OBSP Determination:
TERBUFOS OXON SULFOXIDE
METHOD: 2437 , TESTIDCODE: 68702LCM60

Analysis Date = 09/22/17 SpikeMix = Abs 071917Pest3: 80 µl & Abs 072417Pest3: 80 µl Pct Recovery = 84% Analysis Date = 07/11/17 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 71% Analysis Date = 06/24/17 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 71% Analysis Date = 03/01/17 SpikeMix = Abs 071816: 80 µl & Abs 072516: 80 µl Pct Recovery = 61% Analysis Date = 03/01/17 SpikeMix = Abs 071816: 80 µl & Abs 072516: 80 µl Pct Recovery = 73% Analysis Date = 01/18/17 SpikeMix = Spex Organics TS160511023: 80 µl & Abs 071816: 80 µl Pct Recovery = 185% Analysis Date = 01/17/17 SpikeMix = Spex Organics TS160511023: 80 µl & Abs 071816: 80 µl Pct Recovery = 177% Analysis Date = 12/13/16 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 78% Analysis Date = 12/13/16 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 83% Analysis Date = 08/21/16 SpikeMix = Abs 071816: 80 µl & Abs 072516: 80 µl Pct Recovery = 111% Analysis Date = 08/21/16 SpikeMix = Abs 071816: 80 µl & Abs 072516: 80 µl Pct Recovery = 116% Analysis Date = 10/04/17 SpikeMix = Abs 071917Pest3: 50 µl & Abs 071717Pest3: 50 µl Pct Recovery = 127% Analysis Date = 09/15/17 SpikeMix = Abs 071917Pest3: 50 µl & Abs 072417Pest3: 50 µl Pct Recovery = 120% Analysis Date = 09/06/17 SpikeMix = Abs 072417Pest3: 50 µl & Abs 071917Pest3: 50 µl Pct Recovery = 103% Analysis Date = 07/28/17 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 84% Analysis Date = 06/07/17 SpikeMix = Abs 071216: 40 µl & Abs 071816: 40 µl Pct Recovery = 100% Analysis Date = 05/07/17 SpikeMix = Abs 071816: 40 µl & Abs 072516: 40 µl Pct Recovery = 98% Analysis Date = 01/10/17 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 176% Analysis Date = 01/10/17 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 164% Analysis Date = 11/12/16 SpikeMix = Abs 071816: 40 µl & Abs 072516: 40 µl Pct Recovery = 109% Analysis Date = 11/12/16 SpikeMix = Abs 071816: 40 µl & Abs 072516: 40 µl Pct Recovery = 110% Analysis Date = 11/08/16 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 180% Analysis Date = 11/08/16 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 168% Analysis Date = 09/07/16 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 111% Analysis Date = 09/07/16 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 104% Analysis Date = 08/31/16 SpikeMix = Abs 071216: 40 µl & Abs 071816: 40 µl Pct Recovery = 74% Analysis Date = 08/30/16 SpikeMix = Abs 071216: 40 µl & Abs 071816: 40 µl Pct Recovery = 80% Analysis Date = 10/11/17 SpikeMix = Abs 071917Pest3: 20 µl & Abs 071717Pest3: 20 µl Pct Recovery = 108% Analysis Date = 08/27/17 SpikeMix = Abs 071917Pest3: 20 µl & Abs 072417Pest3: 20 µl Pct Recovery = 134% Analysis Date = 08/08/17 SpikeMix = Abs 071917Pest3: 20 µl & Abs 071717Pest3: 20 µl Pct Recovery = 69% Analysis Date = 11/11/16 SpikeMix = Abs 071216: 10 µl & Abs 071816: 10 µl Pct Recovery = 93% Analysis Date = 11/11/16 SpikeMix = Abs 071216: 10 µl & Abs 071816: 10 µl Pct Recovery = 81% Analysis Date = 10/11/17 Pct Recovery = 107% Analysis Date = 10/08/17 Pct Recovery = 107% Analysis Date = 10/08/17 Pct Recovery = 107% Analysis Date = 10/06/17 Pct Recovery = 106% Analysis Date = 10/06/17 Pct Recovery = 106% Analysis Date = 10/04/17 Pct Recovery = 106% Analysis Date = 10/04/17 Pct Recovery = 106% Analysis Date = 10/02/17 Pct Recovery = 106% Analysis Date = 10/02/17 Pct Recovery = 106% Analysis Date = 09/30/17 Pct Recovery = 105% Analysis Date = 09/30/17 Pct Recovery = 105% Analysis Date = 09/28/17 Pct Recovery = 105% Analysis Date = 09/28/17 Pct Recovery = 105% Analysis Date = 09/26/17 Pct Recovery = 105% Analysis Date = 09/26/17 Pct Recovery = 105% Analysis Date = 09/24/17 Pct Recovery = 104% Analysis Date = 09/24/17 Pct Recovery = 104% Analysis Date = 09/22/17 Pct Recovery = 104% Analysis Date = 09/22/17 Pct Recovery = 104% Analysis Date = 09/20/17 Pct Recovery = 104% Analysis Date = 09/20/17 Pct Recovery = 104% Analysis Date = 09/18/17 Pct Recovery = 103% Analysis Date = 09/18/17 Pct Recovery = 103% Analysis Date = 09/16/17 Pct Recovery = 103% Analysis Date = 09/16/17 Pct Recovery = 103% Analysis Date = 09/13/17 Pct Recovery = 103% Analysis Date = 09/13/17 Pct Recovery = 103% Analysis Date = 09/11/17 Pct Recovery = 102% Analysis Date = 09/11/17 Pct Recovery = 102% Analysis Date = 09/09/17 Pct Recovery = 102% Analysis Date = 09/09/17 Pct Recovery = 102% Analysis Date = 09/07/17 Pct Recovery = 102% Analysis Date = 09/07/17 Pct Recovery = 102% Analysis Date = 09/05/17 Pct Recovery = 101% Analysis Date = 09/05/17 Pct Recovery = 101% Analysis Date = 09/03/17 Pct Recovery = 101% Analysis Date = 09/03/17 Pct Recovery = 101% Analysis Date = 09/01/17 Pct Recovery = 101% Analysis Date = 09/01/17 Pct Recovery = 101% Analysis Date = 08/30/17 Pct Recovery = 101% Analysis Date = 08/30/17 Pct Recovery = 101% Analysis Date = 08/28/17 Pct Recovery = 100% Analysis Date = 08/28/17 Pct Recovery = 100% Analysis Date = 08/26/17 Pct Recovery = 100% Analysis Date = 08/26/17 Pct Recovery = 100% Analysis Date = 08/24/17 Pct Recovery = 100% Analysis Date = 08/24/17 Pct Recovery = 100% Analysis Date = 08/22/17 Pct Recovery = 99% Analysis Date = 08/22/17 Pct Recovery = 99% Analysis Date = 08/20/17 Pct Recovery = 99% Analysis Date = 08/20/17 Pct Recovery = 99% Analysis Date = 08/17/17 Pct Recovery = 99% Analysis Date = 08/17/17 Pct Recovery = 99% Analysis Date = 08/15/17 Pct Recovery = 99% Analysis Date = 08/15/17 Pct Recovery = 99% Analysis Date = 08/13/17 Pct Recovery = 98% Analysis Date = 08/13/17 Pct Recovery = 98% Analysis Date = 08/11/17 Pct Recovery = 98% Analysis Date = 08/11/17 Pct Recovery = 98% Analysis Date = 08/09/17 Pct Recovery = 98% Analysis Date = 08/09/17 Pct Recovery = 98% Analysis Date = 08/07/17 Pct Recovery = 98% Analysis Date = 08/07/17 Pct Recovery = 98% Analysis Date = 08/05/17 Pct Recovery = 97% Analysis Date = 08/05/17 Pct Recovery = 97% Analysis Date = 08/03/17 Pct Recovery = 97% Analysis Date = 08/03/17 Pct Recovery = 97% Analysis Date = 08/01/17 Pct Recovery = 97% Analysis Date = 08/01/17 Pct Recovery = 97% Analysis Date = 07/30/17 Pct Recovery = 97% Analysis Date = 07/30/17 Pct Recovery = 97% Analysis Date = 07/28/17 Pct Recovery = 97% Analysis Date = 07/28/17 Pct Recovery = 97% Analysis Date = 07/26/17 Pct Recovery = 96% Analysis Date = 07/26/17 Pct Recovery = 96% Analysis Date = 07/23/17 Pct Recovery = 96% Analysis Date = 07/23/17 Pct Recovery = 96% Analysis Date = 07/21/17 Pct Recovery = 96% Analysis Date = 07/21/17 Pct Recovery = 96% Analysis Date = 07/19/17 Pct Recovery = 96% Analysis Date = 07/19/17 Pct Recovery = 96% Analysis Date = 07/17/17 Pct Recovery = 96% Analysis Date = 07/17/17 Pct Recovery = 96% Analysis Date = 07/15/17 Pct Recovery = 95% Analysis Date = 07/15/17 Pct Recovery = 95% Analysis Date = 07/13/17 Pct Recovery = 95% Analysis Date = 07/13/17 Pct Recovery = 95% Analysis Date = 07/11/17 Pct Recovery = 95% Analysis Date = 07/11/17 Pct Recovery = 95% Analysis Date = 07/09/17 Pct Recovery = 95% Analysis Date = 07/09/17 Pct Recovery = 95% Analysis Date = 07/07/17 Pct Recovery = 95% Analysis Date = 07/07/17 Pct Recovery = 95% Analysis Date = 07/05/17 Pct Recovery = 94% Analysis Date = 07/05/17 Pct Recovery = 94% Analysis Date = 07/03/17 Pct Recovery = 94% Analysis Date = 07/03/17 Pct Recovery = 94% Analysis Date = 07/01/17 Pct Recovery = 94% Analysis Date = 07/01/17 Pct Recovery = 94% Analysis Date = 06/29/17 Pct Recovery = 94% Analysis Date = 06/29/17 Pct Recovery = 94% Analysis Date = 06/26/17 Pct Recovery = 94% Analysis Date = 06/26/17 Pct Recovery = 94% Analysis Date = 06/24/17 Pct Recovery = 94% Analysis Date = 06/24/17 Pct Recovery = 94% Analysis Date = 06/22/17 Pct Recovery = 94% Analysis Date = 06/22/17 Pct Recovery = 94% Analysis Date = 06/20/17 Pct Recovery = 93% Analysis Date = 06/20/17 Pct Recovery = 93% Analysis Date = 06/18/17 Pct Recovery = 93% Analysis Date = 06/18/17 Pct Recovery = 93% Analysis Date = 06/16/17 Pct Recovery = 93% Analysis Date = 06/16/17 Pct Recovery = 93% Analysis Date = 06/14/17 Pct Recovery = 93% Analysis Date = 06/14/17 Pct Recovery = 93% Analysis Date = 06/12/17 Pct Recovery = 93% Analysis Date = 06/12/17 Pct Recovery = 93% Analysis Date = 06/10/17 Pct Recovery = 93% Analysis Date = 06/10/17 Pct Recovery = 93% Analysis Date = 06/08/17 Pct Recovery = 93% Analysis Date = 06/08/17 Pct Recovery = 93% Analysis Date = 06/06/17 Pct Recovery = 93% Analysis Date = 06/06/17 Pct Recovery = 93% Analysis Date = 06/04/17 Pct Recovery = 93% Analysis Date = 06/04/17 Pct Recovery = 93% Analysis Date = 06/01/17 Pct Recovery = 94% Analysis Date = 06/01/17 Pct Recovery = 94% Analysis Date = 05/30/17 Pct Recovery = 94% Analysis Date = 05/30/17 Pct Recovery = 94% Analysis Date = 05/28/17 Pct Recovery = 95% Analysis Date = 05/28/17 Pct Recovery = 95% Analysis Date = 05/26/17 Pct Recovery = 95% Analysis Date = 05/26/17 Pct Recovery = 95% Analysis Date = 05/24/17 Pct Recovery = 95% Analysis Date = 05/24/17 Pct Recovery = 95% Analysis Date = 05/22/17 Pct Recovery = 96% Analysis Date = 05/22/17 Pct Recovery = 96% Analysis Date = 05/20/17 Pct Recovery = 96% Analysis Date = 05/20/17 Pct Recovery = 96% Analysis Date = 05/18/17 Pct Recovery = 97% Analysis Date = 05/18/17 Pct Recovery = 97% Analysis Date = 05/16/17 Pct Recovery = 97% Analysis Date = 05/16/17 Pct Recovery = 97% Analysis Date = 05/14/17 Pct Recovery = 98% Analysis Date = 05/14/17 Pct Recovery = 98% Analysis Date = 05/12/17 Pct Recovery = 98% Analysis Date = 05/12/17 Pct Recovery = 98% Analysis Date = 05/10/17 Pct Recovery = 98% Analysis Date = 05/10/17 Pct Recovery = 98% Analysis Date = 05/08/17 Pct Recovery = 99% Analysis Date = 05/08/17 Pct Recovery = 99% Analysis Date = 05/05/17 Pct Recovery = 99% Analysis Date = 05/05/17 Pct Recovery = 99% Analysis Date = 05/03/17 Pct Recovery = 100% Analysis Date = 05/03/17 Pct Recovery = 100% Analysis Date = 05/01/17 Pct Recovery = 100% Analysis Date = 05/01/17 Pct Recovery = 100% Analysis Date = 04/29/17 Pct Recovery = 101% Analysis Date = 04/29/17 Pct Recovery = 101% Analysis Date = 04/27/17 Pct Recovery = 101% Analysis Date = 04/27/17 Pct Recovery = 101% Analysis Date = 04/25/17 Pct Recovery = 102% Analysis Date = 04/25/17 Pct Recovery = 102% Analysis Date = 04/23/17 Pct Recovery = 102% Analysis Date = 04/23/17 Pct Recovery = 102% Analysis Date = 04/21/17 Pct Recovery = 102% Analysis Date = 04/21/17 Pct Recovery = 102% Analysis Date = 04/19/17 Pct Recovery = 103% Analysis Date = 04/19/17 Pct Recovery = 103% Analysis Date = 04/17/17 Pct Recovery = 103% Analysis Date = 04/17/17 Pct Recovery = 103% Analysis Date = 04/15/17 Pct Recovery = 104% Analysis Date = 04/15/17 Pct Recovery = 104% Analysis Date = 04/13/17 Pct Recovery = 104% Analysis Date = 04/13/17 Pct Recovery = 104% Analysis Date = 04/10/17 Pct Recovery = 105% Analysis Date = 04/10/17 Pct Recovery = 105% Analysis Date = 04/08/17 Pct Recovery = 105% Analysis Date = 04/08/17 Pct Recovery = 105% Analysis Date = 04/06/17 Pct Recovery = 106% Analysis Date = 04/06/17 Pct Recovery = 106% Analysis Date = 04/04/17 Pct Recovery = 106% Analysis Date = 04/04/17 Pct Recovery = 106% Analysis Date = 04/02/17 Pct Recovery = 106% Analysis Date = 04/02/17 Pct Recovery = 106% Analysis Date = 03/31/17 Pct Recovery = 107% Analysis Date = 03/31/17 Pct Recovery = 107% Analysis Date = 03/29/17 Pct Recovery = 107% Analysis Date = 03/29/17 Pct Recovery = 107% Analysis Date = 03/27/17 Pct Recovery = 108% Analysis Date = 03/27/17 Pct Recovery = 108% Analysis Date = 03/25/17 Pct Recovery = 108% Analysis Date = 03/25/17 Pct Recovery = 108% Analysis Date = 03/23/17 Pct Recovery = 109% Analysis Date = 03/23/17 Pct Recovery = 109% Analysis Date = 03/21/17 Pct Recovery = 109% Analysis Date = 03/21/17 Pct Recovery = 109% Analysis Date = 03/19/17 Pct Recovery = 110% Analysis Date = 03/19/17 Pct Recovery = 110% Analysis Date = 03/17/17 Pct Recovery = 110% Analysis Date = 03/17/17 Pct Recovery = 110% Analysis Date = 03/14/17 Pct Recovery = 110% Analysis Date = 03/14/17 Pct Recovery = 110% Analysis Date = 03/12/17 Pct Recovery = 111% Analysis Date = 03/12/17 Pct Recovery = 111% Analysis Date = 03/10/17 Pct Recovery = 111% Analysis Date = 03/10/17 Pct Recovery = 111% Analysis Date = 03/08/17 Pct Recovery = 112% Analysis Date = 03/08/17 Pct Recovery = 112% Analysis Date = 03/06/17 Pct Recovery = 112% Analysis Date = 03/06/17 Pct Recovery = 112% Analysis Date = 03/04/17 Pct Recovery = 113% Analysis Date = 03/04/17 Pct Recovery = 113% Analysis Date = 03/02/17 Pct Recovery = 113% Analysis Date = 03/02/17 Pct Recovery = 113% Analysis Date = 02/28/17 Pct Recovery = 114% Analysis Date = 02/28/17 Pct Recovery = 114% Analysis Date = 02/26/17 Pct Recovery = 114% Analysis Date = 02/26/17 Pct Recovery = 114% Analysis Date = 02/24/17 Pct Recovery = 114% Analysis Date = 02/24/17 Pct Recovery = 114% Analysis Date = 02/22/17 Pct Recovery = 115% Analysis Date = 02/22/17 Pct Recovery = 115% Analysis Date = 02/20/17 Pct Recovery = 115% Analysis Date = 02/20/17 Pct Recovery = 115% Analysis Date = 02/17/17 Pct Recovery = 116% Analysis Date = 02/17/17 Pct Recovery = 116% Analysis Date = 02/15/17 Pct Recovery = 116% Analysis Date = 02/15/17 Pct Recovery = 116% Analysis Date = 02/13/17 Pct Recovery = 117% Analysis Date = 02/13/17 Pct Recovery = 117% Analysis Date = 02/11/17 Pct Recovery = 117% Analysis Date = 02/11/17 Pct Recovery = 117% Analysis Date = 02/09/17 Pct Recovery = 117% Analysis Date = 02/09/17 Pct Recovery = 117% Analysis Date = 02/07/17 Pct Recovery = 118% Analysis Date = 02/07/17 Pct Recovery = 118% Analysis Date = 02/05/17 Pct Recovery = 118% Analysis Date = 02/05/17 Pct Recovery = 118% Analysis Date = 02/03/17 Pct Recovery = 119% Analysis Date = 02/03/17 Pct Recovery = 119% Analysis Date = 02/01/17 Pct Recovery = 119% Analysis Date = 02/01/17 Pct Recovery = 119% Analysis Date = 01/30/17 Pct Recovery = 120% Analysis Date = 01/30/17 Pct Recovery = 120% Analysis Date = 01/28/17 Pct Recovery = 120% Analysis Date = 01/28/17 Pct Recovery = 120% Analysis Date = 01/26/17 Pct Recovery = 120% Analysis Date = 01/26/17 Pct Recovery = 120% Analysis Date = 01/24/17 Pct Recovery = 121% Analysis Date = 01/24/17 Pct Recovery = 121% Analysis Date = 01/21/17 Pct Recovery = 121% Analysis Date = 01/21/17 Pct Recovery = 121% Analysis Date = 01/19/17 Pct Recovery = 122% Analysis Date = 01/19/17 Pct Recovery = 122% Analysis Date = 01/17/17 Pct Recovery = 122% Analysis Date = 01/17/17 Pct Recovery = 122% Analysis Date = 01/15/17 Pct Recovery = 123% Analysis Date = 01/15/17 Pct Recovery = 123% Analysis Date = 01/13/17 Pct Recovery = 123% Analysis Date = 01/13/17 Pct Recovery = 123% Analysis Date = 01/11/17 Pct Recovery = 124% Analysis Date = 01/11/17 Pct Recovery = 124% Analysis Date = 01/09/17 Pct Recovery = 124% Analysis Date = 01/09/17 Pct Recovery = 124% Analysis Date = 01/07/17 Pct Recovery = 125% Analysis Date = 01/07/17 Pct Recovery = 125% Analysis Date = 01/05/17 Pct Recovery = 125% Analysis Date = 01/05/17 Pct Recovery = 125% Analysis Date = 01/03/17 Pct Recovery = 125% Analysis Date = 01/03/17 Pct Recovery = 125% Analysis Date = 01/01/17 Pct Recovery = 126% Analysis Date = 01/01/17 Pct Recovery = 126% Analysis Date = 12/30/16 Pct Recovery = 126% Analysis Date = 12/30/16 Pct Recovery = 126% Analysis Date = 12/27/16 Pct Recovery = 127% Analysis Date = 12/27/16 Pct Recovery = 127% Analysis Date = 12/25/16 Pct Recovery = 127% Analysis Date = 12/25/16 Pct Recovery = 127% Analysis Date = 12/23/16 Pct Recovery = 127% Analysis Date = 12/23/16 Pct Recovery = 127% Analysis Date = 12/21/16 Pct Recovery = 128% Analysis Date = 12/21/16 Pct Recovery = 128% Analysis Date = 12/19/16 Pct Recovery = 128% Analysis Date = 12/19/16 Pct Recovery = 128% Analysis Date = 12/17/16 Pct Recovery = 129% Analysis Date = 12/17/16 Pct Recovery = 129% Analysis Date = 12/15/16 Pct Recovery = 129% Analysis Date = 12/15/16 Pct Recovery = 129% Analysis Date = 12/13/16 Pct Recovery = 130% Analysis Date = 12/13/16 Pct Recovery = 130% Analysis Date = 12/11/16 Pct Recovery = 129% Analysis Date = 12/11/16 Pct Recovery = 129% Analysis Date = 12/09/16 Pct Recovery = 128% Analysis Date = 12/09/16 Pct Recovery = 128% Analysis Date = 12/07/16 Pct Recovery = 128% Analysis Date = 12/07/16 Pct Recovery = 128% Analysis Date = 12/05/16 Pct Recovery = 127% Analysis Date = 12/05/16 Pct Recovery = 127% Analysis Date = 12/03/16 Pct Recovery = 127% Analysis Date = 12/03/16 Pct Recovery = 127% Analysis Date = 11/30/16 Pct Recovery = 126% Analysis Date = 11/30/16 Pct Recovery = 126% Analysis Date = 11/28/16 Pct Recovery = 125% Analysis Date = 11/28/16 Pct Recovery = 125% Analysis Date = 11/26/16 Pct Recovery = 125% Analysis Date = 11/26/16 Pct Recovery = 125% Analysis Date = 11/24/16 Pct Recovery = 124% Analysis Date = 11/24/16 Pct Recovery = 124% Analysis Date = 11/22/16 Pct Recovery = 124% Analysis Date = 11/22/16 Pct Recovery = 124% Analysis Date = 11/20/16 Pct Recovery = 123% Analysis Date = 11/20/16 Pct Recovery = 123% Analysis Date = 11/18/16 Pct Recovery = 122% Analysis Date = 11/18/16 Pct Recovery = 122% Analysis Date = 11/16/16 Pct Recovery = 122% Analysis Date = 11/16/16 Pct Recovery = 122% Analysis Date = 11/14/16 Pct Recovery = 121% Analysis Date = 11/14/16 Pct Recovery = 121% Analysis Date = 11/12/16 Pct Recovery = 120% Analysis Date = 11/12/16 Pct Recovery = 120% Analysis Date = 11/10/16 Pct Recovery = 120% Analysis Date = 11/10/16 Pct Recovery = 120% Analysis Date = 11/08/16 Pct Recovery = 119% Analysis Date = 11/08/16 Pct Recovery = 119% Analysis Date = 11/05/16 Pct Recovery = 119% Analysis Date = 11/05/16 Pct Recovery = 119% Analysis Date = 11/03/16 Pct Recovery = 118% Analysis Date = 11/03/16 Pct Recovery = 118% Analysis Date = 11/01/16 Pct Recovery = 117% Analysis Date = 11/01/16 Pct Recovery = 117% Analysis Date = 10/30/16 Pct Recovery = 117% Analysis Date = 10/30/16 Pct Recovery = 117% Analysis Date = 10/28/16 Pct Recovery = 116% Analysis Date = 10/28/16 Pct Recovery = 116% Analysis Date = 10/26/16 Pct Recovery = 116% Analysis Date = 10/26/16 Pct Recovery = 116% Analysis Date = 10/24/16 Pct Recovery = 115% Analysis Date = 10/24/16 Pct Recovery = 115% Analysis Date = 10/22/16 Pct Recovery = 114% Analysis Date = 10/22/16 Pct Recovery = 114% Analysis Date = 10/20/16 Pct Recovery = 114% Analysis Date = 10/20/16 Pct Recovery = 114% Analysis Date = 10/18/16 Pct Recovery = 113% Analysis Date = 10/18/16 Pct Recovery = 113% Analysis Date = 10/16/16 Pct Recovery = 113% Analysis Date = 10/16/16 Pct Recovery = 113% Analysis Date = 10/14/16 Pct Recovery = 112% Analysis Date = 10/14/16 Pct Recovery = 112% Analysis Date = 10/12/16 Pct Recovery = 112% Analysis Date = 10/12/16 Pct Recovery = 112% Analysis Date = 10/09/16 Pct Recovery = 111% Analysis Date = 10/09/16 Pct Recovery = 111% Analysis Date = 10/07/16 Pct Recovery = 110% Analysis Date = 10/07/16 Pct Recovery = 110% Analysis Date = 10/05/16 Pct Recovery = 110% Analysis Date = 10/05/16 Pct Recovery = 110% Analysis Date = 10/03/16 Pct Recovery = 109% Analysis Date = 10/03/16 Pct Recovery = 109% Analysis Date = 10/01/16 Pct Recovery = 109% Analysis Date = 10/01/16 Pct Recovery = 109% Analysis Date = 09/29/16 Pct Recovery = 108% Analysis Date = 09/29/16 Pct Recovery = 108% Analysis Date = 09/27/16 Pct Recovery = 107% Analysis Date = 09/27/16 Pct Recovery = 107% Analysis Date = 09/25/16 Pct Recovery = 107% Analysis Date = 09/25/16 Pct Recovery = 107% Analysis Date = 09/23/16 Pct Recovery = 106% Analysis Date = 09/23/16 Pct Recovery = 106% Analysis Date = 09/21/16 Pct Recovery = 106% Analysis Date = 09/21/16 Pct Recovery = 106% Analysis Date = 09/19/16 Pct Recovery = 105% Analysis Date = 09/19/16 Pct Recovery = 105% Analysis Date = 09/17/16 Pct Recovery = 105% Analysis Date = 09/17/16 Pct Recovery = 105% Analysis Date = 09/14/16 Pct Recovery = 104% Analysis Date = 09/14/16 Pct Recovery = 104% Analysis Date = 09/12/16 Pct Recovery = 103% Analysis Date = 09/12/16 Pct Recovery = 103% Analysis Date = 09/10/16 Pct Recovery = 103% Analysis Date = 09/10/16 Pct Recovery = 103% Analysis Date = 09/08/16 Pct Recovery = 102% Analysis Date = 09/08/16 Pct Recovery = 102% Analysis Date = 09/06/16 Pct Recovery = 102% Analysis Date = 09/06/16 Pct Recovery = 102% Analysis Date = 09/04/16 Pct Recovery = 101% Analysis Date = 09/04/16 Pct Recovery = 101% Analysis Date = 09/02/16 Pct Recovery = 101% Analysis Date = 09/02/16 Pct Recovery = 101% Analysis Date = 08/31/16 Pct Recovery = 100% Analysis Date = 08/31/16 Pct Recovery = 100% Analysis Date = 08/29/16 Pct Recovery = 100% Analysis Date = 08/29/16 Pct Recovery = 100% Analysis Date = 08/27/16 Pct Recovery = 99% Analysis Date = 08/27/16 Pct Recovery = 99% Analysis Date = 08/25/16 Pct Recovery = 98% Analysis Date = 08/25/16 Pct Recovery = 98% Analysis Date = 08/23/16 Pct Recovery = 98% Analysis Date = 08/23/16 Pct Recovery = 98% Analysis Date = 08/21/16 Pct Recovery = 97% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TERBUFOS OXON SULFOXIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 87% 8% 87% 9%
>= Reporting Level 30 111% 38% 106% 35%
Total 32 109% 37% 103% 32%

Sample Statistics
TERBUFOS OXON SULFOXIDE

Characteristic N % % Basis
Plotted 32 100% Spiked
Estimated Values 2 6% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 32 .  
False Negatives 0 0% 0 out of 32
Not Spiked 87 .  
False Positives 0 0% 0 out of 85