OBSP Determination:
FIPRONIL AMIDE
METHOD: 2437 , TESTIDCODE: 68604LCM60

Analysis Date = 06/27/17 SpikeMix = Spex Organics TS160511023: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 285% Analysis Date = 06/02/17 SpikeMix = Spex Organics TS160511023: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 220% Analysis Date = 05/17/17 SpikeMix = Spex Organics TS160511023: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 290% Analysis Date = 09/24/17 SpikeMix = Abs 071917Pest3: 80 µl & Abs 072417Pest3: 80 µl Pct Recovery = 91% Analysis Date = 02/01/17 SpikeMix = Spex Organics TS160603008: 100 µl & Spex Organics TS160511023: 100 µl Pct Recovery = 96% Analysis Date = 02/01/17 SpikeMix = Spex Organics TS160603008: 100 µl & Spex Organics TS160511023: 100 µl Pct Recovery = 95% Analysis Date = 01/28/17 SpikeMix = ChemService 5154100: 100 µl & Spex Organics TS160603008: 100 µl Pct Recovery = 91% Analysis Date = 01/28/17 SpikeMix = ChemService 5154100: 100 µl & Spex Organics TS160603008: 100 µl Pct Recovery = 106% Analysis Date = 10/04/17 SpikeMix = Abs 071917Pest3: 50 µl & Abs 071717Pest3: 50 µl Pct Recovery = 125% Analysis Date = 09/13/17 SpikeMix = Abs 071917Pest3: 50 µl & Abs 072417Pest3: 50 µl Pct Recovery = 74% Analysis Date = 09/06/17 SpikeMix = Abs 072417Pest3: 50 µl & Abs 071917Pest3: 50 µl Pct Recovery = 134% Analysis Date = 11/22/16 SpikeMix = Spex Organics TS160603008: 80 µl & Abs 071216: 80 µl Pct Recovery = 105% Analysis Date = 11/22/16 SpikeMix = Spex Organics TS160603008: 80 µl & Abs 071216: 80 µl Pct Recovery = 95% Analysis Date = 07/22/16 SpikeMix = ChemService 5154100: 80 µl & ChemService 5154200: 80 µl & Spex Organics TS160603 Pct Recovery = 149% Analysis Date = 07/22/16 SpikeMix = ChemService 5154100: 80 µl & ChemService 5154200: 80 µl & Spex Organics TS160603 Pct Recovery = 132% Analysis Date = 07/20/16 SpikeMix = Spex Organics TS160603008: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 97% Analysis Date = 07/20/16 SpikeMix = Spex Organics TS160603008: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 87% Analysis Date = 12/13/16 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 111% Analysis Date = 12/13/16 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 81% Analysis Date = 10/07/16 SpikeMix = Spex Organics TS160603008: 40 µl & Abs 071216: 40 µl Pct Recovery = 79% Analysis Date = 10/07/16 SpikeMix = Spex Organics TS160603008: 40 µl & Abs 071216: 40 µl Pct Recovery = 82% Analysis Date = 09/07/16 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 100% Analysis Date = 09/07/16 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 83% Analysis Date = 08/09/16 SpikeMix = Spex Organics TS160603008: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 71% Analysis Date = 08/09/16 SpikeMix = Spex Organics TS160603008: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 83% Analysis Date = 08/05/16 SpikeMix = ChemService 5154100: 40 µl & ChemService 5154200: 40 µl & Spex Organics TS160603 Pct Recovery = 72% Analysis Date = 08/05/16 SpikeMix = ChemService 5154100: 40 µl & ChemService 5154200: 40 µl & Spex Organics TS160603 Pct Recovery = 68% Analysis Date = 10/11/17 SpikeMix = Abs 071917Pest3: 20 µl & Abs 071717Pest3: 20 µl Pct Recovery = 107% Analysis Date = 08/27/17 SpikeMix = Abs 071917Pest3: 20 µl & Abs 072417Pest3: 20 µl Pct Recovery = 121% Analysis Date = 08/08/17 SpikeMix = Abs 071917Pest3: 20 µl & Abs 071717Pest3: 20 µl Pct Recovery = 83% Analysis Date = 10/11/17 Pct Recovery = 110% Analysis Date = 10/08/17 Pct Recovery = 111% Analysis Date = 10/08/17 Pct Recovery = 111% Analysis Date = 10/06/17 Pct Recovery = 112% Analysis Date = 10/06/17 Pct Recovery = 112% Analysis Date = 10/04/17 Pct Recovery = 114% Analysis Date = 10/04/17 Pct Recovery = 114% Analysis Date = 10/02/17 Pct Recovery = 115% Analysis Date = 10/02/17 Pct Recovery = 115% Analysis Date = 09/29/17 Pct Recovery = 116% Analysis Date = 09/29/17 Pct Recovery = 116% Analysis Date = 09/27/17 Pct Recovery = 118% Analysis Date = 09/27/17 Pct Recovery = 118% Analysis Date = 09/25/17 Pct Recovery = 119% Analysis Date = 09/25/17 Pct Recovery = 119% Analysis Date = 09/23/17 Pct Recovery = 120% Analysis Date = 09/23/17 Pct Recovery = 120% Analysis Date = 09/20/17 Pct Recovery = 121% Analysis Date = 09/20/17 Pct Recovery = 121% Analysis Date = 09/18/17 Pct Recovery = 123% Analysis Date = 09/18/17 Pct Recovery = 123% Analysis Date = 09/16/17 Pct Recovery = 124% Analysis Date = 09/16/17 Pct Recovery = 124% Analysis Date = 09/14/17 Pct Recovery = 125% Analysis Date = 09/14/17 Pct Recovery = 125% Analysis Date = 09/11/17 Pct Recovery = 127% Analysis Date = 09/11/17 Pct Recovery = 127% Analysis Date = 09/09/17 Pct Recovery = 128% Analysis Date = 09/09/17 Pct Recovery = 128% Analysis Date = 09/07/17 Pct Recovery = 129% Analysis Date = 09/07/17 Pct Recovery = 129% Analysis Date = 09/05/17 Pct Recovery = 130% Analysis Date = 09/05/17 Pct Recovery = 130% Analysis Date = 09/02/17 Pct Recovery = 131% Analysis Date = 09/02/17 Pct Recovery = 131% Analysis Date = 08/31/17 Pct Recovery = 132% Analysis Date = 08/31/17 Pct Recovery = 132% Analysis Date = 08/29/17 Pct Recovery = 134% Analysis Date = 08/29/17 Pct Recovery = 134% Analysis Date = 08/27/17 Pct Recovery = 135% Analysis Date = 08/27/17 Pct Recovery = 135% Analysis Date = 08/24/17 Pct Recovery = 135% Analysis Date = 08/24/17 Pct Recovery = 135% Analysis Date = 08/22/17 Pct Recovery = 136% Analysis Date = 08/22/17 Pct Recovery = 136% Analysis Date = 08/20/17 Pct Recovery = 137% Analysis Date = 08/20/17 Pct Recovery = 137% Analysis Date = 08/18/17 Pct Recovery = 138% Analysis Date = 08/18/17 Pct Recovery = 138% Analysis Date = 08/16/17 Pct Recovery = 138% Analysis Date = 08/16/17 Pct Recovery = 138% Analysis Date = 08/13/17 Pct Recovery = 139% Analysis Date = 08/13/17 Pct Recovery = 139% Analysis Date = 08/11/17 Pct Recovery = 140% Analysis Date = 08/11/17 Pct Recovery = 140% Analysis Date = 08/09/17 Pct Recovery = 141% Analysis Date = 08/09/17 Pct Recovery = 141% Analysis Date = 08/07/17 Pct Recovery = 141% Analysis Date = 08/07/17 Pct Recovery = 141% Analysis Date = 08/04/17 Pct Recovery = 142% Analysis Date = 08/04/17 Pct Recovery = 142% Analysis Date = 08/02/17 Pct Recovery = 143% Analysis Date = 08/02/17 Pct Recovery = 143% Analysis Date = 07/31/17 Pct Recovery = 144% Analysis Date = 07/31/17 Pct Recovery = 144% Analysis Date = 07/29/17 Pct Recovery = 144% Analysis Date = 07/29/17 Pct Recovery = 144% Analysis Date = 07/26/17 Pct Recovery = 145% Analysis Date = 07/26/17 Pct Recovery = 145% Analysis Date = 07/24/17 Pct Recovery = 146% Analysis Date = 07/24/17 Pct Recovery = 146% Analysis Date = 07/22/17 Pct Recovery = 147% Analysis Date = 07/22/17 Pct Recovery = 147% Analysis Date = 07/20/17 Pct Recovery = 147% Analysis Date = 07/20/17 Pct Recovery = 147% Analysis Date = 07/17/17 Pct Recovery = 148% Analysis Date = 07/17/17 Pct Recovery = 148% Analysis Date = 07/15/17 Pct Recovery = 149% Analysis Date = 07/15/17 Pct Recovery = 149% Analysis Date = 07/13/17 Pct Recovery = 150% Analysis Date = 07/13/17 Pct Recovery = 150% Analysis Date = 07/11/17 Pct Recovery = 150% Analysis Date = 07/11/17 Pct Recovery = 150% Analysis Date = 07/08/17 Pct Recovery = 151% Analysis Date = 07/08/17 Pct Recovery = 151% Analysis Date = 07/06/17 Pct Recovery = 152% Analysis Date = 07/06/17 Pct Recovery = 152% Analysis Date = 07/04/17 Pct Recovery = 153% Analysis Date = 07/04/17 Pct Recovery = 153% Analysis Date = 07/02/17 Pct Recovery = 153% Analysis Date = 07/02/17 Pct Recovery = 153% Analysis Date = 06/29/17 Pct Recovery = 154% Analysis Date = 06/29/17 Pct Recovery = 154% Analysis Date = 06/27/17 Pct Recovery = 155% Analysis Date = 06/27/17 Pct Recovery = 155% Analysis Date = 06/25/17 Pct Recovery = 156% Analysis Date = 06/25/17 Pct Recovery = 156% Analysis Date = 06/23/17 Pct Recovery = 156% Analysis Date = 06/23/17 Pct Recovery = 156% Analysis Date = 06/21/17 Pct Recovery = 157% Analysis Date = 06/21/17 Pct Recovery = 157% Analysis Date = 06/18/17 Pct Recovery = 157% Analysis Date = 06/18/17 Pct Recovery = 157% Analysis Date = 06/16/17 Pct Recovery = 158% Analysis Date = 06/16/17 Pct Recovery = 158% Analysis Date = 06/14/17 Pct Recovery = 158% Analysis Date = 06/14/17 Pct Recovery = 158% Analysis Date = 06/12/17 Pct Recovery = 159% Analysis Date = 06/12/17 Pct Recovery = 159% Analysis Date = 06/09/17 Pct Recovery = 160% Analysis Date = 06/09/17 Pct Recovery = 160% Analysis Date = 06/07/17 Pct Recovery = 160% Analysis Date = 06/07/17 Pct Recovery = 160% Analysis Date = 06/05/17 Pct Recovery = 161% Analysis Date = 06/05/17 Pct Recovery = 161% Analysis Date = 06/03/17 Pct Recovery = 161% Analysis Date = 06/03/17 Pct Recovery = 161% Analysis Date = 05/31/17 Pct Recovery = 162% Analysis Date = 05/31/17 Pct Recovery = 162% Analysis Date = 05/29/17 Pct Recovery = 163% Analysis Date = 05/29/17 Pct Recovery = 163% Analysis Date = 05/27/17 Pct Recovery = 163% Analysis Date = 05/27/17 Pct Recovery = 163% Analysis Date = 05/25/17 Pct Recovery = 164% Analysis Date = 05/25/17 Pct Recovery = 164% Analysis Date = 05/22/17 Pct Recovery = 164% Analysis Date = 05/22/17 Pct Recovery = 164% Analysis Date = 05/20/17 Pct Recovery = 165% Analysis Date = 05/20/17 Pct Recovery = 165% Analysis Date = 05/18/17 Pct Recovery = 166% Analysis Date = 05/18/17 Pct Recovery = 166% Analysis Date = 05/16/17 Pct Recovery = 166% Analysis Date = 05/16/17 Pct Recovery = 166% Analysis Date = 05/13/17 Pct Recovery = 165% Analysis Date = 05/13/17 Pct Recovery = 165% Analysis Date = 05/11/17 Pct Recovery = 164% Analysis Date = 05/11/17 Pct Recovery = 164% Analysis Date = 05/09/17 Pct Recovery = 163% Analysis Date = 05/09/17 Pct Recovery = 163% Analysis Date = 05/07/17 Pct Recovery = 162% Analysis Date = 05/07/17 Pct Recovery = 162% Analysis Date = 05/04/17 Pct Recovery = 162% Analysis Date = 05/04/17 Pct Recovery = 162% Analysis Date = 05/02/17 Pct Recovery = 161% Analysis Date = 05/02/17 Pct Recovery = 161% Analysis Date = 04/30/17 Pct Recovery = 160% Analysis Date = 04/30/17 Pct Recovery = 160% Analysis Date = 04/28/17 Pct Recovery = 159% Analysis Date = 04/28/17 Pct Recovery = 159% Analysis Date = 04/26/17 Pct Recovery = 158% Analysis Date = 04/26/17 Pct Recovery = 158% Analysis Date = 04/23/17 Pct Recovery = 158% Analysis Date = 04/23/17 Pct Recovery = 158% Analysis Date = 04/21/17 Pct Recovery = 157% Analysis Date = 04/21/17 Pct Recovery = 157% Analysis Date = 04/19/17 Pct Recovery = 156% Analysis Date = 04/19/17 Pct Recovery = 156% Analysis Date = 04/17/17 Pct Recovery = 155% Analysis Date = 04/17/17 Pct Recovery = 155% Analysis Date = 04/14/17 Pct Recovery = 155% Analysis Date = 04/14/17 Pct Recovery = 155% Analysis Date = 04/12/17 Pct Recovery = 154% Analysis Date = 04/12/17 Pct Recovery = 154% Analysis Date = 04/10/17 Pct Recovery = 153% Analysis Date = 04/10/17 Pct Recovery = 153% Analysis Date = 04/08/17 Pct Recovery = 152% Analysis Date = 04/08/17 Pct Recovery = 152% Analysis Date = 04/05/17 Pct Recovery = 151% Analysis Date = 04/05/17 Pct Recovery = 151% Analysis Date = 04/03/17 Pct Recovery = 151% Analysis Date = 04/03/17 Pct Recovery = 151% Analysis Date = 04/01/17 Pct Recovery = 150% Analysis Date = 04/01/17 Pct Recovery = 150% Analysis Date = 03/30/17 Pct Recovery = 149% Analysis Date = 03/30/17 Pct Recovery = 149% Analysis Date = 03/27/17 Pct Recovery = 148% Analysis Date = 03/27/17 Pct Recovery = 148% Analysis Date = 03/25/17 Pct Recovery = 147% Analysis Date = 03/25/17 Pct Recovery = 147% Analysis Date = 03/23/17 Pct Recovery = 147% Analysis Date = 03/23/17 Pct Recovery = 147% Analysis Date = 03/21/17 Pct Recovery = 146% Analysis Date = 03/21/17 Pct Recovery = 146% Analysis Date = 03/18/17 Pct Recovery = 145% Analysis Date = 03/18/17 Pct Recovery = 145% Analysis Date = 03/16/17 Pct Recovery = 144% Analysis Date = 03/16/17 Pct Recovery = 144% Analysis Date = 03/14/17 Pct Recovery = 143% Analysis Date = 03/14/17 Pct Recovery = 143% Analysis Date = 03/12/17 Pct Recovery = 143% Analysis Date = 03/12/17 Pct Recovery = 143% Analysis Date = 03/09/17 Pct Recovery = 142% Analysis Date = 03/09/17 Pct Recovery = 142% Analysis Date = 03/07/17 Pct Recovery = 141% Analysis Date = 03/07/17 Pct Recovery = 141% Analysis Date = 03/05/17 Pct Recovery = 140% Analysis Date = 03/05/17 Pct Recovery = 140% Analysis Date = 03/03/17 Pct Recovery = 139% Analysis Date = 03/03/17 Pct Recovery = 139% Analysis Date = 03/01/17 Pct Recovery = 139% Analysis Date = 03/01/17 Pct Recovery = 139% Analysis Date = 02/26/17 Pct Recovery = 138% Analysis Date = 02/26/17 Pct Recovery = 138% Analysis Date = 02/24/17 Pct Recovery = 137% Analysis Date = 02/24/17 Pct Recovery = 137% Analysis Date = 02/22/17 Pct Recovery = 136% Analysis Date = 02/22/17 Pct Recovery = 136% Analysis Date = 02/20/17 Pct Recovery = 135% Analysis Date = 02/20/17 Pct Recovery = 135% Analysis Date = 02/17/17 Pct Recovery = 135% Analysis Date = 02/17/17 Pct Recovery = 135% Analysis Date = 02/15/17 Pct Recovery = 134% Analysis Date = 02/15/17 Pct Recovery = 134% Analysis Date = 02/13/17 Pct Recovery = 133% Analysis Date = 02/13/17 Pct Recovery = 133% Analysis Date = 02/11/17 Pct Recovery = 132% Analysis Date = 02/11/17 Pct Recovery = 132% Analysis Date = 02/08/17 Pct Recovery = 131% Analysis Date = 02/08/17 Pct Recovery = 131% Analysis Date = 02/06/17 Pct Recovery = 131% Analysis Date = 02/06/17 Pct Recovery = 131% Analysis Date = 02/04/17 Pct Recovery = 130% Analysis Date = 02/04/17 Pct Recovery = 130% Analysis Date = 02/02/17 Pct Recovery = 129% Analysis Date = 02/02/17 Pct Recovery = 129% Analysis Date = 01/30/17 Pct Recovery = 127% Analysis Date = 01/30/17 Pct Recovery = 127% Analysis Date = 01/28/17 Pct Recovery = 125% Analysis Date = 01/28/17 Pct Recovery = 125% Analysis Date = 01/26/17 Pct Recovery = 123% Analysis Date = 01/26/17 Pct Recovery = 123% Analysis Date = 01/24/17 Pct Recovery = 122% Analysis Date = 01/24/17 Pct Recovery = 122% Analysis Date = 01/21/17 Pct Recovery = 120% Analysis Date = 01/21/17 Pct Recovery = 120% Analysis Date = 01/19/17 Pct Recovery = 119% Analysis Date = 01/19/17 Pct Recovery = 119% Analysis Date = 01/17/17 Pct Recovery = 117% Analysis Date = 01/17/17 Pct Recovery = 117% Analysis Date = 01/15/17 Pct Recovery = 116% Analysis Date = 01/15/17 Pct Recovery = 116% Analysis Date = 01/12/17 Pct Recovery = 114% Analysis Date = 01/12/17 Pct Recovery = 114% Analysis Date = 01/10/17 Pct Recovery = 113% Analysis Date = 01/10/17 Pct Recovery = 113% Analysis Date = 01/08/17 Pct Recovery = 112% Analysis Date = 01/08/17 Pct Recovery = 112% Analysis Date = 01/06/17 Pct Recovery = 110% Analysis Date = 01/06/17 Pct Recovery = 110% Analysis Date = 01/04/17 Pct Recovery = 109% Analysis Date = 01/04/17 Pct Recovery = 109% Analysis Date = 01/01/17 Pct Recovery = 107% Analysis Date = 01/01/17 Pct Recovery = 107% Analysis Date = 12/30/16 Pct Recovery = 106% Analysis Date = 12/30/16 Pct Recovery = 106% Analysis Date = 12/28/16 Pct Recovery = 104% Analysis Date = 12/28/16 Pct Recovery = 104% Analysis Date = 12/26/16 Pct Recovery = 103% Analysis Date = 12/26/16 Pct Recovery = 103% Analysis Date = 12/23/16 Pct Recovery = 102% Analysis Date = 12/23/16 Pct Recovery = 102% Analysis Date = 12/21/16 Pct Recovery = 100% Analysis Date = 12/21/16 Pct Recovery = 100% Analysis Date = 12/19/16 Pct Recovery = 99% Analysis Date = 12/19/16 Pct Recovery = 99% Analysis Date = 12/17/16 Pct Recovery = 97% Analysis Date = 12/17/16 Pct Recovery = 97% Analysis Date = 12/14/16 Pct Recovery = 96% Analysis Date = 12/14/16 Pct Recovery = 96% Analysis Date = 12/12/16 Pct Recovery = 95% Analysis Date = 12/12/16 Pct Recovery = 95% Analysis Date = 12/10/16 Pct Recovery = 94% Analysis Date = 12/10/16 Pct Recovery = 94% Analysis Date = 12/08/16 Pct Recovery = 94% Analysis Date = 12/08/16 Pct Recovery = 94% Analysis Date = 12/05/16 Pct Recovery = 94% Analysis Date = 12/05/16 Pct Recovery = 94% Analysis Date = 12/03/16 Pct Recovery = 94% Analysis Date = 12/03/16 Pct Recovery = 94% Analysis Date = 12/01/16 Pct Recovery = 94% Analysis Date = 12/01/16 Pct Recovery = 94% Analysis Date = 11/29/16 Pct Recovery = 94% Analysis Date = 11/29/16 Pct Recovery = 94% Analysis Date = 11/26/16 Pct Recovery = 94% Analysis Date = 11/26/16 Pct Recovery = 94% Analysis Date = 11/24/16 Pct Recovery = 94% Analysis Date = 11/24/16 Pct Recovery = 94% Analysis Date = 11/22/16 Pct Recovery = 93% Analysis Date = 11/22/16 Pct Recovery = 93% Analysis Date = 11/20/16 Pct Recovery = 93% Analysis Date = 11/20/16 Pct Recovery = 93% Analysis Date = 11/17/16 Pct Recovery = 93% Analysis Date = 11/17/16 Pct Recovery = 93% Analysis Date = 11/15/16 Pct Recovery = 93% Analysis Date = 11/15/16 Pct Recovery = 93% Analysis Date = 11/13/16 Pct Recovery = 93% Analysis Date = 11/13/16 Pct Recovery = 93% Analysis Date = 11/11/16 Pct Recovery = 93% Analysis Date = 11/11/16 Pct Recovery = 93% Analysis Date = 11/09/16 Pct Recovery = 93% Analysis Date = 11/09/16 Pct Recovery = 93% Analysis Date = 11/06/16 Pct Recovery = 92% Analysis Date = 11/06/16 Pct Recovery = 92% Analysis Date = 11/04/16 Pct Recovery = 92% Analysis Date = 11/04/16 Pct Recovery = 92% Analysis Date = 11/02/16 Pct Recovery = 92% Analysis Date = 11/02/16 Pct Recovery = 92% Analysis Date = 10/31/16 Pct Recovery = 92% Analysis Date = 10/31/16 Pct Recovery = 92% Analysis Date = 10/28/16 Pct Recovery = 92% Analysis Date = 10/28/16 Pct Recovery = 92% Analysis Date = 10/26/16 Pct Recovery = 92% Analysis Date = 10/26/16 Pct Recovery = 92% Analysis Date = 10/24/16 Pct Recovery = 92% Analysis Date = 10/24/16 Pct Recovery = 92% Analysis Date = 10/22/16 Pct Recovery = 91% Analysis Date = 10/22/16 Pct Recovery = 91% Analysis Date = 10/19/16 Pct Recovery = 91% Analysis Date = 10/19/16 Pct Recovery = 91% Analysis Date = 10/17/16 Pct Recovery = 91% Analysis Date = 10/17/16 Pct Recovery = 91% Analysis Date = 10/15/16 Pct Recovery = 91% Analysis Date = 10/15/16 Pct Recovery = 91% Analysis Date = 10/13/16 Pct Recovery = 91% Analysis Date = 10/13/16 Pct Recovery = 91% Analysis Date = 10/10/16 Pct Recovery = 91% Analysis Date = 10/10/16 Pct Recovery = 91% Analysis Date = 10/08/16 Pct Recovery = 91% Analysis Date = 10/08/16 Pct Recovery = 91% Analysis Date = 10/06/16 Pct Recovery = 91% Analysis Date = 10/06/16 Pct Recovery = 91% Analysis Date = 10/04/16 Pct Recovery = 91% Analysis Date = 10/04/16 Pct Recovery = 91% Analysis Date = 10/01/16 Pct Recovery = 91% Analysis Date = 10/01/16 Pct Recovery = 91% Analysis Date = 09/29/16 Pct Recovery = 91% Analysis Date = 09/29/16 Pct Recovery = 91% Analysis Date = 09/27/16 Pct Recovery = 91% Analysis Date = 09/27/16 Pct Recovery = 91% Analysis Date = 09/25/16 Pct Recovery = 91% Analysis Date = 09/25/16 Pct Recovery = 91% Analysis Date = 09/22/16 Pct Recovery = 91% Analysis Date = 09/22/16 Pct Recovery = 91% Analysis Date = 09/20/16 Pct Recovery = 91% Analysis Date = 09/20/16 Pct Recovery = 91% Analysis Date = 09/18/16 Pct Recovery = 91% Analysis Date = 09/18/16 Pct Recovery = 91% Analysis Date = 09/16/16 Pct Recovery = 91% Analysis Date = 09/16/16 Pct Recovery = 91% Analysis Date = 09/14/16 Pct Recovery = 92% Analysis Date = 09/14/16 Pct Recovery = 92% Analysis Date = 09/11/16 Pct Recovery = 92% Analysis Date = 09/11/16 Pct Recovery = 92% Analysis Date = 09/09/16 Pct Recovery = 92% Analysis Date = 09/09/16 Pct Recovery = 92% Analysis Date = 09/07/16 Pct Recovery = 92% Analysis Date = 09/07/16 Pct Recovery = 92% Analysis Date = 09/05/16 Pct Recovery = 92% Analysis Date = 09/05/16 Pct Recovery = 92% Analysis Date = 09/02/16 Pct Recovery = 92% Analysis Date = 09/02/16 Pct Recovery = 92% Analysis Date = 08/31/16 Pct Recovery = 92% Analysis Date = 08/31/16 Pct Recovery = 92% Analysis Date = 08/29/16 Pct Recovery = 93% Analysis Date = 08/29/16 Pct Recovery = 93% Analysis Date = 08/27/16 Pct Recovery = 93% Analysis Date = 08/27/16 Pct Recovery = 93% Analysis Date = 08/24/16 Pct Recovery = 93% Analysis Date = 08/24/16 Pct Recovery = 93% Analysis Date = 08/22/16 Pct Recovery = 93% Analysis Date = 08/22/16 Pct Recovery = 93% Analysis Date = 08/20/16 Pct Recovery = 93% Analysis Date = 08/20/16 Pct Recovery = 93% Analysis Date = 08/18/16 Pct Recovery = 94% Analysis Date = 08/18/16 Pct Recovery = 94% Analysis Date = 08/15/16 Pct Recovery = 94% Analysis Date = 08/15/16 Pct Recovery = 94% Analysis Date = 08/13/16 Pct Recovery = 94% Analysis Date = 08/13/16 Pct Recovery = 94% Analysis Date = 08/11/16 Pct Recovery = 94% Analysis Date = 08/11/16 Pct Recovery = 94% Analysis Date = 08/09/16 Pct Recovery = 94% Analysis Date = 08/09/16 Pct Recovery = 94% Analysis Date = 08/06/16 Pct Recovery = 95% Analysis Date = 08/06/16 Pct Recovery = 95% Analysis Date = 08/04/16 Pct Recovery = 95% Analysis Date = 08/04/16 Pct Recovery = 95% Analysis Date = 08/02/16 Pct Recovery = 95% Analysis Date = 08/02/16 Pct Recovery = 95% Analysis Date = 07/31/16 Pct Recovery = 95% Analysis Date = 07/31/16 Pct Recovery = 95% Analysis Date = 07/28/16 Pct Recovery = 95% Analysis Date = 07/28/16 Pct Recovery = 95% Analysis Date = 07/26/16 Pct Recovery = 96% Analysis Date = 07/26/16 Pct Recovery = 96% Analysis Date = 07/24/16 Pct Recovery = 96% Analysis Date = 07/24/16 Pct Recovery = 96% Analysis Date = 07/22/16 Pct Recovery = 96% Analysis Date = 07/22/16 Pct Recovery = 96% Analysis Date = 07/20/16 Pct Recovery = 97% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FIPRONIL AMIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 30 114% 56% 96% 29%
Total 30 114% 56% 96% 29%

Sample Statistics
FIPRONIL AMIDE

Characteristic N % % Basis
Plotted 30 100% Spiked
Estimated Values 2 7% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 30 .  
False Negatives 0 0% 0 out of 30
Not Spiked 89 .  
False Positives 25 28% 25 out of 89