OBSP Determination:
CHLORPHENIRAMINE
METHOD: 2440 , TESTIDCODE: 67497LCM56

Analysis Date = 09/09/17 SpikeMix = Abs 071817Pharm: 80 µl & Abs 072517Pharm1: 80 µl Pct Recovery = 71% Analysis Date = 11/09/17 SpikeMix = ERA 06281704: 50 µl & ERA 06281702: 50 µl Pct Recovery = 65% Analysis Date = 10/21/17 SpikeMix = ERA 06281702: 50 µl & ERA 06281703: 50 µl Pct Recovery = 55% Analysis Date = 09/21/17 SpikeMix = Abs 071817Pharm: 50 µl & Abs 072517Pharm1: 50 µl Pct Recovery = 51% Analysis Date = 08/28/17 SpikeMix = Abs 072517Pharm1: 50 µl & Abs 072517Pharm2: 50 µl Pct Recovery = 48% Analysis Date = 08/26/17 SpikeMix = Abs 072517Pharm1: 50 µl & Abs 071817Pharm: 50 µl Pct Recovery = 45% Analysis Date = 11/09/17 SpikeMix = ERA 06281702: 20 µl & Abs 072517Pharm2: 20 µl Pct Recovery = 55% Analysis Date = 11/08/17 SpikeMix = ERA 06281704: 20 µl & Abs 072517Pharm1: 20 µl Pct Recovery = 62% Analysis Date = 09/23/17 SpikeMix = Abs 072517Pharm1: 20 µl & Abs 072517Pharm2: 20 µl Pct Recovery = 71% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 50% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 52% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 26% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 46% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 32% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 39% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 40% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 53% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 42% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 41% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 40% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 33% Analysis Date = 02/07/17 SpikeMix = Abs 061416: 100 µl & ERA 04281603: 100 µl Pct Recovery = 59% Analysis Date = 02/07/17 SpikeMix = Abs 061416: 100 µl & ERA 04281603: 100 µl Pct Recovery = 61% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 38% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 33% Analysis Date = 08/10/17 SpikeMix = Crescent EN160610015: 80 µl & ERA 04281603: 80 µl Pct Recovery = 45% Analysis Date = 06/17/17 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 63% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 46% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 41% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 48% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 39% Analysis Date = 04/20/17 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 69% Analysis Date = 04/07/17 SpikeMix = ERA 04281603: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 86% Analysis Date = 04/06/17 SpikeMix = ERA 04281604: 40 µl & ERA 04281603: 40 µl Pct Recovery = 89% Analysis Date = 04/06/17 SpikeMix = ERA 04281603: 40 µl & ERA 04281604: 40 µl Pct Recovery = 91% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 31% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 27% Analysis Date = 08/11/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 84% Analysis Date = 07/15/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 76% Analysis Date = 06/18/17 SpikeMix = Crescent EN160610015: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 127% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 67% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 78% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 53% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 46% Analysis Date = 11/08/17 Pct Recovery = 58% Analysis Date = 11/06/17 Pct Recovery = 58% Analysis Date = 11/06/17 Pct Recovery = 58% Analysis Date = 11/04/17 Pct Recovery = 58% Analysis Date = 11/04/17 Pct Recovery = 58% Analysis Date = 11/01/17 Pct Recovery = 59% Analysis Date = 11/01/17 Pct Recovery = 59% Analysis Date = 10/30/17 Pct Recovery = 59% Analysis Date = 10/30/17 Pct Recovery = 59% Analysis Date = 10/28/17 Pct Recovery = 59% Analysis Date = 10/28/17 Pct Recovery = 59% Analysis Date = 10/25/17 Pct Recovery = 59% Analysis Date = 10/25/17 Pct Recovery = 59% Analysis Date = 10/23/17 Pct Recovery = 60% Analysis Date = 10/23/17 Pct Recovery = 60% Analysis Date = 10/21/17 Pct Recovery = 60% Analysis Date = 10/21/17 Pct Recovery = 60% Analysis Date = 10/18/17 Pct Recovery = 60% Analysis Date = 10/18/17 Pct Recovery = 60% Analysis Date = 10/16/17 Pct Recovery = 60% Analysis Date = 10/16/17 Pct Recovery = 60% Analysis Date = 10/13/17 Pct Recovery = 61% Analysis Date = 10/13/17 Pct Recovery = 61% Analysis Date = 10/11/17 Pct Recovery = 61% Analysis Date = 10/11/17 Pct Recovery = 61% Analysis Date = 10/09/17 Pct Recovery = 61% Analysis Date = 10/09/17 Pct Recovery = 61% Analysis Date = 10/06/17 Pct Recovery = 61% Analysis Date = 10/06/17 Pct Recovery = 61% Analysis Date = 10/04/17 Pct Recovery = 62% Analysis Date = 10/04/17 Pct Recovery = 62% Analysis Date = 10/02/17 Pct Recovery = 62% Analysis Date = 10/02/17 Pct Recovery = 62% Analysis Date = 09/29/17 Pct Recovery = 62% Analysis Date = 09/29/17 Pct Recovery = 62% Analysis Date = 09/27/17 Pct Recovery = 62% Analysis Date = 09/27/17 Pct Recovery = 62% Analysis Date = 09/24/17 Pct Recovery = 63% Analysis Date = 09/24/17 Pct Recovery = 63% Analysis Date = 09/22/17 Pct Recovery = 63% Analysis Date = 09/22/17 Pct Recovery = 63% Analysis Date = 09/20/17 Pct Recovery = 63% Analysis Date = 09/20/17 Pct Recovery = 63% Analysis Date = 09/17/17 Pct Recovery = 63% Analysis Date = 09/17/17 Pct Recovery = 63% Analysis Date = 09/15/17 Pct Recovery = 64% Analysis Date = 09/15/17 Pct Recovery = 64% Analysis Date = 09/13/17 Pct Recovery = 64% Analysis Date = 09/13/17 Pct Recovery = 64% Analysis Date = 09/10/17 Pct Recovery = 64% Analysis Date = 09/10/17 Pct Recovery = 64% Analysis Date = 09/08/17 Pct Recovery = 64% Analysis Date = 09/08/17 Pct Recovery = 64% Analysis Date = 09/06/17 Pct Recovery = 64% Analysis Date = 09/06/17 Pct Recovery = 64% Analysis Date = 09/03/17 Pct Recovery = 65% Analysis Date = 09/03/17 Pct Recovery = 65% Analysis Date = 09/01/17 Pct Recovery = 65% Analysis Date = 09/01/17 Pct Recovery = 65% Analysis Date = 08/29/17 Pct Recovery = 65% Analysis Date = 08/29/17 Pct Recovery = 65% Analysis Date = 08/27/17 Pct Recovery = 65% Analysis Date = 08/27/17 Pct Recovery = 65% Analysis Date = 08/25/17 Pct Recovery = 65% Analysis Date = 08/25/17 Pct Recovery = 65% Analysis Date = 08/22/17 Pct Recovery = 66% Analysis Date = 08/22/17 Pct Recovery = 66% Analysis Date = 08/20/17 Pct Recovery = 66% Analysis Date = 08/20/17 Pct Recovery = 66% Analysis Date = 08/18/17 Pct Recovery = 66% Analysis Date = 08/18/17 Pct Recovery = 66% Analysis Date = 08/15/17 Pct Recovery = 66% Analysis Date = 08/15/17 Pct Recovery = 66% Analysis Date = 08/13/17 Pct Recovery = 66% Analysis Date = 08/13/17 Pct Recovery = 66% Analysis Date = 08/10/17 Pct Recovery = 67% Analysis Date = 08/10/17 Pct Recovery = 67% Analysis Date = 08/08/17 Pct Recovery = 67% Analysis Date = 08/08/17 Pct Recovery = 67% Analysis Date = 08/06/17 Pct Recovery = 67% Analysis Date = 08/06/17 Pct Recovery = 67% Analysis Date = 08/03/17 Pct Recovery = 67% Analysis Date = 08/03/17 Pct Recovery = 67% Analysis Date = 08/01/17 Pct Recovery = 67% Analysis Date = 08/01/17 Pct Recovery = 67% Analysis Date = 07/30/17 Pct Recovery = 67% Analysis Date = 07/30/17 Pct Recovery = 67% Analysis Date = 07/27/17 Pct Recovery = 68% Analysis Date = 07/27/17 Pct Recovery = 68% Analysis Date = 07/25/17 Pct Recovery = 68% Analysis Date = 07/25/17 Pct Recovery = 68% Analysis Date = 07/22/17 Pct Recovery = 68% Analysis Date = 07/22/17 Pct Recovery = 68% Analysis Date = 07/20/17 Pct Recovery = 68% Analysis Date = 07/20/17 Pct Recovery = 68% Analysis Date = 07/18/17 Pct Recovery = 68% Analysis Date = 07/18/17 Pct Recovery = 68% Analysis Date = 07/15/17 Pct Recovery = 69% Analysis Date = 07/15/17 Pct Recovery = 69% Analysis Date = 07/13/17 Pct Recovery = 69% Analysis Date = 07/13/17 Pct Recovery = 69% Analysis Date = 07/11/17 Pct Recovery = 69% Analysis Date = 07/11/17 Pct Recovery = 69% Analysis Date = 07/08/17 Pct Recovery = 69% Analysis Date = 07/08/17 Pct Recovery = 69% Analysis Date = 07/06/17 Pct Recovery = 69% Analysis Date = 07/06/17 Pct Recovery = 69% Analysis Date = 07/04/17 Pct Recovery = 69% Analysis Date = 07/04/17 Pct Recovery = 69% Analysis Date = 07/01/17 Pct Recovery = 69% Analysis Date = 07/01/17 Pct Recovery = 69% Analysis Date = 06/29/17 Pct Recovery = 70% Analysis Date = 06/29/17 Pct Recovery = 70% Analysis Date = 06/26/17 Pct Recovery = 70% Analysis Date = 06/26/17 Pct Recovery = 70% Analysis Date = 06/24/17 Pct Recovery = 70% Analysis Date = 06/24/17 Pct Recovery = 70% Analysis Date = 06/22/17 Pct Recovery = 70% Analysis Date = 06/22/17 Pct Recovery = 70% Analysis Date = 06/19/17 Pct Recovery = 70% Analysis Date = 06/19/17 Pct Recovery = 70% Analysis Date = 06/17/17 Pct Recovery = 70% Analysis Date = 06/17/17 Pct Recovery = 70% Analysis Date = 06/15/17 Pct Recovery = 70% Analysis Date = 06/15/17 Pct Recovery = 70% Analysis Date = 06/12/17 Pct Recovery = 71% Analysis Date = 06/12/17 Pct Recovery = 71% Analysis Date = 06/10/17 Pct Recovery = 71% Analysis Date = 06/10/17 Pct Recovery = 71% Analysis Date = 06/07/17 Pct Recovery = 71% Analysis Date = 06/07/17 Pct Recovery = 71% Analysis Date = 06/05/17 Pct Recovery = 71% Analysis Date = 06/05/17 Pct Recovery = 71% Analysis Date = 06/03/17 Pct Recovery = 71% Analysis Date = 06/03/17 Pct Recovery = 71% Analysis Date = 05/31/17 Pct Recovery = 71% Analysis Date = 05/31/17 Pct Recovery = 71% Analysis Date = 05/29/17 Pct Recovery = 71% Analysis Date = 05/29/17 Pct Recovery = 71% Analysis Date = 05/27/17 Pct Recovery = 72% Analysis Date = 05/27/17 Pct Recovery = 72% Analysis Date = 05/24/17 Pct Recovery = 72% Analysis Date = 05/24/17 Pct Recovery = 72% Analysis Date = 05/22/17 Pct Recovery = 72% Analysis Date = 05/22/17 Pct Recovery = 72% Analysis Date = 05/19/17 Pct Recovery = 72% Analysis Date = 05/19/17 Pct Recovery = 72% Analysis Date = 05/17/17 Pct Recovery = 72% Analysis Date = 05/17/17 Pct Recovery = 72% Analysis Date = 05/15/17 Pct Recovery = 72% Analysis Date = 05/15/17 Pct Recovery = 72% Analysis Date = 05/12/17 Pct Recovery = 72% Analysis Date = 05/12/17 Pct Recovery = 72% Analysis Date = 05/10/17 Pct Recovery = 72% Analysis Date = 05/10/17 Pct Recovery = 72% Analysis Date = 05/08/17 Pct Recovery = 73% Analysis Date = 05/08/17 Pct Recovery = 73% Analysis Date = 05/05/17 Pct Recovery = 73% Analysis Date = 05/05/17 Pct Recovery = 73% Analysis Date = 05/03/17 Pct Recovery = 73% Analysis Date = 05/03/17 Pct Recovery = 73% Analysis Date = 05/01/17 Pct Recovery = 73% Analysis Date = 05/01/17 Pct Recovery = 73% Analysis Date = 04/28/17 Pct Recovery = 73% Analysis Date = 04/28/17 Pct Recovery = 73% Analysis Date = 04/26/17 Pct Recovery = 73% Analysis Date = 04/26/17 Pct Recovery = 73% Analysis Date = 04/23/17 Pct Recovery = 73% Analysis Date = 04/23/17 Pct Recovery = 73% Analysis Date = 04/21/17 Pct Recovery = 74% Analysis Date = 04/21/17 Pct Recovery = 74% Analysis Date = 04/19/17 Pct Recovery = 74% Analysis Date = 04/19/17 Pct Recovery = 74% Analysis Date = 04/16/17 Pct Recovery = 74% Analysis Date = 04/16/17 Pct Recovery = 74% Analysis Date = 04/14/17 Pct Recovery = 74% Analysis Date = 04/14/17 Pct Recovery = 74% Analysis Date = 04/12/17 Pct Recovery = 74% Analysis Date = 04/12/17 Pct Recovery = 74% Analysis Date = 04/09/17 Pct Recovery = 74% Analysis Date = 04/09/17 Pct Recovery = 74% Analysis Date = 04/07/17 Pct Recovery = 74% Analysis Date = 04/07/17 Pct Recovery = 74% Analysis Date = 04/04/17 Pct Recovery = 74% Analysis Date = 04/04/17 Pct Recovery = 74% Analysis Date = 04/02/17 Pct Recovery = 74% Analysis Date = 04/02/17 Pct Recovery = 74% Analysis Date = 03/31/17 Pct Recovery = 73% Analysis Date = 03/31/17 Pct Recovery = 73% Analysis Date = 03/28/17 Pct Recovery = 73% Analysis Date = 03/28/17 Pct Recovery = 73% Analysis Date = 03/26/17 Pct Recovery = 73% Analysis Date = 03/26/17 Pct Recovery = 73% Analysis Date = 03/24/17 Pct Recovery = 72% Analysis Date = 03/24/17 Pct Recovery = 72% Analysis Date = 03/21/17 Pct Recovery = 72% Analysis Date = 03/21/17 Pct Recovery = 72% Analysis Date = 03/19/17 Pct Recovery = 71% Analysis Date = 03/19/17 Pct Recovery = 71% Analysis Date = 03/16/17 Pct Recovery = 71% Analysis Date = 03/16/17 Pct Recovery = 71% Analysis Date = 03/14/17 Pct Recovery = 70% Analysis Date = 03/14/17 Pct Recovery = 70% Analysis Date = 03/12/17 Pct Recovery = 70% Analysis Date = 03/12/17 Pct Recovery = 70% Analysis Date = 03/09/17 Pct Recovery = 69% Analysis Date = 03/09/17 Pct Recovery = 69% Analysis Date = 03/07/17 Pct Recovery = 69% Analysis Date = 03/07/17 Pct Recovery = 69% Analysis Date = 03/05/17 Pct Recovery = 69% Analysis Date = 03/05/17 Pct Recovery = 69% Analysis Date = 03/02/17 Pct Recovery = 68% Analysis Date = 03/02/17 Pct Recovery = 68% Analysis Date = 02/28/17 Pct Recovery = 68% Analysis Date = 02/28/17 Pct Recovery = 68% Analysis Date = 02/26/17 Pct Recovery = 67% Analysis Date = 02/26/17 Pct Recovery = 67% Analysis Date = 02/23/17 Pct Recovery = 67% Analysis Date = 02/23/17 Pct Recovery = 67% Analysis Date = 02/21/17 Pct Recovery = 66% Analysis Date = 02/21/17 Pct Recovery = 66% Analysis Date = 02/18/17 Pct Recovery = 66% Analysis Date = 02/18/17 Pct Recovery = 66% Analysis Date = 02/16/17 Pct Recovery = 65% Analysis Date = 02/16/17 Pct Recovery = 65% Analysis Date = 02/14/17 Pct Recovery = 65% Analysis Date = 02/14/17 Pct Recovery = 65% Analysis Date = 02/11/17 Pct Recovery = 65% Analysis Date = 02/11/17 Pct Recovery = 65% Analysis Date = 02/09/17 Pct Recovery = 64% Analysis Date = 02/09/17 Pct Recovery = 64% Analysis Date = 02/07/17 Pct Recovery = 64% Analysis Date = 02/07/17 Pct Recovery = 64% Analysis Date = 02/04/17 Pct Recovery = 63% Analysis Date = 02/04/17 Pct Recovery = 63% Analysis Date = 02/02/17 Pct Recovery = 62% Analysis Date = 02/02/17 Pct Recovery = 62% Analysis Date = 01/30/17 Pct Recovery = 62% Analysis Date = 01/30/17 Pct Recovery = 62% Analysis Date = 01/28/17 Pct Recovery = 61% Analysis Date = 01/28/17 Pct Recovery = 61% Analysis Date = 01/26/17 Pct Recovery = 61% Analysis Date = 01/26/17 Pct Recovery = 61% Analysis Date = 01/23/17 Pct Recovery = 60% Analysis Date = 01/23/17 Pct Recovery = 60% Analysis Date = 01/21/17 Pct Recovery = 59% Analysis Date = 01/21/17 Pct Recovery = 59% Analysis Date = 01/19/17 Pct Recovery = 59% Analysis Date = 01/19/17 Pct Recovery = 59% Analysis Date = 01/16/17 Pct Recovery = 58% Analysis Date = 01/16/17 Pct Recovery = 58% Analysis Date = 01/14/17 Pct Recovery = 58% Analysis Date = 01/14/17 Pct Recovery = 58% Analysis Date = 01/12/17 Pct Recovery = 57% Analysis Date = 01/12/17 Pct Recovery = 57% Analysis Date = 01/09/17 Pct Recovery = 56% Analysis Date = 01/09/17 Pct Recovery = 56% Analysis Date = 01/07/17 Pct Recovery = 56% Analysis Date = 01/07/17 Pct Recovery = 56% Analysis Date = 01/04/17 Pct Recovery = 55% Analysis Date = 01/04/17 Pct Recovery = 55% Analysis Date = 01/02/17 Pct Recovery = 55% Analysis Date = 01/02/17 Pct Recovery = 55% Analysis Date = 12/31/16 Pct Recovery = 54% Analysis Date = 12/31/16 Pct Recovery = 54% Analysis Date = 12/28/16 Pct Recovery = 54% Analysis Date = 12/28/16 Pct Recovery = 54% Analysis Date = 12/26/16 Pct Recovery = 53% Analysis Date = 12/26/16 Pct Recovery = 53% Analysis Date = 12/24/16 Pct Recovery = 53% Analysis Date = 12/24/16 Pct Recovery = 53% Analysis Date = 12/21/16 Pct Recovery = 53% Analysis Date = 12/21/16 Pct Recovery = 53% Analysis Date = 12/19/16 Pct Recovery = 52% Analysis Date = 12/19/16 Pct Recovery = 52% Analysis Date = 12/16/16 Pct Recovery = 52% Analysis Date = 12/16/16 Pct Recovery = 52% Analysis Date = 12/14/16 Pct Recovery = 51% Analysis Date = 12/14/16 Pct Recovery = 51% Analysis Date = 12/12/16 Pct Recovery = 51% Analysis Date = 12/12/16 Pct Recovery = 51% Analysis Date = 12/09/16 Pct Recovery = 50% Analysis Date = 12/09/16 Pct Recovery = 50% Analysis Date = 12/07/16 Pct Recovery = 50% Analysis Date = 12/07/16 Pct Recovery = 50% Analysis Date = 12/05/16 Pct Recovery = 50% Analysis Date = 12/05/16 Pct Recovery = 50% Analysis Date = 12/02/16 Pct Recovery = 49% Analysis Date = 12/02/16 Pct Recovery = 49% Analysis Date = 11/30/16 Pct Recovery = 49% Analysis Date = 11/30/16 Pct Recovery = 49% Analysis Date = 11/27/16 Pct Recovery = 48% Analysis Date = 11/27/16 Pct Recovery = 48% Analysis Date = 11/25/16 Pct Recovery = 48% Analysis Date = 11/25/16 Pct Recovery = 48% Analysis Date = 11/23/16 Pct Recovery = 47% Analysis Date = 11/23/16 Pct Recovery = 47% Analysis Date = 11/20/16 Pct Recovery = 47% Analysis Date = 11/20/16 Pct Recovery = 47% Analysis Date = 11/18/16 Pct Recovery = 46% Analysis Date = 11/18/16 Pct Recovery = 46% Analysis Date = 11/16/16 Pct Recovery = 46% Analysis Date = 11/16/16 Pct Recovery = 46% Analysis Date = 11/13/16 Pct Recovery = 46% Analysis Date = 11/13/16 Pct Recovery = 46% Analysis Date = 11/11/16 Pct Recovery = 46% Analysis Date = 11/11/16 Pct Recovery = 46% Analysis Date = 11/09/16 Pct Recovery = 45% Analysis Date = 11/09/16 Pct Recovery = 45% Analysis Date = 11/06/16 Pct Recovery = 45% Analysis Date = 11/06/16 Pct Recovery = 45% Analysis Date = 11/04/16 Pct Recovery = 45% Analysis Date = 11/04/16 Pct Recovery = 45% Analysis Date = 11/01/16 Pct Recovery = 45% Analysis Date = 11/01/16 Pct Recovery = 45% Analysis Date = 10/30/16 Pct Recovery = 44% Analysis Date = 10/30/16 Pct Recovery = 44% Analysis Date = 10/28/16 Pct Recovery = 44% Analysis Date = 10/28/16 Pct Recovery = 44% Analysis Date = 10/25/16 Pct Recovery = 44% Analysis Date = 10/25/16 Pct Recovery = 44% Analysis Date = 10/23/16 Pct Recovery = 44% Analysis Date = 10/23/16 Pct Recovery = 44% Analysis Date = 10/21/16 Pct Recovery = 44% Analysis Date = 10/21/16 Pct Recovery = 44% Analysis Date = 10/18/16 Pct Recovery = 43% Analysis Date = 10/18/16 Pct Recovery = 43% Analysis Date = 10/16/16 Pct Recovery = 43% Analysis Date = 10/16/16 Pct Recovery = 43% Analysis Date = 10/13/16 Pct Recovery = 43% Analysis Date = 10/13/16 Pct Recovery = 43% Analysis Date = 10/11/16 Pct Recovery = 43% Analysis Date = 10/11/16 Pct Recovery = 43% Analysis Date = 10/09/16 Pct Recovery = 43% Analysis Date = 10/09/16 Pct Recovery = 43% Analysis Date = 10/06/16 Pct Recovery = 43% Analysis Date = 10/06/16 Pct Recovery = 43% Analysis Date = 10/04/16 Pct Recovery = 42% Analysis Date = 10/04/16 Pct Recovery = 42% Analysis Date = 10/02/16 Pct Recovery = 42% Analysis Date = 10/02/16 Pct Recovery = 42% Analysis Date = 09/29/16 Pct Recovery = 42% Analysis Date = 09/29/16 Pct Recovery = 42% Analysis Date = 09/27/16 Pct Recovery = 42% Analysis Date = 09/27/16 Pct Recovery = 42% Analysis Date = 09/24/16 Pct Recovery = 42% Analysis Date = 09/24/16 Pct Recovery = 42% Analysis Date = 09/22/16 Pct Recovery = 42% Analysis Date = 09/22/16 Pct Recovery = 42% Analysis Date = 09/20/16 Pct Recovery = 42% Analysis Date = 09/20/16 Pct Recovery = 42% Analysis Date = 09/17/16 Pct Recovery = 41% Analysis Date = 09/17/16 Pct Recovery = 41% Analysis Date = 09/15/16 Pct Recovery = 41% Analysis Date = 09/15/16 Pct Recovery = 41% Analysis Date = 09/13/16 Pct Recovery = 41% Analysis Date = 09/13/16 Pct Recovery = 41% Analysis Date = 09/10/16 Pct Recovery = 41% Analysis Date = 09/10/16 Pct Recovery = 41% Analysis Date = 09/08/16 Pct Recovery = 41% Analysis Date = 09/08/16 Pct Recovery = 41% Analysis Date = 09/06/16 Pct Recovery = 41% Analysis Date = 09/06/16 Pct Recovery = 41% Analysis Date = 09/03/16 Pct Recovery = 41% Analysis Date = 09/03/16 Pct Recovery = 41% Analysis Date = 09/01/16 Pct Recovery = 40% Analysis Date = 09/01/16 Pct Recovery = 40% Analysis Date = 08/29/16 Pct Recovery = 40% Analysis Date = 08/29/16 Pct Recovery = 40% Analysis Date = 08/27/16 Pct Recovery = 40% Analysis Date = 08/27/16 Pct Recovery = 40% Analysis Date = 08/25/16 Pct Recovery = 40% Analysis Date = 08/25/16 Pct Recovery = 40% Analysis Date = 08/22/16 Pct Recovery = 40% Analysis Date = 08/22/16 Pct Recovery = 40% Analysis Date = 08/20/16 Pct Recovery = 40% Analysis Date = 08/20/16 Pct Recovery = 40% Analysis Date = 08/18/16 Pct Recovery = 40% Analysis Date = 08/18/16 Pct Recovery = 40% Analysis Date = 08/15/16 Pct Recovery = 40% Analysis Date = 08/15/16 Pct Recovery = 40% Analysis Date = 08/13/16 Pct Recovery = 39% Analysis Date = 08/13/16 Pct Recovery = 39% Analysis Date = 08/10/16 Pct Recovery = 39% Analysis Date = 08/10/16 Pct Recovery = 39% Analysis Date = 08/08/16 Pct Recovery = 39% Analysis Date = 08/08/16 Pct Recovery = 39% Analysis Date = 08/06/16 Pct Recovery = 39% Analysis Date = 08/06/16 Pct Recovery = 39% Analysis Date = 08/03/16 Pct Recovery = 39% Analysis Date = 08/03/16 Pct Recovery = 39% Analysis Date = 08/01/16 Pct Recovery = 39% Analysis Date = 08/01/16 Pct Recovery = 39% Analysis Date = 07/30/16 Pct Recovery = 39% Analysis Date = 07/30/16 Pct Recovery = 39% Analysis Date = 07/27/16 Pct Recovery = 39% Analysis Date = 07/27/16 Pct Recovery = 39% Analysis Date = 07/25/16 Pct Recovery = 38% Analysis Date = 07/25/16 Pct Recovery = 38% Analysis Date = 07/23/16 Pct Recovery = 38% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CHLORPHENIRAMINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 23 61% 24% 59% 27%
>= Reporting Level 21 48% 12% 48% 11%
Total 44 55% 20% 50% 19%

Sample Statistics
CHLORPHENIRAMINE

Characteristic N % % Basis
Plotted 44 86% Spiked
Estimated Values 39 76% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 5 10% Spiked
Spiked 51 .  
False Negatives 2 4% 2 out of 51
Not Spiked 35 .  
False Positives 0 0% 0 out of 35