BQS OBSP Determination:
ANTIPYRENE
METHOD: 2440 , TESTIDCODE: 67477LCM56
Open Data Set

Analysis Date = 02/07/17 SpikeMix = Abs 061416: 100 µl & ERA 04281603: 100 µl Pct Recovery = 83% Analysis Date = 02/07/17 SpikeMix = Abs 061416: 100 µl & ERA 04281603: 100 µl Pct Recovery = 86% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 97% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 90% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 81% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 76% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 76% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 81% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 75% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 79% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 79% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 73% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 73% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 78% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 80% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 89% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 90% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 97% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 100% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 88% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 78% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 84% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 76% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 73% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 97% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 72% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 76% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 96% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 70% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 84% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 67% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 68% Analysis Date = 03/14/17 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 89% Analysis Date = 03/14/17 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 87% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 102% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 117% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 90% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 86% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 80% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 79% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 69% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 77% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 72% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 61% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 89% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 63% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 66% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 81% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 83% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 84% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 79% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 77% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 78% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 78% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 73% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 74% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 78% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 58% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 55% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 81% Analysis Date = 03/13/17 Pct Recovery = 94% Analysis Date = 03/10/17 Pct Recovery = 93% Analysis Date = 03/10/17 Pct Recovery = 93% Analysis Date = 03/06/17 Pct Recovery = 93% Analysis Date = 03/06/17 Pct Recovery = 93% Analysis Date = 03/02/17 Pct Recovery = 93% Analysis Date = 03/02/17 Pct Recovery = 93% Analysis Date = 02/26/17 Pct Recovery = 92% Analysis Date = 02/26/17 Pct Recovery = 92% Analysis Date = 02/22/17 Pct Recovery = 92% Analysis Date = 02/22/17 Pct Recovery = 92% Analysis Date = 02/18/17 Pct Recovery = 92% Analysis Date = 02/18/17 Pct Recovery = 92% Analysis Date = 02/15/17 Pct Recovery = 91% Analysis Date = 02/15/17 Pct Recovery = 91% Analysis Date = 02/11/17 Pct Recovery = 91% Analysis Date = 02/11/17 Pct Recovery = 91% Analysis Date = 02/07/17 Pct Recovery = 91% Analysis Date = 02/07/17 Pct Recovery = 91% Analysis Date = 02/03/17 Pct Recovery = 90% Analysis Date = 02/03/17 Pct Recovery = 90% Analysis Date = 01/30/17 Pct Recovery = 90% Analysis Date = 01/30/17 Pct Recovery = 90% Analysis Date = 01/26/17 Pct Recovery = 90% Analysis Date = 01/26/17 Pct Recovery = 90% Analysis Date = 01/23/17 Pct Recovery = 89% Analysis Date = 01/23/17 Pct Recovery = 89% Analysis Date = 01/19/17 Pct Recovery = 89% Analysis Date = 01/19/17 Pct Recovery = 89% Analysis Date = 01/15/17 Pct Recovery = 88% Analysis Date = 01/15/17 Pct Recovery = 88% Analysis Date = 01/11/17 Pct Recovery = 88% Analysis Date = 01/11/17 Pct Recovery = 88% Analysis Date = 01/07/17 Pct Recovery = 88% Analysis Date = 01/07/17 Pct Recovery = 88% Analysis Date = 01/03/17 Pct Recovery = 87% Analysis Date = 01/03/17 Pct Recovery = 87% Analysis Date = 12/31/16 Pct Recovery = 87% Analysis Date = 12/31/16 Pct Recovery = 87% Analysis Date = 12/27/16 Pct Recovery = 87% Analysis Date = 12/27/16 Pct Recovery = 87% Analysis Date = 12/23/16 Pct Recovery = 86% Analysis Date = 12/23/16 Pct Recovery = 86% Analysis Date = 12/19/16 Pct Recovery = 86% Analysis Date = 12/19/16 Pct Recovery = 86% Analysis Date = 12/15/16 Pct Recovery = 86% Analysis Date = 12/15/16 Pct Recovery = 86% Analysis Date = 12/11/16 Pct Recovery = 85% Analysis Date = 12/11/16 Pct Recovery = 85% Analysis Date = 12/08/16 Pct Recovery = 85% Analysis Date = 12/08/16 Pct Recovery = 85% Analysis Date = 12/04/16 Pct Recovery = 85% Analysis Date = 12/04/16 Pct Recovery = 85% Analysis Date = 11/30/16 Pct Recovery = 84% Analysis Date = 11/30/16 Pct Recovery = 84% Analysis Date = 11/26/16 Pct Recovery = 84% Analysis Date = 11/26/16 Pct Recovery = 84% Analysis Date = 11/22/16 Pct Recovery = 84% Analysis Date = 11/22/16 Pct Recovery = 84% Analysis Date = 11/18/16 Pct Recovery = 83% Analysis Date = 11/18/16 Pct Recovery = 83% Analysis Date = 11/15/16 Pct Recovery = 83% Analysis Date = 11/15/16 Pct Recovery = 83% Analysis Date = 11/11/16 Pct Recovery = 83% Analysis Date = 11/11/16 Pct Recovery = 83% Analysis Date = 11/07/16 Pct Recovery = 82% Analysis Date = 11/07/16 Pct Recovery = 82% Analysis Date = 11/03/16 Pct Recovery = 82% Analysis Date = 11/03/16 Pct Recovery = 82% Analysis Date = 10/30/16 Pct Recovery = 82% Analysis Date = 10/30/16 Pct Recovery = 82% Analysis Date = 10/26/16 Pct Recovery = 81% Analysis Date = 10/26/16 Pct Recovery = 81% Analysis Date = 10/23/16 Pct Recovery = 81% Analysis Date = 10/23/16 Pct Recovery = 81% Analysis Date = 10/19/16 Pct Recovery = 81% Analysis Date = 10/19/16 Pct Recovery = 81% Analysis Date = 10/15/16 Pct Recovery = 81% Analysis Date = 10/15/16 Pct Recovery = 81% Analysis Date = 10/11/16 Pct Recovery = 80% Analysis Date = 10/11/16 Pct Recovery = 80% Analysis Date = 10/07/16 Pct Recovery = 80% Analysis Date = 10/07/16 Pct Recovery = 80% Analysis Date = 10/03/16 Pct Recovery = 80% Analysis Date = 10/03/16 Pct Recovery = 80% Analysis Date = 09/30/16 Pct Recovery = 79% Analysis Date = 09/30/16 Pct Recovery = 79% Analysis Date = 09/26/16 Pct Recovery = 79% Analysis Date = 09/26/16 Pct Recovery = 79% Analysis Date = 09/22/16 Pct Recovery = 79% Analysis Date = 09/22/16 Pct Recovery = 79% Analysis Date = 09/18/16 Pct Recovery = 78% Analysis Date = 09/18/16 Pct Recovery = 78% Analysis Date = 09/14/16 Pct Recovery = 78% Analysis Date = 09/14/16 Pct Recovery = 78% Analysis Date = 09/10/16 Pct Recovery = 78% Analysis Date = 09/10/16 Pct Recovery = 78% Analysis Date = 09/07/16 Pct Recovery = 78% Analysis Date = 09/07/16 Pct Recovery = 78% Analysis Date = 09/03/16 Pct Recovery = 77% Analysis Date = 09/03/16 Pct Recovery = 77% Analysis Date = 08/30/16 Pct Recovery = 77% Analysis Date = 08/30/16 Pct Recovery = 77% Analysis Date = 08/26/16 Pct Recovery = 77% Analysis Date = 08/26/16 Pct Recovery = 77% Analysis Date = 08/22/16 Pct Recovery = 76% Analysis Date = 08/22/16 Pct Recovery = 76% Analysis Date = 08/18/16 Pct Recovery = 76% Analysis Date = 08/18/16 Pct Recovery = 76% Analysis Date = 08/15/16 Pct Recovery = 76% Analysis Date = 08/15/16 Pct Recovery = 76% Analysis Date = 08/11/16 Pct Recovery = 76% Analysis Date = 08/11/16 Pct Recovery = 76% Analysis Date = 08/07/16 Pct Recovery = 76% Analysis Date = 08/07/16 Pct Recovery = 76% Analysis Date = 08/03/16 Pct Recovery = 75% Analysis Date = 08/03/16 Pct Recovery = 75% Analysis Date = 07/30/16 Pct Recovery = 75% Analysis Date = 07/30/16 Pct Recovery = 75% Analysis Date = 07/26/16 Pct Recovery = 75% Analysis Date = 07/26/16 Pct Recovery = 75% Analysis Date = 07/23/16 Pct Recovery = 75% Analysis Date = 07/23/16 Pct Recovery = 75% Analysis Date = 07/19/16 Pct Recovery = 75% Analysis Date = 07/19/16 Pct Recovery = 75% Analysis Date = 07/15/16 Pct Recovery = 75% Analysis Date = 07/15/16 Pct Recovery = 75% Analysis Date = 07/11/16 Pct Recovery = 75% Analysis Date = 07/11/16 Pct Recovery = 75% Analysis Date = 07/07/16 Pct Recovery = 75% Analysis Date = 07/07/16 Pct Recovery = 75% Analysis Date = 07/03/16 Pct Recovery = 75% Analysis Date = 07/03/16 Pct Recovery = 75% Analysis Date = 06/30/16 Pct Recovery = 75% Analysis Date = 06/30/16 Pct Recovery = 75% Analysis Date = 06/26/16 Pct Recovery = 75% Analysis Date = 06/26/16 Pct Recovery = 75% Analysis Date = 06/22/16 Pct Recovery = 75% Analysis Date = 06/22/16 Pct Recovery = 75% Analysis Date = 06/18/16 Pct Recovery = 75% Analysis Date = 06/18/16 Pct Recovery = 75% Analysis Date = 06/14/16 Pct Recovery = 75% Analysis Date = 06/14/16 Pct Recovery = 75% Analysis Date = 06/10/16 Pct Recovery = 75% Analysis Date = 06/10/16 Pct Recovery = 75% Analysis Date = 06/07/16 Pct Recovery = 75% Analysis Date = 06/07/16 Pct Recovery = 75% Analysis Date = 06/03/16 Pct Recovery = 75% Analysis Date = 06/03/16 Pct Recovery = 75% Analysis Date = 05/30/16 Pct Recovery = 75% Analysis Date = 05/30/16 Pct Recovery = 75% Analysis Date = 05/26/16 Pct Recovery = 75% Analysis Date = 05/26/16 Pct Recovery = 75% Analysis Date = 05/22/16 Pct Recovery = 75% Analysis Date = 05/22/16 Pct Recovery = 75% Analysis Date = 05/18/16 Pct Recovery = 75% Analysis Date = 05/18/16 Pct Recovery = 75% Analysis Date = 05/15/16 Pct Recovery = 75% Analysis Date = 05/15/16 Pct Recovery = 75% Analysis Date = 05/11/16 Pct Recovery = 75% Analysis Date = 05/11/16 Pct Recovery = 75% Analysis Date = 05/07/16 Pct Recovery = 75% Analysis Date = 05/07/16 Pct Recovery = 75% Analysis Date = 05/03/16 Pct Recovery = 75% Analysis Date = 05/03/16 Pct Recovery = 75% Analysis Date = 04/29/16 Pct Recovery = 75% Analysis Date = 04/29/16 Pct Recovery = 75% Analysis Date = 04/25/16 Pct Recovery = 74% Analysis Date = 04/25/16 Pct Recovery = 74% Analysis Date = 04/22/16 Pct Recovery = 74% Analysis Date = 04/22/16 Pct Recovery = 74% Analysis Date = 04/18/16 Pct Recovery = 74% Analysis Date = 04/18/16 Pct Recovery = 74% Analysis Date = 04/14/16 Pct Recovery = 74% Analysis Date = 04/14/16 Pct Recovery = 74% Analysis Date = 04/10/16 Pct Recovery = 74% Analysis Date = 04/10/16 Pct Recovery = 74% Analysis Date = 04/06/16 Pct Recovery = 74% Analysis Date = 04/06/16 Pct Recovery = 74% Analysis Date = 04/02/16 Pct Recovery = 75% Analysis Date = 04/02/16 Pct Recovery = 75% Analysis Date = 03/30/16 Pct Recovery = 75% Analysis Date = 03/30/16 Pct Recovery = 75% Analysis Date = 03/26/16 Pct Recovery = 75% Analysis Date = 03/26/16 Pct Recovery = 75% Analysis Date = 03/22/16 Pct Recovery = 75% Analysis Date = 03/22/16 Pct Recovery = 75% Analysis Date = 03/18/16 Pct Recovery = 75% Analysis Date = 03/18/16 Pct Recovery = 75% Analysis Date = 03/14/16 Pct Recovery = 75% Analysis Date = 03/14/16 Pct Recovery = 75% Analysis Date = 03/10/16 Pct Recovery = 75% Analysis Date = 03/10/16 Pct Recovery = 75% Analysis Date = 03/07/16 Pct Recovery = 75% Analysis Date = 03/07/16 Pct Recovery = 75% Analysis Date = 03/03/16 Pct Recovery = 75% Analysis Date = 03/03/16 Pct Recovery = 75% Analysis Date = 02/28/16 Pct Recovery = 75% Analysis Date = 02/28/16 Pct Recovery = 75% Analysis Date = 02/24/16 Pct Recovery = 75% Analysis Date = 02/24/16 Pct Recovery = 75% Analysis Date = 02/20/16 Pct Recovery = 75% Analysis Date = 02/20/16 Pct Recovery = 75% Analysis Date = 02/16/16 Pct Recovery = 75% Analysis Date = 02/16/16 Pct Recovery = 75% Analysis Date = 02/12/16 Pct Recovery = 75% Analysis Date = 02/12/16 Pct Recovery = 75% Analysis Date = 02/09/16 Pct Recovery = 75% Analysis Date = 02/09/16 Pct Recovery = 75% Analysis Date = 02/05/16 Pct Recovery = 75% Analysis Date = 02/05/16 Pct Recovery = 75% Analysis Date = 02/01/16 Pct Recovery = 75% Analysis Date = 02/01/16 Pct Recovery = 75% Analysis Date = 01/28/16 Pct Recovery = 75% Analysis Date = 01/28/16 Pct Recovery = 75% Analysis Date = 01/24/16 Pct Recovery = 75% Analysis Date = 01/24/16 Pct Recovery = 75% Analysis Date = 01/20/16 Pct Recovery = 76% Analysis Date = 01/20/16 Pct Recovery = 76% Analysis Date = 01/17/16 Pct Recovery = 76% Analysis Date = 01/17/16 Pct Recovery = 76% Analysis Date = 01/13/16 Pct Recovery = 76% Analysis Date = 01/13/16 Pct Recovery = 76% Analysis Date = 01/09/16 Pct Recovery = 76% Analysis Date = 01/09/16 Pct Recovery = 76% Analysis Date = 01/05/16 Pct Recovery = 76% Analysis Date = 01/05/16 Pct Recovery = 76% Analysis Date = 01/01/16 Pct Recovery = 76% Analysis Date = 01/01/16 Pct Recovery = 76% Analysis Date = 12/28/15 Pct Recovery = 76% Analysis Date = 12/28/15 Pct Recovery = 76% Analysis Date = 12/25/15 Pct Recovery = 76% Analysis Date = 12/25/15 Pct Recovery = 76% Analysis Date = 12/21/15 Pct Recovery = 77% Analysis Date = 12/21/15 Pct Recovery = 77% Analysis Date = 12/17/15 Pct Recovery = 77% Analysis Date = 12/17/15 Pct Recovery = 77% Analysis Date = 12/13/15 Pct Recovery = 77% Analysis Date = 12/13/15 Pct Recovery = 77% Analysis Date = 12/09/15 Pct Recovery = 77% Analysis Date = 12/09/15 Pct Recovery = 77% Analysis Date = 12/05/15 Pct Recovery = 77% Analysis Date = 12/05/15 Pct Recovery = 77% Analysis Date = 12/02/15 Pct Recovery = 77% Analysis Date = 12/02/15 Pct Recovery = 77% Analysis Date = 11/28/15 Pct Recovery = 77% Analysis Date = 11/28/15 Pct Recovery = 77% Analysis Date = 11/24/15 Pct Recovery = 77% Analysis Date = 11/24/15 Pct Recovery = 77% Analysis Date = 11/20/15 Pct Recovery = 78% Analysis Date = 11/20/15 Pct Recovery = 78% Analysis Date = 11/16/15 Pct Recovery = 78% Analysis Date = 11/16/15 Pct Recovery = 78% Analysis Date = 11/12/15 Pct Recovery = 78% Analysis Date = 11/12/15 Pct Recovery = 78% Analysis Date = 11/09/15 Pct Recovery = 78% Analysis Date = 11/09/15 Pct Recovery = 78% Analysis Date = 11/05/15 Pct Recovery = 78% Analysis Date = 11/05/15 Pct Recovery = 78% Analysis Date = 11/01/15 Pct Recovery = 79% Analysis Date = 11/01/15 Pct Recovery = 79% Analysis Date = 10/28/15 Pct Recovery = 79% Analysis Date = 10/28/15 Pct Recovery = 79% Analysis Date = 10/24/15 Pct Recovery = 79% Analysis Date = 10/24/15 Pct Recovery = 79% Analysis Date = 10/20/15 Pct Recovery = 79% Analysis Date = 10/20/15 Pct Recovery = 79% Analysis Date = 10/17/15 Pct Recovery = 79% Analysis Date = 10/17/15 Pct Recovery = 79% Analysis Date = 10/13/15 Pct Recovery = 79% Analysis Date = 10/13/15 Pct Recovery = 79% Analysis Date = 10/09/15 Pct Recovery = 80% Analysis Date = 10/09/15 Pct Recovery = 80% Analysis Date = 10/05/15 Pct Recovery = 80% Analysis Date = 10/05/15 Pct Recovery = 80% Analysis Date = 10/01/15 Pct Recovery = 80% Analysis Date = 10/01/15 Pct Recovery = 80% Analysis Date = 09/27/15 Pct Recovery = 80% Analysis Date = 09/27/15 Pct Recovery = 80% Analysis Date = 09/24/15 Pct Recovery = 80% Analysis Date = 09/24/15 Pct Recovery = 80% Analysis Date = 09/20/15 Pct Recovery = 80% Analysis Date = 09/20/15 Pct Recovery = 80% Analysis Date = 09/16/15 Pct Recovery = 81% Analysis Date = 09/16/15 Pct Recovery = 81% Analysis Date = 09/12/15 Pct Recovery = 81% Analysis Date = 09/12/15 Pct Recovery = 81% Analysis Date = 09/08/15 Pct Recovery = 81% Analysis Date = 09/08/15 Pct Recovery = 81% Analysis Date = 09/04/15 Pct Recovery = 81% Analysis Date = 09/04/15 Pct Recovery = 81% Analysis Date = 09/01/15 Pct Recovery = 81% Analysis Date = 09/01/15 Pct Recovery = 81% Analysis Date = 08/28/15 Pct Recovery = 81% Analysis Date = 08/28/15 Pct Recovery = 81% Analysis Date = 08/24/15 Pct Recovery = 82% Analysis Date = 08/24/15 Pct Recovery = 82% Analysis Date = 08/20/15 Pct Recovery = 82% Analysis Date = 08/20/15 Pct Recovery = 82% Analysis Date = 08/16/15 Pct Recovery = 82% Analysis Date = 08/16/15 Pct Recovery = 82% Analysis Date = 08/12/15 Pct Recovery = 82% Analysis Date = 08/12/15 Pct Recovery = 82% Analysis Date = 08/09/15 Pct Recovery = 82% Analysis Date = 08/09/15 Pct Recovery = 82% Analysis Date = 08/05/15 Pct Recovery = 82% Analysis Date = 08/05/15 Pct Recovery = 82% Analysis Date = 08/01/15 Pct Recovery = 82% Analysis Date = 08/01/15 Pct Recovery = 82% Analysis Date = 07/28/15 Pct Recovery = 83% Analysis Date = 07/28/15 Pct Recovery = 83% Analysis Date = 07/24/15 Pct Recovery = 83% Analysis Date = 07/24/15 Pct Recovery = 83% Analysis Date = 07/20/15 Pct Recovery = 83% Analysis Date = 07/20/15 Pct Recovery = 83% Analysis Date = 07/17/15 Pct Recovery = 83% Analysis Date = 07/17/15 Pct Recovery = 83% Analysis Date = 07/13/15 Pct Recovery = 83% Analysis Date = 07/13/15 Pct Recovery = 83% Analysis Date = 07/09/15 Pct Recovery = 83% Analysis Date = 07/09/15 Pct Recovery = 83% Analysis Date = 07/05/15 Pct Recovery = 83% Analysis Date = 07/05/15 Pct Recovery = 83% Analysis Date = 07/01/15 Pct Recovery = 84% Analysis Date = 07/01/15 Pct Recovery = 84% Analysis Date = 06/27/15 Pct Recovery = 84% Analysis Date = 06/27/15 Pct Recovery = 84% Analysis Date = 06/24/15 Pct Recovery = 84% Analysis Date = 06/24/15 Pct Recovery = 84% Analysis Date = 06/20/15 Pct Recovery = 84% Analysis Date = 06/20/15 Pct Recovery = 84% Analysis Date = 06/16/15 Pct Recovery = 84% Analysis Date = 06/16/15 Pct Recovery = 84% Analysis Date = 06/12/15 Pct Recovery = 84% Analysis Date = 06/12/15 Pct Recovery = 84% Analysis Date = 06/08/15 Pct Recovery = 85% Analysis Date = 06/08/15 Pct Recovery = 85% Analysis Date = 06/04/15 Pct Recovery = 85% Analysis Date = 06/04/15 Pct Recovery = 85% Analysis Date = 06/01/15 Pct Recovery = 85% Analysis Date = 06/01/15 Pct Recovery = 85% Analysis Date = 05/28/15 Pct Recovery = 85% Analysis Date = 05/28/15 Pct Recovery = 85% Analysis Date = 05/24/15 Pct Recovery = 85% Analysis Date = 05/24/15 Pct Recovery = 85% Analysis Date = 05/20/15 Pct Recovery = 85% Analysis Date = 05/20/15 Pct Recovery = 85% Analysis Date = 05/16/15 Pct Recovery = 85% Analysis Date = 05/16/15 Pct Recovery = 85% Analysis Date = 05/12/15 Pct Recovery = 86% Analysis Date = 05/12/15 Pct Recovery = 86% Analysis Date = 05/09/15 Pct Recovery = 86% Analysis Date = 05/09/15 Pct Recovery = 86% Analysis Date = 05/05/15 Pct Recovery = 86% Analysis Date = 05/05/15 Pct Recovery = 86% Analysis Date = 05/01/15 Pct Recovery = 86% Analysis Date = 05/01/15 Pct Recovery = 86% Analysis Date = 04/27/15 Pct Recovery = 86% Analysis Date = 04/27/15 Pct Recovery = 86% Analysis Date = 04/23/15 Pct Recovery = 86% Analysis Date = 04/23/15 Pct Recovery = 86% Analysis Date = 04/19/15 Pct Recovery = 87% Analysis Date = 04/19/15 Pct Recovery = 87% Analysis Date = 04/16/15 Pct Recovery = 87% Analysis Date = 04/16/15 Pct Recovery = 87% Analysis Date = 04/12/15 Pct Recovery = 87% Analysis Date = 04/12/15 Pct Recovery = 87% Analysis Date = 04/08/15 Pct Recovery = 87% Analysis Date = 04/08/15 Pct Recovery = 87% Analysis Date = 04/04/15 Pct Recovery = 87% Analysis Date = 04/04/15 Pct Recovery = 87% Analysis Date = 03/31/15 Pct Recovery = 87% Analysis Date = 03/31/15 Pct Recovery = 87% Analysis Date = 03/27/15 Pct Recovery = 88% Analysis Date = 03/27/15 Pct Recovery = 88% Analysis Date = 03/24/15 Pct Recovery = 88% Analysis Date = 03/24/15 Pct Recovery = 88% Analysis Date = 03/20/15 Pct Recovery = 88% Analysis Date = 03/20/15 Pct Recovery = 88% Analysis Date = 03/16/15 Pct Recovery = 88% Analysis Date = 03/16/15 Pct Recovery = 88% Analysis Date = 03/12/15 Pct Recovery = 88% Analysis Date = 03/12/15 Pct Recovery = 88% Analysis Date = 03/08/15 Pct Recovery = 88% Analysis Date = 03/08/15 Pct Recovery = 88% Analysis Date = 03/04/15 Pct Recovery = 88% Analysis Date = 03/04/15 Pct Recovery = 88% Analysis Date = 03/01/15 Pct Recovery = 89% Analysis Date = 03/01/15 Pct Recovery = 89% Analysis Date = 02/25/15 Pct Recovery = 89% Analysis Date = 02/25/15 Pct Recovery = 89% Analysis Date = 02/21/15 Pct Recovery = 89% Analysis Date = 02/21/15 Pct Recovery = 89% Analysis Date = 02/17/15 Pct Recovery = 89% Analysis Date = 02/17/15 Pct Recovery = 89% Analysis Date = 02/13/15 Pct Recovery = 89% Analysis Date = 02/13/15 Pct Recovery = 89% Analysis Date = 02/09/15 Pct Recovery = 89% Analysis Date = 02/09/15 Pct Recovery = 89% Analysis Date = 02/06/15 Pct Recovery = 90% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ANTIPYRENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 68% 18% 68% 19%
>= Reporting Level 58 81% 11% 79% 10%
Total 60 80% 11% 79% 10%

Sample Statistics
ANTIPYRENE

Characteristic N % % Basis
Plotted 60 100% Spiked
Estimated Values 5 8% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 60 .  
False Negatives 0 0% 0 out of 60
Not Spiked 33 .  
False Positives 0 0% 0 out of 33