OBSP Determination:
ACYCLOVIR
METHOD: 2440 , TESTIDCODE: 67484LCM56

Analysis Date = 09/21/17 SpikeMix = Abs 072517Pharm2: 80 µl & Abs 071817Pharm: 80 µl Pct Recovery = 249% Analysis Date = 08/25/17 SpikeMix = Abs 072517Pharm2: 50 µl & Abs 071817Pharm: 50 µl Pct Recovery = 267% Analysis Date = 02/07/17 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 279% Analysis Date = 02/07/17 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 234% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 327% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 307% Analysis Date = 11/08/17 SpikeMix = Abs 072517Pharm2: 20 µl & ERA 06281704: 20 µl Pct Recovery = 534% Analysis Date = 10/22/17 SpikeMix = ERA 06281703: 20 µl & ERA 06281704: 20 µl Pct Recovery = 207% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 239% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 313% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 281% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 336% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 41% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 46% Analysis Date = 06/17/17 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 64% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 44% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 46% Analysis Date = 11/09/17 SpikeMix = ERA 06281704: 50 µl & ERA 06281702: 50 µl Pct Recovery = 78% Analysis Date = 08/11/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 82% Analysis Date = 04/06/17 SpikeMix = ERA 04281604: 40 µl & ERA 04281603: 40 µl Pct Recovery = 56% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 111% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 104% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 57% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 48% Analysis Date = 11/08/17 SpikeMix = ERA 06281704: 20 µl & Abs 072517Pharm1: 20 µl Pct Recovery = 94% Analysis Date = 08/11/17 SpikeMix = Abs 060916PHARM: 20 µl & Abs 071817Pharm: 20 µl Pct Recovery = 124% Analysis Date = 10/02/17 Pct Recovery = 204% Analysis Date = 10/02/17 Pct Recovery = 204% Analysis Date = 09/29/17 Pct Recovery = 203% Analysis Date = 09/29/17 Pct Recovery = 203% Analysis Date = 09/26/17 Pct Recovery = 201% Analysis Date = 09/26/17 Pct Recovery = 201% Analysis Date = 09/23/17 Pct Recovery = 200% Analysis Date = 09/23/17 Pct Recovery = 200% Analysis Date = 09/20/17 Pct Recovery = 198% Analysis Date = 09/20/17 Pct Recovery = 198% Analysis Date = 09/17/17 Pct Recovery = 197% Analysis Date = 09/17/17 Pct Recovery = 197% Analysis Date = 09/14/17 Pct Recovery = 195% Analysis Date = 09/14/17 Pct Recovery = 195% Analysis Date = 09/12/17 Pct Recovery = 194% Analysis Date = 09/12/17 Pct Recovery = 194% Analysis Date = 09/09/17 Pct Recovery = 192% Analysis Date = 09/09/17 Pct Recovery = 192% Analysis Date = 09/06/17 Pct Recovery = 191% Analysis Date = 09/06/17 Pct Recovery = 191% Analysis Date = 09/03/17 Pct Recovery = 189% Analysis Date = 09/03/17 Pct Recovery = 189% Analysis Date = 08/31/17 Pct Recovery = 188% Analysis Date = 08/31/17 Pct Recovery = 188% Analysis Date = 08/28/17 Pct Recovery = 186% Analysis Date = 08/28/17 Pct Recovery = 186% Analysis Date = 08/25/17 Pct Recovery = 185% Analysis Date = 08/25/17 Pct Recovery = 185% Analysis Date = 08/22/17 Pct Recovery = 184% Analysis Date = 08/22/17 Pct Recovery = 184% Analysis Date = 08/19/17 Pct Recovery = 182% Analysis Date = 08/19/17 Pct Recovery = 182% Analysis Date = 08/17/17 Pct Recovery = 181% Analysis Date = 08/17/17 Pct Recovery = 181% Analysis Date = 08/14/17 Pct Recovery = 179% Analysis Date = 08/14/17 Pct Recovery = 179% Analysis Date = 08/11/17 Pct Recovery = 178% Analysis Date = 08/11/17 Pct Recovery = 178% Analysis Date = 08/08/17 Pct Recovery = 177% Analysis Date = 08/08/17 Pct Recovery = 177% Analysis Date = 08/05/17 Pct Recovery = 176% Analysis Date = 08/05/17 Pct Recovery = 176% Analysis Date = 08/02/17 Pct Recovery = 174% Analysis Date = 08/02/17 Pct Recovery = 174% Analysis Date = 07/30/17 Pct Recovery = 173% Analysis Date = 07/30/17 Pct Recovery = 173% Analysis Date = 07/27/17 Pct Recovery = 172% Analysis Date = 07/27/17 Pct Recovery = 172% Analysis Date = 07/24/17 Pct Recovery = 171% Analysis Date = 07/24/17 Pct Recovery = 171% Analysis Date = 07/21/17 Pct Recovery = 170% Analysis Date = 07/21/17 Pct Recovery = 170% Analysis Date = 07/19/17 Pct Recovery = 169% Analysis Date = 07/19/17 Pct Recovery = 169% Analysis Date = 07/16/17 Pct Recovery = 168% Analysis Date = 07/16/17 Pct Recovery = 168% Analysis Date = 07/13/17 Pct Recovery = 167% Analysis Date = 07/13/17 Pct Recovery = 167% Analysis Date = 07/10/17 Pct Recovery = 166% Analysis Date = 07/10/17 Pct Recovery = 166% Analysis Date = 07/07/17 Pct Recovery = 164% Analysis Date = 07/07/17 Pct Recovery = 164% Analysis Date = 07/04/17 Pct Recovery = 163% Analysis Date = 07/04/17 Pct Recovery = 163% Analysis Date = 07/01/17 Pct Recovery = 162% Analysis Date = 07/01/17 Pct Recovery = 162% Analysis Date = 06/28/17 Pct Recovery = 161% Analysis Date = 06/28/17 Pct Recovery = 161% Analysis Date = 06/25/17 Pct Recovery = 160% Analysis Date = 06/25/17 Pct Recovery = 160% Analysis Date = 06/23/17 Pct Recovery = 159% Analysis Date = 06/23/17 Pct Recovery = 159% Analysis Date = 06/20/17 Pct Recovery = 158% Analysis Date = 06/20/17 Pct Recovery = 158% Analysis Date = 06/17/17 Pct Recovery = 157% Analysis Date = 06/17/17 Pct Recovery = 157% Analysis Date = 06/14/17 Pct Recovery = 156% Analysis Date = 06/14/17 Pct Recovery = 156% Analysis Date = 06/11/17 Pct Recovery = 155% Analysis Date = 06/11/17 Pct Recovery = 155% Analysis Date = 06/08/17 Pct Recovery = 153% Analysis Date = 06/08/17 Pct Recovery = 153% Analysis Date = 06/05/17 Pct Recovery = 152% Analysis Date = 06/05/17 Pct Recovery = 152% Analysis Date = 06/02/17 Pct Recovery = 151% Analysis Date = 06/02/17 Pct Recovery = 151% Analysis Date = 05/30/17 Pct Recovery = 150% Analysis Date = 05/30/17 Pct Recovery = 150% Analysis Date = 05/27/17 Pct Recovery = 149% Analysis Date = 05/27/17 Pct Recovery = 149% Analysis Date = 05/25/17 Pct Recovery = 148% Analysis Date = 05/25/17 Pct Recovery = 148% Analysis Date = 05/22/17 Pct Recovery = 147% Analysis Date = 05/22/17 Pct Recovery = 147% Analysis Date = 05/19/17 Pct Recovery = 146% Analysis Date = 05/19/17 Pct Recovery = 146% Analysis Date = 05/16/17 Pct Recovery = 145% Analysis Date = 05/16/17 Pct Recovery = 145% Analysis Date = 05/13/17 Pct Recovery = 144% Analysis Date = 05/13/17 Pct Recovery = 144% Analysis Date = 05/10/17 Pct Recovery = 142% Analysis Date = 05/10/17 Pct Recovery = 142% Analysis Date = 05/07/17 Pct Recovery = 141% Analysis Date = 05/07/17 Pct Recovery = 141% Analysis Date = 05/04/17 Pct Recovery = 140% Analysis Date = 05/04/17 Pct Recovery = 140% Analysis Date = 05/01/17 Pct Recovery = 139% Analysis Date = 05/01/17 Pct Recovery = 139% Analysis Date = 04/29/17 Pct Recovery = 138% Analysis Date = 04/29/17 Pct Recovery = 138% Analysis Date = 04/26/17 Pct Recovery = 137% Analysis Date = 04/26/17 Pct Recovery = 137% Analysis Date = 04/23/17 Pct Recovery = 136% Analysis Date = 04/23/17 Pct Recovery = 136% Analysis Date = 04/20/17 Pct Recovery = 135% Analysis Date = 04/20/17 Pct Recovery = 135% Analysis Date = 04/17/17 Pct Recovery = 134% Analysis Date = 04/17/17 Pct Recovery = 134% Analysis Date = 04/14/17 Pct Recovery = 133% Analysis Date = 04/14/17 Pct Recovery = 133% Analysis Date = 04/11/17 Pct Recovery = 131% Analysis Date = 04/11/17 Pct Recovery = 131% Analysis Date = 04/08/17 Pct Recovery = 130% Analysis Date = 04/08/17 Pct Recovery = 130% Analysis Date = 04/05/17 Pct Recovery = 129% Analysis Date = 04/05/17 Pct Recovery = 129% Analysis Date = 04/02/17 Pct Recovery = 129% Analysis Date = 04/02/17 Pct Recovery = 129% Analysis Date = 03/31/17 Pct Recovery = 129% Analysis Date = 03/31/17 Pct Recovery = 129% Analysis Date = 03/28/17 Pct Recovery = 129% Analysis Date = 03/28/17 Pct Recovery = 129% Analysis Date = 03/25/17 Pct Recovery = 129% Analysis Date = 03/25/17 Pct Recovery = 129% Analysis Date = 03/22/17 Pct Recovery = 129% Analysis Date = 03/22/17 Pct Recovery = 129% Analysis Date = 03/19/17 Pct Recovery = 129% Analysis Date = 03/19/17 Pct Recovery = 129% Analysis Date = 03/16/17 Pct Recovery = 129% Analysis Date = 03/16/17 Pct Recovery = 129% Analysis Date = 03/13/17 Pct Recovery = 128% Analysis Date = 03/13/17 Pct Recovery = 128% Analysis Date = 03/10/17 Pct Recovery = 128% Analysis Date = 03/10/17 Pct Recovery = 128% Analysis Date = 03/07/17 Pct Recovery = 128% Analysis Date = 03/07/17 Pct Recovery = 128% Analysis Date = 03/05/17 Pct Recovery = 128% Analysis Date = 03/05/17 Pct Recovery = 128% Analysis Date = 03/02/17 Pct Recovery = 128% Analysis Date = 03/02/17 Pct Recovery = 128% Analysis Date = 02/27/17 Pct Recovery = 128% Analysis Date = 02/27/17 Pct Recovery = 128% Analysis Date = 02/24/17 Pct Recovery = 128% Analysis Date = 02/24/17 Pct Recovery = 128% Analysis Date = 02/21/17 Pct Recovery = 128% Analysis Date = 02/21/17 Pct Recovery = 128% Analysis Date = 02/18/17 Pct Recovery = 128% Analysis Date = 02/18/17 Pct Recovery = 128% Analysis Date = 02/15/17 Pct Recovery = 127% Analysis Date = 02/15/17 Pct Recovery = 127% Analysis Date = 02/12/17 Pct Recovery = 127% Analysis Date = 02/12/17 Pct Recovery = 127% Analysis Date = 02/09/17 Pct Recovery = 127% Analysis Date = 02/09/17 Pct Recovery = 127% Analysis Date = 02/06/17 Pct Recovery = 127% Analysis Date = 02/06/17 Pct Recovery = 127% Analysis Date = 02/04/17 Pct Recovery = 127% Analysis Date = 02/04/17 Pct Recovery = 127% Analysis Date = 02/01/17 Pct Recovery = 126% Analysis Date = 02/01/17 Pct Recovery = 126% Analysis Date = 01/29/17 Pct Recovery = 125% Analysis Date = 01/29/17 Pct Recovery = 125% Analysis Date = 01/26/17 Pct Recovery = 125% Analysis Date = 01/26/17 Pct Recovery = 125% Analysis Date = 01/23/17 Pct Recovery = 124% Analysis Date = 01/23/17 Pct Recovery = 124% Analysis Date = 01/20/17 Pct Recovery = 124% Analysis Date = 01/20/17 Pct Recovery = 124% Analysis Date = 01/17/17 Pct Recovery = 123% Analysis Date = 01/17/17 Pct Recovery = 123% Analysis Date = 01/14/17 Pct Recovery = 122% Analysis Date = 01/14/17 Pct Recovery = 122% Analysis Date = 01/11/17 Pct Recovery = 122% Analysis Date = 01/11/17 Pct Recovery = 122% Analysis Date = 01/09/17 Pct Recovery = 121% Analysis Date = 01/09/17 Pct Recovery = 121% Analysis Date = 01/06/17 Pct Recovery = 121% Analysis Date = 01/06/17 Pct Recovery = 121% Analysis Date = 01/03/17 Pct Recovery = 121% Analysis Date = 01/03/17 Pct Recovery = 121% Analysis Date = 12/31/16 Pct Recovery = 121% Analysis Date = 12/31/16 Pct Recovery = 121% Analysis Date = 12/28/16 Pct Recovery = 122% Analysis Date = 12/28/16 Pct Recovery = 122% Analysis Date = 12/25/16 Pct Recovery = 122% Analysis Date = 12/25/16 Pct Recovery = 122% Analysis Date = 12/22/16 Pct Recovery = 123% Analysis Date = 12/22/16 Pct Recovery = 123% Analysis Date = 12/19/16 Pct Recovery = 123% Analysis Date = 12/19/16 Pct Recovery = 123% Analysis Date = 12/16/16 Pct Recovery = 123% Analysis Date = 12/16/16 Pct Recovery = 123% Analysis Date = 12/13/16 Pct Recovery = 124% Analysis Date = 12/13/16 Pct Recovery = 124% Analysis Date = 12/11/16 Pct Recovery = 124% Analysis Date = 12/11/16 Pct Recovery = 124% Analysis Date = 12/08/16 Pct Recovery = 125% Analysis Date = 12/08/16 Pct Recovery = 125% Analysis Date = 12/05/16 Pct Recovery = 125% Analysis Date = 12/05/16 Pct Recovery = 125% Analysis Date = 12/02/16 Pct Recovery = 126% Analysis Date = 12/02/16 Pct Recovery = 126% Analysis Date = 11/29/16 Pct Recovery = 126% Analysis Date = 11/29/16 Pct Recovery = 126% Analysis Date = 11/26/16 Pct Recovery = 127% Analysis Date = 11/26/16 Pct Recovery = 127% Analysis Date = 11/23/16 Pct Recovery = 127% Analysis Date = 11/23/16 Pct Recovery = 127% Analysis Date = 11/20/16 Pct Recovery = 128% Analysis Date = 11/20/16 Pct Recovery = 128% Analysis Date = 11/17/16 Pct Recovery = 128% Analysis Date = 11/17/16 Pct Recovery = 128% Analysis Date = 11/15/16 Pct Recovery = 128% Analysis Date = 11/15/16 Pct Recovery = 128% Analysis Date = 11/12/16 Pct Recovery = 129% Analysis Date = 11/12/16 Pct Recovery = 129% Analysis Date = 11/09/16 Pct Recovery = 129% Analysis Date = 11/09/16 Pct Recovery = 129% Analysis Date = 11/06/16 Pct Recovery = 130% Analysis Date = 11/06/16 Pct Recovery = 130% Analysis Date = 11/03/16 Pct Recovery = 130% Analysis Date = 11/03/16 Pct Recovery = 130% Analysis Date = 10/31/16 Pct Recovery = 131% Analysis Date = 10/31/16 Pct Recovery = 131% Analysis Date = 10/28/16 Pct Recovery = 132% Analysis Date = 10/28/16 Pct Recovery = 132% Analysis Date = 10/25/16 Pct Recovery = 135% Analysis Date = 10/25/16 Pct Recovery = 135% Analysis Date = 10/22/16 Pct Recovery = 137% Analysis Date = 10/22/16 Pct Recovery = 137% Analysis Date = 10/19/16 Pct Recovery = 140% Analysis Date = 10/19/16 Pct Recovery = 140% Analysis Date = 10/17/16 Pct Recovery = 143% Analysis Date = 10/17/16 Pct Recovery = 143% Analysis Date = 10/14/16 Pct Recovery = 145% Analysis Date = 10/14/16 Pct Recovery = 145% Analysis Date = 10/11/16 Pct Recovery = 148% Analysis Date = 10/11/16 Pct Recovery = 148% Analysis Date = 10/08/16 Pct Recovery = 151% Analysis Date = 10/08/16 Pct Recovery = 151% Analysis Date = 10/05/16 Pct Recovery = 154% Analysis Date = 10/05/16 Pct Recovery = 154% Analysis Date = 10/02/16 Pct Recovery = 156% Analysis Date = 10/02/16 Pct Recovery = 156% Analysis Date = 09/29/16 Pct Recovery = 159% Analysis Date = 09/29/16 Pct Recovery = 159% Analysis Date = 09/26/16 Pct Recovery = 162% Analysis Date = 09/26/16 Pct Recovery = 162% Analysis Date = 09/23/16 Pct Recovery = 164% Analysis Date = 09/23/16 Pct Recovery = 164% Analysis Date = 09/21/16 Pct Recovery = 167% Analysis Date = 09/21/16 Pct Recovery = 167% Analysis Date = 09/18/16 Pct Recovery = 170% Analysis Date = 09/18/16 Pct Recovery = 170% Analysis Date = 09/15/16 Pct Recovery = 172% Analysis Date = 09/15/16 Pct Recovery = 172% Analysis Date = 09/12/16 Pct Recovery = 175% Analysis Date = 09/12/16 Pct Recovery = 175% Analysis Date = 09/09/16 Pct Recovery = 178% Analysis Date = 09/09/16 Pct Recovery = 178% Analysis Date = 09/06/16 Pct Recovery = 180% Analysis Date = 09/06/16 Pct Recovery = 180% Analysis Date = 09/03/16 Pct Recovery = 183% Analysis Date = 09/03/16 Pct Recovery = 183% Analysis Date = 08/31/16 Pct Recovery = 186% Analysis Date = 08/31/16 Pct Recovery = 186% Analysis Date = 08/28/16 Pct Recovery = 188% Analysis Date = 08/28/16 Pct Recovery = 188% Analysis Date = 08/25/16 Pct Recovery = 191% Analysis Date = 08/25/16 Pct Recovery = 191% Analysis Date = 08/23/16 Pct Recovery = 194% Analysis Date = 08/23/16 Pct Recovery = 194% Analysis Date = 08/20/16 Pct Recovery = 197% Analysis Date = 08/20/16 Pct Recovery = 197% Analysis Date = 08/17/16 Pct Recovery = 199% Analysis Date = 08/17/16 Pct Recovery = 199% Analysis Date = 08/14/16 Pct Recovery = 202% Analysis Date = 08/14/16 Pct Recovery = 202% Analysis Date = 08/11/16 Pct Recovery = 205% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ACYCLOVIR

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 336% . 336% 0%
>= Reporting Level 25 169% 128% 111% 156%
Total 26 176% 130% 118% 164%

Sample Statistics
ACYCLOVIR

Characteristic N % % Basis
Plotted 26 74% Spiked
Estimated Values 20 57% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 6% Spiked
Spiked 35 .  
False Negatives 7 20% 7 out of 35
Not Spiked 47 .  
False Positives 16 34% 16 out of 47