OBSP Determination:
ISOXAFLUTOLE ACID METABOLITE RPA 203328
METHOD: 2437 , TESTIDCODE: 68633LCM60

Analysis Date = 09/24/17 SpikeMix = Abs 071917Pest3: 80 µl & Abs 072417Pest3: 80 µl Pct Recovery = 118% Analysis Date = 02/01/17 SpikeMix = Spex Organics TS160603008: 100 µl & Spex Organics TS160511023: 100 µl Pct Recovery = 117% Analysis Date = 02/01/17 SpikeMix = Spex Organics TS160603008: 100 µl & Spex Organics TS160511023: 100 µl Pct Recovery = 127% Analysis Date = 03/08/17 SpikeMix = Abs 072516: 100 µl & Abs 071216: 100 µl Pct Recovery = 122% Analysis Date = 03/08/17 SpikeMix = Abs 072516: 100 µl & Abs 071216: 100 µl Pct Recovery = 128% Analysis Date = 02/16/17 SpikeMix = Abs 071216: 100 µl & ChemService 5154100: 100 µl Pct Recovery = 135% Analysis Date = 02/16/17 SpikeMix = Abs 071216: 100 µl & ChemService 5154100: 100 µl Pct Recovery = 145% Analysis Date = 08/25/16 SpikeMix = Abs 072516: 100 µl & Abs 071216: 100 µl Pct Recovery = 144% Analysis Date = 08/25/16 SpikeMix = Abs 072516: 100 µl & Abs 071216: 100 µl Pct Recovery = 131% Analysis Date = 09/13/17 SpikeMix = Abs 071917Pest3: 50 µl & Abs 072417Pest3: 50 µl Pct Recovery = 108% Analysis Date = 09/06/17 SpikeMix = Abs 072417Pest3: 50 µl & Abs 071917Pest3: 50 µl Pct Recovery = 112% Analysis Date = 08/24/17 SpikeMix = Abs 071717Pest3: 50 µl & Abs 072417Pest3: 50 µl Pct Recovery = 104% Analysis Date = 07/18/17 SpikeMix = Spex Organics TS160511023: 80 µl & Abs 072516: 80 µl Pct Recovery = 114% Analysis Date = 01/17/17 SpikeMix = Spex Organics TS160511023: 80 µl & Abs 071816: 80 µl Pct Recovery = 131% Analysis Date = 01/17/17 SpikeMix = Spex Organics TS160511023: 80 µl & Abs 071816: 80 µl Pct Recovery = 115% Analysis Date = 09/13/16 SpikeMix = Abs 072516: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 140% Analysis Date = 09/13/16 SpikeMix = Abs 072516: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 113% Analysis Date = 07/20/16 SpikeMix = Spex Organics TS160603008: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 107% Analysis Date = 07/20/16 SpikeMix = Spex Organics TS160603008: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 104% Analysis Date = 07/11/17 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 105% Analysis Date = 06/21/17 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 141% Analysis Date = 04/18/17 SpikeMix = Abs 071216: 80 µl & ChemService 5154100: 80 µl Pct Recovery = 119% Analysis Date = 12/13/16 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 128% Analysis Date = 12/13/16 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 140% Analysis Date = 11/22/16 SpikeMix = Spex Organics TS160603008: 80 µl & Abs 071216: 80 µl Pct Recovery = 111% Analysis Date = 11/22/16 SpikeMix = Spex Organics TS160603008: 80 µl & Abs 071216: 80 µl Pct Recovery = 118% Analysis Date = 05/05/16 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 120% Analysis Date = 05/05/16 SpikeMix = ERA 0406-15-05: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 111% Analysis Date = 03/16/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 90% Analysis Date = 03/16/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 98% Analysis Date = 03/16/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 89% Analysis Date = 03/09/16 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 94% Analysis Date = 03/09/16 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 84% Analysis Date = 03/09/16 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 100% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 119% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 96% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 97% Analysis Date = 07/26/17 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 117% Analysis Date = 06/27/17 SpikeMix = Spex Organics TS160511023: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 117% Analysis Date = 06/02/17 SpikeMix = Spex Organics TS160511023: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 104% Analysis Date = 05/17/17 SpikeMix = Spex Organics TS160511023: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 113% Analysis Date = 01/05/17 SpikeMix = Abs 072516: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 109% Analysis Date = 01/04/17 SpikeMix = Abs 072516: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 122% Analysis Date = 11/09/16 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 182% Analysis Date = 11/09/16 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 171% Analysis Date = 08/12/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 151% Analysis Date = 08/12/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 120% Analysis Date = 08/09/16 SpikeMix = Spex Organics TS160603008: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 118% Analysis Date = 08/09/16 SpikeMix = Spex Organics TS160603008: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 124% Analysis Date = 08/05/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 151% Analysis Date = 08/05/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 127% Analysis Date = 07/08/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 128% Analysis Date = 07/08/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 129% Analysis Date = 07/06/17 SpikeMix = Abs 071216: 40 µl & Abs 072516: 40 µl Pct Recovery = 128% Analysis Date = 05/27/17 SpikeMix = Abs 071216: 40 µl & Abs 071816: 40 µl Pct Recovery = 99% Analysis Date = 11/01/16 SpikeMix = Abs 072516: 40 µl & Abs 071216: 40 µl Pct Recovery = 114% Analysis Date = 11/01/16 SpikeMix = Abs 072516: 40 µl & Abs 071216: 40 µl Pct Recovery = 85% Analysis Date = 10/07/16 SpikeMix = Spex Organics TS160603008: 40 µl & Abs 071216: 40 µl Pct Recovery = 119% Analysis Date = 10/07/16 SpikeMix = Spex Organics TS160603008: 40 µl & Abs 071216: 40 µl Pct Recovery = 137% Analysis Date = 09/21/16 SpikeMix = Abs 071216: 40 µl & ChemService 5154100: 40 µl Pct Recovery = 131% Analysis Date = 09/21/16 SpikeMix = Abs 071216: 40 µl & ChemService 5154100: 40 µl Pct Recovery = 128% Analysis Date = 08/31/16 SpikeMix = Abs 071216: 40 µl & Abs 071816: 40 µl Pct Recovery = 102% Analysis Date = 08/31/16 SpikeMix = Abs 071216: 40 µl & Abs 071816: 40 µl Pct Recovery = 117% Analysis Date = 09/22/17 SpikeMix = Abs 071717Pest3: 20 µl & Abs 072417Pest3: 20 µl Pct Recovery = 83% Analysis Date = 08/27/17 SpikeMix = Abs 071917Pest3: 20 µl & Abs 072417Pest3: 20 µl Pct Recovery = 116% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 107% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 107% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 104% Analysis Date = 02/20/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 94% Analysis Date = 02/20/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 97% Analysis Date = 02/20/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 96% Analysis Date = 02/02/16 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ChemService 3995200: 1 Pct Recovery = 87% Analysis Date = 02/02/16 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ChemService 3995200: 1 Pct Recovery = 104% Analysis Date = 02/02/16 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ChemService 3995200: 1 Pct Recovery = 113% Analysis Date = 01/27/16 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 99% Analysis Date = 01/27/16 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 97% Analysis Date = 01/27/16 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 109% Analysis Date = 10/20/16 SpikeMix = Abs 071216: 10 µl & Abs 071816: 10 µl Pct Recovery = 150% Analysis Date = 10/20/16 SpikeMix = Abs 071216: 10 µl & Abs 071816: 10 µl Pct Recovery = 115% Analysis Date = 09/23/17 Pct Recovery = 107% Analysis Date = 09/20/17 Pct Recovery = 108% Analysis Date = 09/20/17 Pct Recovery = 108% Analysis Date = 09/17/17 Pct Recovery = 108% Analysis Date = 09/17/17 Pct Recovery = 108% Analysis Date = 09/14/17 Pct Recovery = 108% Analysis Date = 09/14/17 Pct Recovery = 108% Analysis Date = 09/11/17 Pct Recovery = 108% Analysis Date = 09/11/17 Pct Recovery = 108% Analysis Date = 09/08/17 Pct Recovery = 109% Analysis Date = 09/08/17 Pct Recovery = 109% Analysis Date = 09/05/17 Pct Recovery = 109% Analysis Date = 09/05/17 Pct Recovery = 109% Analysis Date = 09/02/17 Pct Recovery = 109% Analysis Date = 09/02/17 Pct Recovery = 109% Analysis Date = 08/30/17 Pct Recovery = 109% Analysis Date = 08/30/17 Pct Recovery = 109% Analysis Date = 08/27/17 Pct Recovery = 110% Analysis Date = 08/27/17 Pct Recovery = 110% Analysis Date = 08/24/17 Pct Recovery = 110% Analysis Date = 08/24/17 Pct Recovery = 110% Analysis Date = 08/21/17 Pct Recovery = 110% Analysis Date = 08/21/17 Pct Recovery = 110% Analysis Date = 08/18/17 Pct Recovery = 110% Analysis Date = 08/18/17 Pct Recovery = 110% Analysis Date = 08/15/17 Pct Recovery = 111% Analysis Date = 08/15/17 Pct Recovery = 111% Analysis Date = 08/12/17 Pct Recovery = 111% Analysis Date = 08/12/17 Pct Recovery = 111% Analysis Date = 08/09/17 Pct Recovery = 111% Analysis Date = 08/09/17 Pct Recovery = 111% Analysis Date = 08/06/17 Pct Recovery = 111% Analysis Date = 08/06/17 Pct Recovery = 111% Analysis Date = 08/03/17 Pct Recovery = 111% Analysis Date = 08/03/17 Pct Recovery = 111% Analysis Date = 07/31/17 Pct Recovery = 112% Analysis Date = 07/31/17 Pct Recovery = 112% Analysis Date = 07/28/17 Pct Recovery = 112% Analysis Date = 07/28/17 Pct Recovery = 112% Analysis Date = 07/25/17 Pct Recovery = 112% Analysis Date = 07/25/17 Pct Recovery = 112% Analysis Date = 07/22/17 Pct Recovery = 112% Analysis Date = 07/22/17 Pct Recovery = 112% Analysis Date = 07/19/17 Pct Recovery = 113% Analysis Date = 07/19/17 Pct Recovery = 113% Analysis Date = 07/16/17 Pct Recovery = 113% Analysis Date = 07/16/17 Pct Recovery = 113% Analysis Date = 07/13/17 Pct Recovery = 113% Analysis Date = 07/13/17 Pct Recovery = 113% Analysis Date = 07/10/17 Pct Recovery = 113% Analysis Date = 07/10/17 Pct Recovery = 113% Analysis Date = 07/07/17 Pct Recovery = 114% Analysis Date = 07/07/17 Pct Recovery = 114% Analysis Date = 07/04/17 Pct Recovery = 114% Analysis Date = 07/04/17 Pct Recovery = 114% Analysis Date = 07/01/17 Pct Recovery = 114% Analysis Date = 07/01/17 Pct Recovery = 114% Analysis Date = 06/28/17 Pct Recovery = 114% Analysis Date = 06/28/17 Pct Recovery = 114% Analysis Date = 06/25/17 Pct Recovery = 115% Analysis Date = 06/25/17 Pct Recovery = 115% Analysis Date = 06/22/17 Pct Recovery = 115% Analysis Date = 06/22/17 Pct Recovery = 115% Analysis Date = 06/19/17 Pct Recovery = 115% Analysis Date = 06/19/17 Pct Recovery = 115% Analysis Date = 06/16/17 Pct Recovery = 115% Analysis Date = 06/16/17 Pct Recovery = 115% Analysis Date = 06/12/17 Pct Recovery = 115% Analysis Date = 06/12/17 Pct Recovery = 115% Analysis Date = 06/09/17 Pct Recovery = 116% Analysis Date = 06/09/17 Pct Recovery = 116% Analysis Date = 06/06/17 Pct Recovery = 116% Analysis Date = 06/06/17 Pct Recovery = 116% Analysis Date = 06/03/17 Pct Recovery = 116% Analysis Date = 06/03/17 Pct Recovery = 116% Analysis Date = 05/31/17 Pct Recovery = 116% Analysis Date = 05/31/17 Pct Recovery = 116% Analysis Date = 05/28/17 Pct Recovery = 117% Analysis Date = 05/28/17 Pct Recovery = 117% Analysis Date = 05/25/17 Pct Recovery = 117% Analysis Date = 05/25/17 Pct Recovery = 117% Analysis Date = 05/22/17 Pct Recovery = 117% Analysis Date = 05/22/17 Pct Recovery = 117% Analysis Date = 05/19/17 Pct Recovery = 117% Analysis Date = 05/19/17 Pct Recovery = 117% Analysis Date = 05/16/17 Pct Recovery = 118% Analysis Date = 05/16/17 Pct Recovery = 118% Analysis Date = 05/13/17 Pct Recovery = 118% Analysis Date = 05/13/17 Pct Recovery = 118% Analysis Date = 05/10/17 Pct Recovery = 118% Analysis Date = 05/10/17 Pct Recovery = 118% Analysis Date = 05/07/17 Pct Recovery = 118% Analysis Date = 05/07/17 Pct Recovery = 118% Analysis Date = 05/04/17 Pct Recovery = 118% Analysis Date = 05/04/17 Pct Recovery = 118% Analysis Date = 05/01/17 Pct Recovery = 119% Analysis Date = 05/01/17 Pct Recovery = 119% Analysis Date = 04/28/17 Pct Recovery = 119% Analysis Date = 04/28/17 Pct Recovery = 119% Analysis Date = 04/25/17 Pct Recovery = 119% Analysis Date = 04/25/17 Pct Recovery = 119% Analysis Date = 04/22/17 Pct Recovery = 119% Analysis Date = 04/22/17 Pct Recovery = 119% Analysis Date = 04/19/17 Pct Recovery = 119% Analysis Date = 04/19/17 Pct Recovery = 119% Analysis Date = 04/16/17 Pct Recovery = 120% Analysis Date = 04/16/17 Pct Recovery = 120% Analysis Date = 04/13/17 Pct Recovery = 120% Analysis Date = 04/13/17 Pct Recovery = 120% Analysis Date = 04/10/17 Pct Recovery = 120% Analysis Date = 04/10/17 Pct Recovery = 120% Analysis Date = 04/07/17 Pct Recovery = 120% Analysis Date = 04/07/17 Pct Recovery = 120% Analysis Date = 04/04/17 Pct Recovery = 120% Analysis Date = 04/04/17 Pct Recovery = 120% Analysis Date = 04/01/17 Pct Recovery = 121% Analysis Date = 04/01/17 Pct Recovery = 121% Analysis Date = 03/29/17 Pct Recovery = 121% Analysis Date = 03/29/17 Pct Recovery = 121% Analysis Date = 03/26/17 Pct Recovery = 121% Analysis Date = 03/26/17 Pct Recovery = 121% Analysis Date = 03/23/17 Pct Recovery = 121% Analysis Date = 03/23/17 Pct Recovery = 121% Analysis Date = 03/20/17 Pct Recovery = 122% Analysis Date = 03/20/17 Pct Recovery = 122% Analysis Date = 03/17/17 Pct Recovery = 122% Analysis Date = 03/17/17 Pct Recovery = 122% Analysis Date = 03/14/17 Pct Recovery = 122% Analysis Date = 03/14/17 Pct Recovery = 122% Analysis Date = 03/11/17 Pct Recovery = 122% Analysis Date = 03/11/17 Pct Recovery = 122% Analysis Date = 03/08/17 Pct Recovery = 122% Analysis Date = 03/08/17 Pct Recovery = 122% Analysis Date = 03/04/17 Pct Recovery = 123% Analysis Date = 03/04/17 Pct Recovery = 123% Analysis Date = 03/01/17 Pct Recovery = 123% Analysis Date = 03/01/17 Pct Recovery = 123% Analysis Date = 02/26/17 Pct Recovery = 123% Analysis Date = 02/26/17 Pct Recovery = 123% Analysis Date = 02/23/17 Pct Recovery = 123% Analysis Date = 02/23/17 Pct Recovery = 123% Analysis Date = 02/20/17 Pct Recovery = 123% Analysis Date = 02/20/17 Pct Recovery = 123% Analysis Date = 02/17/17 Pct Recovery = 124% Analysis Date = 02/17/17 Pct Recovery = 124% Analysis Date = 02/14/17 Pct Recovery = 124% Analysis Date = 02/14/17 Pct Recovery = 124% Analysis Date = 02/11/17 Pct Recovery = 124% Analysis Date = 02/11/17 Pct Recovery = 124% Analysis Date = 02/08/17 Pct Recovery = 124% Analysis Date = 02/08/17 Pct Recovery = 124% Analysis Date = 02/05/17 Pct Recovery = 124% Analysis Date = 02/05/17 Pct Recovery = 124% Analysis Date = 02/02/17 Pct Recovery = 125% Analysis Date = 02/02/17 Pct Recovery = 125% Analysis Date = 01/30/17 Pct Recovery = 125% Analysis Date = 01/30/17 Pct Recovery = 125% Analysis Date = 01/27/17 Pct Recovery = 125% Analysis Date = 01/27/17 Pct Recovery = 125% Analysis Date = 01/24/17 Pct Recovery = 125% Analysis Date = 01/24/17 Pct Recovery = 125% Analysis Date = 01/21/17 Pct Recovery = 125% Analysis Date = 01/21/17 Pct Recovery = 125% Analysis Date = 01/18/17 Pct Recovery = 126% Analysis Date = 01/18/17 Pct Recovery = 126% Analysis Date = 01/15/17 Pct Recovery = 126% Analysis Date = 01/15/17 Pct Recovery = 126% Analysis Date = 01/12/17 Pct Recovery = 126% Analysis Date = 01/12/17 Pct Recovery = 126% Analysis Date = 01/09/17 Pct Recovery = 126% Analysis Date = 01/09/17 Pct Recovery = 126% Analysis Date = 01/06/17 Pct Recovery = 126% Analysis Date = 01/06/17 Pct Recovery = 126% Analysis Date = 01/03/17 Pct Recovery = 127% Analysis Date = 01/03/17 Pct Recovery = 127% Analysis Date = 12/31/16 Pct Recovery = 127% Analysis Date = 12/31/16 Pct Recovery = 127% Analysis Date = 12/28/16 Pct Recovery = 127% Analysis Date = 12/28/16 Pct Recovery = 127% Analysis Date = 12/25/16 Pct Recovery = 127% Analysis Date = 12/25/16 Pct Recovery = 127% Analysis Date = 12/22/16 Pct Recovery = 127% Analysis Date = 12/22/16 Pct Recovery = 127% Analysis Date = 12/19/16 Pct Recovery = 127% Analysis Date = 12/19/16 Pct Recovery = 127% Analysis Date = 12/16/16 Pct Recovery = 127% Analysis Date = 12/16/16 Pct Recovery = 127% Analysis Date = 12/13/16 Pct Recovery = 127% Analysis Date = 12/13/16 Pct Recovery = 127% Analysis Date = 12/10/16 Pct Recovery = 127% Analysis Date = 12/10/16 Pct Recovery = 127% Analysis Date = 12/07/16 Pct Recovery = 127% Analysis Date = 12/07/16 Pct Recovery = 127% Analysis Date = 12/04/16 Pct Recovery = 127% Analysis Date = 12/04/16 Pct Recovery = 127% Analysis Date = 12/01/16 Pct Recovery = 127% Analysis Date = 12/01/16 Pct Recovery = 127% Analysis Date = 11/28/16 Pct Recovery = 127% Analysis Date = 11/28/16 Pct Recovery = 127% Analysis Date = 11/24/16 Pct Recovery = 127% Analysis Date = 11/24/16 Pct Recovery = 127% Analysis Date = 11/21/16 Pct Recovery = 127% Analysis Date = 11/21/16 Pct Recovery = 127% Analysis Date = 11/18/16 Pct Recovery = 127% Analysis Date = 11/18/16 Pct Recovery = 127% Analysis Date = 11/15/16 Pct Recovery = 127% Analysis Date = 11/15/16 Pct Recovery = 127% Analysis Date = 11/12/16 Pct Recovery = 127% Analysis Date = 11/12/16 Pct Recovery = 127% Analysis Date = 11/09/16 Pct Recovery = 127% Analysis Date = 11/09/16 Pct Recovery = 127% Analysis Date = 11/06/16 Pct Recovery = 127% Analysis Date = 11/06/16 Pct Recovery = 127% Analysis Date = 11/03/16 Pct Recovery = 127% Analysis Date = 11/03/16 Pct Recovery = 127% Analysis Date = 10/31/16 Pct Recovery = 127% Analysis Date = 10/31/16 Pct Recovery = 127% Analysis Date = 10/28/16 Pct Recovery = 127% Analysis Date = 10/28/16 Pct Recovery = 127% Analysis Date = 10/25/16 Pct Recovery = 127% Analysis Date = 10/25/16 Pct Recovery = 127% Analysis Date = 10/22/16 Pct Recovery = 127% Analysis Date = 10/22/16 Pct Recovery = 127% Analysis Date = 10/19/16 Pct Recovery = 127% Analysis Date = 10/19/16 Pct Recovery = 127% Analysis Date = 10/16/16 Pct Recovery = 127% Analysis Date = 10/16/16 Pct Recovery = 127% Analysis Date = 10/13/16 Pct Recovery = 127% Analysis Date = 10/13/16 Pct Recovery = 127% Analysis Date = 10/10/16 Pct Recovery = 127% Analysis Date = 10/10/16 Pct Recovery = 127% Analysis Date = 10/07/16 Pct Recovery = 127% Analysis Date = 10/07/16 Pct Recovery = 127% Analysis Date = 10/04/16 Pct Recovery = 127% Analysis Date = 10/04/16 Pct Recovery = 127% Analysis Date = 10/01/16 Pct Recovery = 127% Analysis Date = 10/01/16 Pct Recovery = 127% Analysis Date = 09/28/16 Pct Recovery = 127% Analysis Date = 09/28/16 Pct Recovery = 127% Analysis Date = 09/25/16 Pct Recovery = 127% Analysis Date = 09/25/16 Pct Recovery = 127% Analysis Date = 09/22/16 Pct Recovery = 127% Analysis Date = 09/22/16 Pct Recovery = 127% Analysis Date = 09/19/16 Pct Recovery = 127% Analysis Date = 09/19/16 Pct Recovery = 127% Analysis Date = 09/16/16 Pct Recovery = 127% Analysis Date = 09/16/16 Pct Recovery = 127% Analysis Date = 09/13/16 Pct Recovery = 127% Analysis Date = 09/13/16 Pct Recovery = 127% Analysis Date = 09/10/16 Pct Recovery = 126% Analysis Date = 09/10/16 Pct Recovery = 126% Analysis Date = 09/07/16 Pct Recovery = 126% Analysis Date = 09/07/16 Pct Recovery = 126% Analysis Date = 09/04/16 Pct Recovery = 126% Analysis Date = 09/04/16 Pct Recovery = 126% Analysis Date = 09/01/16 Pct Recovery = 126% Analysis Date = 09/01/16 Pct Recovery = 126% Analysis Date = 08/29/16 Pct Recovery = 126% Analysis Date = 08/29/16 Pct Recovery = 126% Analysis Date = 08/26/16 Pct Recovery = 126% Analysis Date = 08/26/16 Pct Recovery = 126% Analysis Date = 08/23/16 Pct Recovery = 126% Analysis Date = 08/23/16 Pct Recovery = 126% Analysis Date = 08/20/16 Pct Recovery = 125% Analysis Date = 08/20/16 Pct Recovery = 125% Analysis Date = 08/17/16 Pct Recovery = 125% Analysis Date = 08/17/16 Pct Recovery = 125% Analysis Date = 08/13/16 Pct Recovery = 125% Analysis Date = 08/13/16 Pct Recovery = 125% Analysis Date = 08/10/16 Pct Recovery = 125% Analysis Date = 08/10/16 Pct Recovery = 125% Analysis Date = 08/07/16 Pct Recovery = 124% Analysis Date = 08/07/16 Pct Recovery = 124% Analysis Date = 08/04/16 Pct Recovery = 124% Analysis Date = 08/04/16 Pct Recovery = 124% Analysis Date = 08/01/16 Pct Recovery = 123% Analysis Date = 08/01/16 Pct Recovery = 123% Analysis Date = 07/29/16 Pct Recovery = 123% Analysis Date = 07/29/16 Pct Recovery = 123% Analysis Date = 07/26/16 Pct Recovery = 122% Analysis Date = 07/26/16 Pct Recovery = 122% Analysis Date = 07/23/16 Pct Recovery = 122% Analysis Date = 07/23/16 Pct Recovery = 122% Analysis Date = 07/20/16 Pct Recovery = 122% Analysis Date = 07/20/16 Pct Recovery = 122% Analysis Date = 07/17/16 Pct Recovery = 121% Analysis Date = 07/17/16 Pct Recovery = 121% Analysis Date = 07/14/16 Pct Recovery = 121% Analysis Date = 07/14/16 Pct Recovery = 121% Analysis Date = 07/11/16 Pct Recovery = 120% Analysis Date = 07/11/16 Pct Recovery = 120% Analysis Date = 07/08/16 Pct Recovery = 120% Analysis Date = 07/08/16 Pct Recovery = 120% Analysis Date = 07/05/16 Pct Recovery = 119% Analysis Date = 07/05/16 Pct Recovery = 119% Analysis Date = 07/02/16 Pct Recovery = 119% Analysis Date = 07/02/16 Pct Recovery = 119% Analysis Date = 06/29/16 Pct Recovery = 118% Analysis Date = 06/29/16 Pct Recovery = 118% Analysis Date = 06/26/16 Pct Recovery = 118% Analysis Date = 06/26/16 Pct Recovery = 118% Analysis Date = 06/23/16 Pct Recovery = 118% Analysis Date = 06/23/16 Pct Recovery = 118% Analysis Date = 06/20/16 Pct Recovery = 117% Analysis Date = 06/20/16 Pct Recovery = 117% Analysis Date = 06/17/16 Pct Recovery = 117% Analysis Date = 06/17/16 Pct Recovery = 117% Analysis Date = 06/14/16 Pct Recovery = 116% Analysis Date = 06/14/16 Pct Recovery = 116% Analysis Date = 06/11/16 Pct Recovery = 116% Analysis Date = 06/11/16 Pct Recovery = 116% Analysis Date = 06/08/16 Pct Recovery = 115% Analysis Date = 06/08/16 Pct Recovery = 115% Analysis Date = 06/05/16 Pct Recovery = 115% Analysis Date = 06/05/16 Pct Recovery = 115% Analysis Date = 06/02/16 Pct Recovery = 115% Analysis Date = 06/02/16 Pct Recovery = 115% Analysis Date = 05/30/16 Pct Recovery = 114% Analysis Date = 05/30/16 Pct Recovery = 114% Analysis Date = 05/27/16 Pct Recovery = 114% Analysis Date = 05/27/16 Pct Recovery = 114% Analysis Date = 05/24/16 Pct Recovery = 113% Analysis Date = 05/24/16 Pct Recovery = 113% Analysis Date = 05/21/16 Pct Recovery = 113% Analysis Date = 05/21/16 Pct Recovery = 113% Analysis Date = 05/18/16 Pct Recovery = 112% Analysis Date = 05/18/16 Pct Recovery = 112% Analysis Date = 05/15/16 Pct Recovery = 112% Analysis Date = 05/15/16 Pct Recovery = 112% Analysis Date = 05/12/16 Pct Recovery = 112% Analysis Date = 05/12/16 Pct Recovery = 112% Analysis Date = 05/09/16 Pct Recovery = 111% Analysis Date = 05/09/16 Pct Recovery = 111% Analysis Date = 05/05/16 Pct Recovery = 111% Analysis Date = 05/05/16 Pct Recovery = 111% Analysis Date = 05/02/16 Pct Recovery = 110% Analysis Date = 05/02/16 Pct Recovery = 110% Analysis Date = 04/29/16 Pct Recovery = 110% Analysis Date = 04/29/16 Pct Recovery = 110% Analysis Date = 04/26/16 Pct Recovery = 109% Analysis Date = 04/26/16 Pct Recovery = 109% Analysis Date = 04/23/16 Pct Recovery = 109% Analysis Date = 04/23/16 Pct Recovery = 109% Analysis Date = 04/20/16 Pct Recovery = 109% Analysis Date = 04/20/16 Pct Recovery = 109% Analysis Date = 04/17/16 Pct Recovery = 108% Analysis Date = 04/17/16 Pct Recovery = 108% Analysis Date = 04/14/16 Pct Recovery = 108% Analysis Date = 04/14/16 Pct Recovery = 108% Analysis Date = 04/11/16 Pct Recovery = 107% Analysis Date = 04/11/16 Pct Recovery = 107% Analysis Date = 04/08/16 Pct Recovery = 107% Analysis Date = 04/08/16 Pct Recovery = 107% Analysis Date = 04/05/16 Pct Recovery = 106% Analysis Date = 04/05/16 Pct Recovery = 106% Analysis Date = 04/02/16 Pct Recovery = 106% Analysis Date = 04/02/16 Pct Recovery = 106% Analysis Date = 03/30/16 Pct Recovery = 106% Analysis Date = 03/30/16 Pct Recovery = 106% Analysis Date = 03/27/16 Pct Recovery = 105% Analysis Date = 03/27/16 Pct Recovery = 105% Analysis Date = 03/24/16 Pct Recovery = 105% Analysis Date = 03/24/16 Pct Recovery = 105% Analysis Date = 03/21/16 Pct Recovery = 104% Analysis Date = 03/21/16 Pct Recovery = 104% Analysis Date = 03/18/16 Pct Recovery = 104% Analysis Date = 03/18/16 Pct Recovery = 104% Analysis Date = 03/15/16 Pct Recovery = 103% Analysis Date = 03/15/16 Pct Recovery = 103% Analysis Date = 03/12/16 Pct Recovery = 103% Analysis Date = 03/12/16 Pct Recovery = 103% Analysis Date = 03/09/16 Pct Recovery = 103% Analysis Date = 03/09/16 Pct Recovery = 103% Analysis Date = 03/06/16 Pct Recovery = 102% Analysis Date = 03/06/16 Pct Recovery = 102% Analysis Date = 03/03/16 Pct Recovery = 102% Analysis Date = 03/03/16 Pct Recovery = 102% Analysis Date = 02/29/16 Pct Recovery = 101% Analysis Date = 02/29/16 Pct Recovery = 101% Analysis Date = 02/26/16 Pct Recovery = 101% Analysis Date = 02/26/16 Pct Recovery = 101% Analysis Date = 02/23/16 Pct Recovery = 100% Analysis Date = 02/23/16 Pct Recovery = 100% Analysis Date = 02/20/16 Pct Recovery = 100% Analysis Date = 02/20/16 Pct Recovery = 100% Analysis Date = 02/17/16 Pct Recovery = 100% Analysis Date = 02/17/16 Pct Recovery = 100% Analysis Date = 02/14/16 Pct Recovery = 99% Analysis Date = 02/14/16 Pct Recovery = 99% Analysis Date = 02/11/16 Pct Recovery = 99% Analysis Date = 02/11/16 Pct Recovery = 99% Analysis Date = 02/08/16 Pct Recovery = 98% Analysis Date = 02/08/16 Pct Recovery = 98% Analysis Date = 02/05/16 Pct Recovery = 98% Analysis Date = 02/05/16 Pct Recovery = 98% Analysis Date = 02/02/16 Pct Recovery = 98% Analysis Date = 02/02/16 Pct Recovery = 98% Analysis Date = 01/30/16 Pct Recovery = 97% Analysis Date = 01/30/16 Pct Recovery = 97% Analysis Date = 01/27/16 Pct Recovery = 97% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ISOXAFLUTOLE ACID METABOLITE RPA 203328

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 133% 25% 133% 26%
>= Reporting Level 77 116% 19% 115% 18%
Total 79 116% 19% 115% 18%

Sample Statistics
ISOXAFLUTOLE ACID METABOLITE RPA 203328

Characteristic N % % Basis
Plotted 79 100% Spiked
Estimated Values 9 11% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 79 .  
False Negatives 0 0% 0 out of 79
Not Spiked 40 .  
False Positives 0 0% 0 out of 40