 Pct Recovery = 53% Analysis Date = 02/08/17 Pct Recovery = 53% Analysis Date = 02/06/17 Pct Recovery = 52% Analysis Date = 02/06/17 Pct Recovery = 52% Analysis Date = 02/04/17 Pct Recovery = 52% Analysis Date = 02/04/17 Pct Recovery = 52% Analysis Date = 02/01/17 Pct Recovery = 52% Analysis Date = 02/01/17 Pct Recovery = 52% Analysis Date = 01/30/17 Pct Recovery = 51% Analysis Date = 01/30/17 Pct Recovery = 51% Analysis Date = 01/28/17 Pct Recovery = 51% Analysis Date = 01/28/17 Pct Recovery = 51% Analysis Date = 01/25/17 Pct Recovery = 51% Analysis Date = 01/25/17 Pct Recovery = 51% Analysis Date = 01/23/17 Pct Recovery = 50% Analysis Date = 01/23/17 Pct Recovery = 50% Analysis Date = 01/20/17 Pct Recovery = 50% Analysis Date = 01/20/17 Pct Recovery = 50% Analysis Date = 01/18/17 Pct Recovery = 50% Analysis Date = 01/18/17 Pct Recovery = 50% Analysis Date = 01/16/17 Pct Recovery = 49% Analysis Date = 01/16/17 Pct Recovery = 49% Analysis Date = 01/13/17 Pct Recovery = 49% Analysis Date = 01/13/17 Pct Recovery = 49% Analysis Date = 01/11/17 Pct Recovery = 49% Analysis Date = 01/11/17 Pct Recovery = 49% Analysis Date = 01/09/17 Pct Recovery = 48% Analysis Date = 01/09/17 Pct Recovery = 48% Analysis Date = 01/06/17 Pct Recovery = 48% Analysis Date = 01/06/17 Pct Recovery = 48% Analysis Date = 01/04/17 Pct Recovery = 48% Analysis Date = 01/04/17 Pct Recovery = 48% Analysis Date = 01/01/17 Pct Recovery = 47% Analysis Date = 01/01/17 Pct Recovery = 47% Analysis Date = 12/30/16 Pct Recovery = 47% Analysis Date = 12/30/16 Pct Recovery = 47% Analysis Date = 12/28/16 Pct Recovery = 47% Analysis Date = 12/28/16 Pct Recovery = 47% Analysis Date = 12/25/16 Pct Recovery = 46% Analysis Date = 12/25/16 Pct Recovery = 46% Analysis Date = 12/23/16 Pct Recovery = 46% Analysis Date = 12/23/16 Pct Recovery = 46% Analysis Date = 12/21/16 Pct Recovery = 46% Analysis Date = 12/21/16 Pct Recovery = 46% Analysis Date = 12/18/16 Pct Recovery = 45% Analysis Date = 12/18/16 Pct Recovery = 45% Analysis Date = 12/16/16 Pct Recovery = 45% Analysis Date = 12/16/16 Pct Recovery = 45% Analysis Date = 12/13/16 Pct Recovery = 44% Analysis Date = 12/13/16 Pct Recovery = 44% Analysis Date = 12/11/16 Pct Recovery = 44% Analysis Date = 12/11/16 Pct Recovery = 44% Analysis Date = 12/09/16 Pct Recovery = 43% Analysis Date = 12/09/16 Pct Recovery = 43% Analysis Date = 12/06/16 Pct Recovery = 43% Analysis Date = 12/06/16 Pct Recovery = 43% Analysis Date = 12/04/16 Pct Recovery = 42% Analysis Date = 12/04/16 Pct Recovery = 42% Analysis Date = 12/02/16 Pct Recovery = 42% Analysis Date = 12/02/16 Pct Recovery = 42% Analysis Date = 11/29/16 Pct Recovery = 41% Analysis Date = 11/29/16 Pct Recovery = 41% Analysis Date = 11/27/16 Pct Recovery = 41% Analysis Date = 11/27/16 Pct Recovery = 41% Analysis Date = 11/24/16 Pct Recovery = 41% Analysis Date = 11/24/16 Pct Recovery = 41% Analysis Date = 11/22/16 Pct Recovery = 40% Analysis Date = 11/22/16 Pct Recovery = 40% Analysis Date = 11/20/16 Pct Recovery = 40% Analysis Date = 11/20/16 Pct Recovery = 40% Analysis Date = 11/17/16 Pct Recovery = 39% Analysis Date = 11/17/16 Pct Recovery = 39% Analysis Date = 11/15/16 Pct Recovery = 39% Analysis Date = 11/15/16 Pct Recovery = 39% Analysis Date = 11/13/16 Pct Recovery = 38% Analysis Date = 11/13/16 Pct Recovery = 38% Analysis Date = 11/10/16 Pct Recovery = 38% Analysis Date = 11/10/16 Pct Recovery = 38% Analysis Date = 11/08/16 Pct Recovery = 37% Analysis Date = 11/08/16 Pct Recovery = 37% Analysis Date = 11/05/16 Pct Recovery = 37% Analysis Date = 11/05/16 Pct Recovery = 37% Analysis Date = 11/03/16 Pct Recovery = 36% Analysis Date = 11/03/16 Pct Recovery = 36% Analysis Date = 11/01/16 Pct Recovery = 35% Analysis Date = 11/01/16 Pct Recovery = 35% Analysis Date = 10/29/16 Pct Recovery = 35% Analysis Date = 10/29/16 Pct Recovery = 35% Analysis Date = 10/27/16 Pct Recovery = 34% Analysis Date = 10/27/16 Pct Recovery = 34% Analysis Date = 10/25/16 Pct Recovery = 33% Analysis Date = 10/25/16 Pct Recovery = 33% Analysis Date = 10/22/16 Pct Recovery = 33% Analysis Date = 10/22/16 Pct Recovery = 33% Analysis Date = 10/20/16 Pct Recovery = 32% Analysis Date = 10/20/16 Pct Recovery = 32% Analysis Date = 10/17/16 Pct Recovery = 31% Analysis Date = 10/17/16 Pct Recovery = 31% Analysis Date = 10/15/16 Pct Recovery = 30% Analysis Date = 10/15/16 Pct Recovery = 30% Analysis Date = 10/13/16 Pct Recovery = 30% Analysis Date = 10/13/16 Pct Recovery = 30% Analysis Date = 10/10/16 Pct Recovery = 29% Analysis Date = 10/10/16 Pct Recovery = 29% Analysis Date = 10/08/16 Pct Recovery = 28% Analysis Date = 10/08/16 Pct Recovery = 28% Analysis Date = 10/06/16 Pct Recovery = 27% Analysis Date = 10/06/16 Pct Recovery = 27% Analysis Date = 10/03/16 Pct Recovery = 27% Analysis Date = 10/03/16 Pct Recovery = 27% Analysis Date = 10/01/16 Pct Recovery = 26% Analysis Date = 10/01/16 Pct Recovery = 26% Analysis Date = 09/28/16 Pct Recovery = 25% Analysis Date = 09/28/16 Pct Recovery = 25% Analysis Date = 09/26/16 Pct Recovery = 24% Analysis Date = 09/26/16 Pct Recovery = 24% Analysis Date = 09/24/16 Pct Recovery = 24% Analysis Date = 09/24/16 Pct Recovery = 24% Analysis Date = 09/21/16 Pct Recovery = 23% Analysis Date = 09/21/16 Pct Recovery = 23% Analysis Date = 09/19/16 Pct Recovery = 22% Analysis Date = 09/19/16 Pct Recovery = 22% Analysis Date = 09/17/16 Pct Recovery = 22% Analysis Date = 09/17/16 Pct Recovery = 22% Analysis Date = 09/14/16 Pct Recovery = 21% Analysis Date = 09/14/16 Pct Recovery = 21% Analysis Date = 09/12/16 Pct Recovery = 21% Analysis Date = 09/12/16 Pct Recovery = 21% Analysis Date = 09/09/16 Pct Recovery = 20% Analysis Date = 09/09/16 Pct Recovery = 20% Analysis Date = 09/07/16 Pct Recovery = 19% Analysis Date = 09/07/16 Pct Recovery = 19% Analysis Date = 09/05/16 Pct Recovery = 19% Analysis Date = 09/05/16 Pct Recovery = 19% Analysis Date = 09/02/16 Pct Recovery = 18% Analysis Date = 09/02/16 Pct Recovery = 18% Analysis Date = 08/31/16 Pct Recovery = 17% Analysis Date = 08/31/16 Pct Recovery = 17% Analysis Date = 08/29/16 Pct Recovery = 17% Analysis Date = 08/29/16 Pct Recovery = 17% Analysis Date = 08/26/16 Pct Recovery = 16% Analysis Date = 08/26/16 Pct Recovery = 16% Analysis Date = 08/24/16 Pct Recovery = 16% Analysis Date = 08/24/16 Pct Recovery = 16% Analysis Date = 08/21/16 Pct Recovery = 15% Analysis Date = 08/21/16 Pct Recovery = 15% Analysis Date = 08/19/16 Pct Recovery = 14% Analysis Date = 08/19/16 Pct Recovery = 14% Analysis Date = 08/17/16 Pct Recovery = 14% Analysis Date = 08/17/16 Pct Recovery = 14% Analysis Date = 08/14/16 Pct Recovery = 13% Analysis Date = 08/14/16 Pct Recovery = 13% Analysis Date = 08/12/16 Pct Recovery = 13% Analysis Date = 08/12/16 Pct Recovery = 13% Analysis Date = 08/10/16 Pct Recovery = 12% Analysis Date = 08/10/16 Pct Recovery = 12% Analysis Date = 08/07/16 Pct Recovery = 11% Analysis Date = 08/07/16 Pct Recovery = 11% Analysis Date = 08/05/16 Pct Recovery = 11% Analysis Date = 08/05/16 Pct Recovery = 11% Analysis Date = 08/02/16 Pct Recovery = 10% Analysis Date = 08/02/16 Pct Recovery = 10% Analysis Date = 07/31/16 Pct Recovery = 10% Analysis Date = 07/31/16 Pct Recovery = 10% Analysis Date = 07/29/16 Pct Recovery = 9% Analysis Date = 07/29/16 Pct Recovery = 9% Analysis Date = 07/26/16 Pct Recovery = 8% Analysis Date = 07/26/16 Pct Recovery = 8% Analysis Date = 07/24/16 Pct Recovery = 8% Analysis Date = 07/24/16 Pct Recovery = 8% Analysis Date = 07/22/16 Pct Recovery = 7% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FAMOTIDINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 9 60% 18% 57% 6%
>= Reporting Level 26 32% 23% 21% 23%
Total 35 39% 25% 39% 33%

Sample Statistics
FAMOTIDINE

Characteristic N % % Basis
Plotted 35 63% Spiked
Estimated Values 35 63% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 12 21% Spiked
Spiked 56 .  
False Negatives 9 16% 9 out of 56
Not Spiked 30 .  
False Positives 0 0% 0 out of 30