OBSP Determination:
DISULFOTON OXON
METHOD: 2437 , TESTIDCODE: 68586LCM60

Analysis Date = 08/11/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 290% Analysis Date = 03/10/17 SpikeMix = Abs 072516: 100 µl & Abs 071216: 100 µl Pct Recovery = 48% Analysis Date = 03/10/17 SpikeMix = Abs 072516: 100 µl & Abs 071216: 100 µl Pct Recovery = 58% Analysis Date = 02/01/17 SpikeMix = Spex Organics TS160603008: 100 µl & Spex Organics TS160511023: 100 µl Pct Recovery = 61% Analysis Date = 02/01/17 SpikeMix = Spex Organics TS160603008: 100 µl & Spex Organics TS160511023: 100 µl Pct Recovery = 63% Analysis Date = 10/04/17 SpikeMix = Abs 071917Pest3: 50 µl & Abs 071717Pest3: 50 µl Pct Recovery = 89% Analysis Date = 08/23/17 SpikeMix = Abs 071717Pest3: 50 µl & Abs 072417Pest3: 50 µl Pct Recovery = 101% Analysis Date = 07/19/17 SpikeMix = Spex Organics TS160511023: 80 µl & Abs 072516: 80 µl Pct Recovery = 55% Analysis Date = 07/11/17 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 65% Analysis Date = 06/02/17 SpikeMix = Abs 071216: 80 µl & ChemService 5154100: 80 µl Pct Recovery = 65% Analysis Date = 01/18/17 SpikeMix = Spex Organics TS160511023: 80 µl & Abs 071816: 80 µl Pct Recovery = 50% Analysis Date = 01/17/17 SpikeMix = Spex Organics TS160511023: 80 µl & Abs 071816: 80 µl Pct Recovery = 46% Analysis Date = 12/13/16 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 67% Analysis Date = 12/13/16 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 64% Analysis Date = 09/13/16 SpikeMix = Abs 072516: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 61% Analysis Date = 09/13/16 SpikeMix = Abs 072516: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 49% Analysis Date = 07/12/16 SpikeMix = Spex Organics TS160603008: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 55% Analysis Date = 07/12/16 SpikeMix = Spex Organics TS160603008: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 60% Analysis Date = 03/17/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 58% Analysis Date = 03/17/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 98% Analysis Date = 03/17/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 68% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 73% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 62% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 61% Analysis Date = 05/06/16 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 92% Analysis Date = 05/06/16 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 101% Analysis Date = 02/17/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 60% Analysis Date = 02/17/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 61% Analysis Date = 02/17/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 68% Analysis Date = 07/28/17 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 75% Analysis Date = 07/12/17 SpikeMix = Spex Organics TS160511023: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 61% Analysis Date = 06/07/17 SpikeMix = Abs 071216: 40 µl & Abs 071816: 40 µl Pct Recovery = 77% Analysis Date = 06/05/17 SpikeMix = Spex Organics TS160511023: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 59% Analysis Date = 05/17/17 SpikeMix = Spex Organics TS160511023: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 71% Analysis Date = 01/04/17 SpikeMix = Abs 072516: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 74% Analysis Date = 01/04/17 SpikeMix = Abs 072516: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 59% Analysis Date = 11/08/16 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 58% Analysis Date = 11/08/16 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 59% Analysis Date = 08/11/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 159% Analysis Date = 08/03/16 SpikeMix = Spex Organics TS160603008: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 50% Analysis Date = 08/03/16 SpikeMix = Spex Organics TS160603008: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 46% Analysis Date = 07/29/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 41% Analysis Date = 07/29/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 27% Analysis Date = 06/29/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 24% Analysis Date = 06/29/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 36% Analysis Date = 10/11/17 SpikeMix = Abs 071917Pest3: 20 µl & Abs 071717Pest3: 20 µl Pct Recovery = 99% Analysis Date = 09/23/17 SpikeMix = Abs 071717Pest3: 20 µl & Abs 072417Pest3: 20 µl Pct Recovery = 70% Analysis Date = 08/08/17 SpikeMix = Abs 071917Pest3: 20 µl & Abs 071717Pest3: 20 µl Pct Recovery = 96% Analysis Date = 03/23/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ChemService 4047000: 1 Pct Recovery = 71% Analysis Date = 03/23/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ChemService 4047000: 1 Pct Recovery = 56% Analysis Date = 03/23/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ChemService 4047000: 1 Pct Recovery = 87% Analysis Date = 02/19/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 60% Analysis Date = 02/19/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 65% Analysis Date = 02/19/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 70% Analysis Date = 03/02/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 73% Analysis Date = 03/02/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 106% Analysis Date = 03/02/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 100% Analysis Date = 02/18/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 83% Analysis Date = 02/18/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 86% Analysis Date = 02/18/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 75% Analysis Date = 02/12/16 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 70% Analysis Date = 02/12/16 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 81% Analysis Date = 02/12/16 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 71% Analysis Date = 10/10/17 Pct Recovery = 83% Analysis Date = 10/07/17 Pct Recovery = 83% Analysis Date = 10/07/17 Pct Recovery = 83% Analysis Date = 10/04/17 Pct Recovery = 83% Analysis Date = 10/04/17 Pct Recovery = 83% Analysis Date = 10/01/17 Pct Recovery = 82% Analysis Date = 10/01/17 Pct Recovery = 82% Analysis Date = 09/28/17 Pct Recovery = 82% Analysis Date = 09/28/17 Pct Recovery = 82% Analysis Date = 09/25/17 Pct Recovery = 82% Analysis Date = 09/25/17 Pct Recovery = 82% Analysis Date = 09/22/17 Pct Recovery = 81% Analysis Date = 09/22/17 Pct Recovery = 81% Analysis Date = 09/19/17 Pct Recovery = 81% Analysis Date = 09/19/17 Pct Recovery = 81% Analysis Date = 09/16/17 Pct Recovery = 81% Analysis Date = 09/16/17 Pct Recovery = 81% Analysis Date = 09/13/17 Pct Recovery = 80% Analysis Date = 09/13/17 Pct Recovery = 80% Analysis Date = 09/10/17 Pct Recovery = 80% Analysis Date = 09/10/17 Pct Recovery = 80% Analysis Date = 09/07/17 Pct Recovery = 80% Analysis Date = 09/07/17 Pct Recovery = 80% Analysis Date = 09/04/17 Pct Recovery = 80% Analysis Date = 09/04/17 Pct Recovery = 80% Analysis Date = 09/01/17 Pct Recovery = 79% Analysis Date = 09/01/17 Pct Recovery = 79% Analysis Date = 08/29/17 Pct Recovery = 79% Analysis Date = 08/29/17 Pct Recovery = 79% Analysis Date = 08/26/17 Pct Recovery = 79% Analysis Date = 08/26/17 Pct Recovery = 79% Analysis Date = 08/23/17 Pct Recovery = 78% Analysis Date = 08/23/17 Pct Recovery = 78% Analysis Date = 08/20/17 Pct Recovery = 78% Analysis Date = 08/20/17 Pct Recovery = 78% Analysis Date = 08/17/17 Pct Recovery = 78% Analysis Date = 08/17/17 Pct Recovery = 78% Analysis Date = 08/14/17 Pct Recovery = 78% Analysis Date = 08/14/17 Pct Recovery = 78% Analysis Date = 08/11/17 Pct Recovery = 77% Analysis Date = 08/11/17 Pct Recovery = 77% Analysis Date = 08/08/17 Pct Recovery = 77% Analysis Date = 08/08/17 Pct Recovery = 77% Analysis Date = 08/05/17 Pct Recovery = 77% Analysis Date = 08/05/17 Pct Recovery = 77% Analysis Date = 08/02/17 Pct Recovery = 76% Analysis Date = 08/02/17 Pct Recovery = 76% Analysis Date = 07/30/17 Pct Recovery = 76% Analysis Date = 07/30/17 Pct Recovery = 76% Analysis Date = 07/27/17 Pct Recovery = 76% Analysis Date = 07/27/17 Pct Recovery = 76% Analysis Date = 07/24/17 Pct Recovery = 75% Analysis Date = 07/24/17 Pct Recovery = 75% Analysis Date = 07/21/17 Pct Recovery = 75% Analysis Date = 07/21/17 Pct Recovery = 75% Analysis Date = 07/18/17 Pct Recovery = 75% Analysis Date = 07/18/17 Pct Recovery = 75% Analysis Date = 07/14/17 Pct Recovery = 75% Analysis Date = 07/14/17 Pct Recovery = 75% Analysis Date = 07/11/17 Pct Recovery = 74% Analysis Date = 07/11/17 Pct Recovery = 74% Analysis Date = 07/08/17 Pct Recovery = 74% Analysis Date = 07/08/17 Pct Recovery = 74% Analysis Date = 07/05/17 Pct Recovery = 74% Analysis Date = 07/05/17 Pct Recovery = 74% Analysis Date = 07/02/17 Pct Recovery = 74% Analysis Date = 07/02/17 Pct Recovery = 74% Analysis Date = 06/29/17 Pct Recovery = 73% Analysis Date = 06/29/17 Pct Recovery = 73% Analysis Date = 06/26/17 Pct Recovery = 73% Analysis Date = 06/26/17 Pct Recovery = 73% Analysis Date = 06/23/17 Pct Recovery = 73% Analysis Date = 06/23/17 Pct Recovery = 73% Analysis Date = 06/20/17 Pct Recovery = 72% Analysis Date = 06/20/17 Pct Recovery = 72% Analysis Date = 06/17/17 Pct Recovery = 72% Analysis Date = 06/17/17 Pct Recovery = 72% Analysis Date = 06/14/17 Pct Recovery = 72% Analysis Date = 06/14/17 Pct Recovery = 72% Analysis Date = 06/11/17 Pct Recovery = 72% Analysis Date = 06/11/17 Pct Recovery = 72% Analysis Date = 06/08/17 Pct Recovery = 71% Analysis Date = 06/08/17 Pct Recovery = 71% Analysis Date = 06/05/17 Pct Recovery = 71% Analysis Date = 06/05/17 Pct Recovery = 71% Analysis Date = 06/02/17 Pct Recovery = 71% Analysis Date = 06/02/17 Pct Recovery = 71% Analysis Date = 05/30/17 Pct Recovery = 71% Analysis Date = 05/30/17 Pct Recovery = 71% Analysis Date = 05/27/17 Pct Recovery = 71% Analysis Date = 05/27/17 Pct Recovery = 71% Analysis Date = 05/24/17 Pct Recovery = 70% Analysis Date = 05/24/17 Pct Recovery = 70% Analysis Date = 05/21/17 Pct Recovery = 70% Analysis Date = 05/21/17 Pct Recovery = 70% Analysis Date = 05/18/17 Pct Recovery = 70% Analysis Date = 05/18/17 Pct Recovery = 70% Analysis Date = 05/15/17 Pct Recovery = 70% Analysis Date = 05/15/17 Pct Recovery = 70% Analysis Date = 05/12/17 Pct Recovery = 70% Analysis Date = 05/12/17 Pct Recovery = 70% Analysis Date = 05/09/17 Pct Recovery = 70% Analysis Date = 05/09/17 Pct Recovery = 70% Analysis Date = 05/06/17 Pct Recovery = 70% Analysis Date = 05/06/17 Pct Recovery = 70% Analysis Date = 05/03/17 Pct Recovery = 69% Analysis Date = 05/03/17 Pct Recovery = 69% Analysis Date = 04/30/17 Pct Recovery = 69% Analysis Date = 04/30/17 Pct Recovery = 69% Analysis Date = 04/27/17 Pct Recovery = 69% Analysis Date = 04/27/17 Pct Recovery = 69% Analysis Date = 04/24/17 Pct Recovery = 69% Analysis Date = 04/24/17 Pct Recovery = 69% Analysis Date = 04/21/17 Pct Recovery = 69% Analysis Date = 04/21/17 Pct Recovery = 69% Analysis Date = 04/17/17 Pct Recovery = 69% Analysis Date = 04/17/17 Pct Recovery = 69% Analysis Date = 04/14/17 Pct Recovery = 68% Analysis Date = 04/14/17 Pct Recovery = 68% Analysis Date = 04/11/17 Pct Recovery = 68% Analysis Date = 04/11/17 Pct Recovery = 68% Analysis Date = 04/08/17 Pct Recovery = 68% Analysis Date = 04/08/17 Pct Recovery = 68% Analysis Date = 04/05/17 Pct Recovery = 68% Analysis Date = 04/05/17 Pct Recovery = 68% Analysis Date = 04/02/17 Pct Recovery = 68% Analysis Date = 04/02/17 Pct Recovery = 68% Analysis Date = 03/30/17 Pct Recovery = 68% Analysis Date = 03/30/17 Pct Recovery = 68% Analysis Date = 03/27/17 Pct Recovery = 68% Analysis Date = 03/27/17 Pct Recovery = 68% Analysis Date = 03/24/17 Pct Recovery = 67% Analysis Date = 03/24/17 Pct Recovery = 67% Analysis Date = 03/21/17 Pct Recovery = 67% Analysis Date = 03/21/17 Pct Recovery = 67% Analysis Date = 03/18/17 Pct Recovery = 67% Analysis Date = 03/18/17 Pct Recovery = 67% Analysis Date = 03/15/17 Pct Recovery = 67% Analysis Date = 03/15/17 Pct Recovery = 67% Analysis Date = 03/12/17 Pct Recovery = 67% Analysis Date = 03/12/17 Pct Recovery = 67% Analysis Date = 03/09/17 Pct Recovery = 67% Analysis Date = 03/09/17 Pct Recovery = 67% Analysis Date = 03/06/17 Pct Recovery = 67% Analysis Date = 03/06/17 Pct Recovery = 67% Analysis Date = 03/03/17 Pct Recovery = 66% Analysis Date = 03/03/17 Pct Recovery = 66% Analysis Date = 02/28/17 Pct Recovery = 66% Analysis Date = 02/28/17 Pct Recovery = 66% Analysis Date = 02/25/17 Pct Recovery = 66% Analysis Date = 02/25/17 Pct Recovery = 66% Analysis Date = 02/22/17 Pct Recovery = 66% Analysis Date = 02/22/17 Pct Recovery = 66% Analysis Date = 02/19/17 Pct Recovery = 66% Analysis Date = 02/19/17 Pct Recovery = 66% Analysis Date = 02/16/17 Pct Recovery = 66% Analysis Date = 02/16/17 Pct Recovery = 66% Analysis Date = 02/13/17 Pct Recovery = 66% Analysis Date = 02/13/17 Pct Recovery = 66% Analysis Date = 02/10/17 Pct Recovery = 65% Analysis Date = 02/10/17 Pct Recovery = 65% Analysis Date = 02/07/17 Pct Recovery = 65% Analysis Date = 02/07/17 Pct Recovery = 65% Analysis Date = 02/04/17 Pct Recovery = 65% Analysis Date = 02/04/17 Pct Recovery = 65% Analysis Date = 02/01/17 Pct Recovery = 65% Analysis Date = 02/01/17 Pct Recovery = 65% Analysis Date = 01/29/17 Pct Recovery = 65% Analysis Date = 01/29/17 Pct Recovery = 65% Analysis Date = 01/26/17 Pct Recovery = 65% Analysis Date = 01/26/17 Pct Recovery = 65% Analysis Date = 01/22/17 Pct Recovery = 65% Analysis Date = 01/22/17 Pct Recovery = 65% Analysis Date = 01/19/17 Pct Recovery = 65% Analysis Date = 01/19/17 Pct Recovery = 65% Analysis Date = 01/16/17 Pct Recovery = 65% Analysis Date = 01/16/17 Pct Recovery = 65% Analysis Date = 01/13/17 Pct Recovery = 65% Analysis Date = 01/13/17 Pct Recovery = 65% Analysis Date = 01/10/17 Pct Recovery = 66% Analysis Date = 01/10/17 Pct Recovery = 66% Analysis Date = 01/07/17 Pct Recovery = 66% Analysis Date = 01/07/17 Pct Recovery = 66% Analysis Date = 01/04/17 Pct Recovery = 66% Analysis Date = 01/04/17 Pct Recovery = 66% Analysis Date = 01/01/17 Pct Recovery = 66% Analysis Date = 01/01/17 Pct Recovery = 66% Analysis Date = 12/29/16 Pct Recovery = 66% Analysis Date = 12/29/16 Pct Recovery = 66% Analysis Date = 12/26/16 Pct Recovery = 66% Analysis Date = 12/26/16 Pct Recovery = 66% Analysis Date = 12/23/16 Pct Recovery = 66% Analysis Date = 12/23/16 Pct Recovery = 66% Analysis Date = 12/20/16 Pct Recovery = 66% Analysis Date = 12/20/16 Pct Recovery = 66% Analysis Date = 12/17/16 Pct Recovery = 66% Analysis Date = 12/17/16 Pct Recovery = 66% Analysis Date = 12/14/16 Pct Recovery = 66% Analysis Date = 12/14/16 Pct Recovery = 66% Analysis Date = 12/11/16 Pct Recovery = 66% Analysis Date = 12/11/16 Pct Recovery = 66% Analysis Date = 12/08/16 Pct Recovery = 67% Analysis Date = 12/08/16 Pct Recovery = 67% Analysis Date = 12/05/16 Pct Recovery = 67% Analysis Date = 12/05/16 Pct Recovery = 67% Analysis Date = 12/02/16 Pct Recovery = 67% Analysis Date = 12/02/16 Pct Recovery = 67% Analysis Date = 11/29/16 Pct Recovery = 67% Analysis Date = 11/29/16 Pct Recovery = 67% Analysis Date = 11/26/16 Pct Recovery = 67% Analysis Date = 11/26/16 Pct Recovery = 67% Analysis Date = 11/23/16 Pct Recovery = 67% Analysis Date = 11/23/16 Pct Recovery = 67% Analysis Date = 11/20/16 Pct Recovery = 67% Analysis Date = 11/20/16 Pct Recovery = 67% Analysis Date = 11/17/16 Pct Recovery = 67% Analysis Date = 11/17/16 Pct Recovery = 67% Analysis Date = 11/14/16 Pct Recovery = 67% Analysis Date = 11/14/16 Pct Recovery = 67% Analysis Date = 11/11/16 Pct Recovery = 67% Analysis Date = 11/11/16 Pct Recovery = 67% Analysis Date = 11/08/16 Pct Recovery = 67% Analysis Date = 11/08/16 Pct Recovery = 67% Analysis Date = 11/05/16 Pct Recovery = 68% Analysis Date = 11/05/16 Pct Recovery = 68% Analysis Date = 11/02/16 Pct Recovery = 68% Analysis Date = 11/02/16 Pct Recovery = 68% Analysis Date = 10/30/16 Pct Recovery = 68% Analysis Date = 10/30/16 Pct Recovery = 68% Analysis Date = 10/26/16 Pct Recovery = 68% Analysis Date = 10/26/16 Pct Recovery = 68% Analysis Date = 10/23/16 Pct Recovery = 69% Analysis Date = 10/23/16 Pct Recovery = 69% Analysis Date = 10/20/16 Pct Recovery = 69% Analysis Date = 10/20/16 Pct Recovery = 69% Analysis Date = 10/17/16 Pct Recovery = 69% Analysis Date = 10/17/16 Pct Recovery = 69% Analysis Date = 10/14/16 Pct Recovery = 69% Analysis Date = 10/14/16 Pct Recovery = 69% Analysis Date = 10/11/16 Pct Recovery = 70% Analysis Date = 10/11/16 Pct Recovery = 70% Analysis Date = 10/08/16 Pct Recovery = 70% Analysis Date = 10/08/16 Pct Recovery = 70% Analysis Date = 10/05/16 Pct Recovery = 70% Analysis Date = 10/05/16 Pct Recovery = 70% Analysis Date = 10/02/16 Pct Recovery = 70% Analysis Date = 10/02/16 Pct Recovery = 70% Analysis Date = 09/29/16 Pct Recovery = 71% Analysis Date = 09/29/16 Pct Recovery = 71% Analysis Date = 09/26/16 Pct Recovery = 71% Analysis Date = 09/26/16 Pct Recovery = 71% Analysis Date = 09/23/16 Pct Recovery = 71% Analysis Date = 09/23/16 Pct Recovery = 71% Analysis Date = 09/20/16 Pct Recovery = 71% Analysis Date = 09/20/16 Pct Recovery = 71% Analysis Date = 09/17/16 Pct Recovery = 72% Analysis Date = 09/17/16 Pct Recovery = 72% Analysis Date = 09/14/16 Pct Recovery = 72% Analysis Date = 09/14/16 Pct Recovery = 72% Analysis Date = 09/11/16 Pct Recovery = 72% Analysis Date = 09/11/16 Pct Recovery = 72% Analysis Date = 09/08/16 Pct Recovery = 73% Analysis Date = 09/08/16 Pct Recovery = 73% Analysis Date = 09/05/16 Pct Recovery = 73% Analysis Date = 09/05/16 Pct Recovery = 73% Analysis Date = 09/02/16 Pct Recovery = 73% Analysis Date = 09/02/16 Pct Recovery = 73% Analysis Date = 08/30/16 Pct Recovery = 73% Analysis Date = 08/30/16 Pct Recovery = 73% Analysis Date = 08/27/16 Pct Recovery = 74% Analysis Date = 08/27/16 Pct Recovery = 74% Analysis Date = 08/24/16 Pct Recovery = 74% Analysis Date = 08/24/16 Pct Recovery = 74% Analysis Date = 08/21/16 Pct Recovery = 74% Analysis Date = 08/21/16 Pct Recovery = 74% Analysis Date = 08/18/16 Pct Recovery = 74% Analysis Date = 08/18/16 Pct Recovery = 74% Analysis Date = 08/15/16 Pct Recovery = 75% Analysis Date = 08/15/16 Pct Recovery = 75% Analysis Date = 08/12/16 Pct Recovery = 75% Analysis Date = 08/12/16 Pct Recovery = 75% Analysis Date = 08/09/16 Pct Recovery = 75% Analysis Date = 08/09/16 Pct Recovery = 75% Analysis Date = 08/06/16 Pct Recovery = 75% Analysis Date = 08/06/16 Pct Recovery = 75% Analysis Date = 08/02/16 Pct Recovery = 76% Analysis Date = 08/02/16 Pct Recovery = 76% Analysis Date = 07/30/16 Pct Recovery = 76% Analysis Date = 07/30/16 Pct Recovery = 76% Analysis Date = 07/27/16 Pct Recovery = 76% Analysis Date = 07/27/16 Pct Recovery = 76% Analysis Date = 07/24/16 Pct Recovery = 76% Analysis Date = 07/24/16 Pct Recovery = 76% Analysis Date = 07/21/16 Pct Recovery = 76% Analysis Date = 07/21/16 Pct Recovery = 76% Analysis Date = 07/18/16 Pct Recovery = 76% Analysis Date = 07/18/16 Pct Recovery = 76% Analysis Date = 07/15/16 Pct Recovery = 76% Analysis Date = 07/15/16 Pct Recovery = 76% Analysis Date = 07/12/16 Pct Recovery = 76% Analysis Date = 07/12/16 Pct Recovery = 76% Analysis Date = 07/09/16 Pct Recovery = 76% Analysis Date = 07/09/16 Pct Recovery = 76% Analysis Date = 07/06/16 Pct Recovery = 76% Analysis Date = 07/06/16 Pct Recovery = 76% Analysis Date = 07/03/16 Pct Recovery = 76% Analysis Date = 07/03/16 Pct Recovery = 76% Analysis Date = 06/30/16 Pct Recovery = 76% Analysis Date = 06/30/16 Pct Recovery = 76% Analysis Date = 06/27/16 Pct Recovery = 76% Analysis Date = 06/27/16 Pct Recovery = 76% Analysis Date = 06/24/16 Pct Recovery = 76% Analysis Date = 06/24/16 Pct Recovery = 76% Analysis Date = 06/21/16 Pct Recovery = 76% Analysis Date = 06/21/16 Pct Recovery = 76% Analysis Date = 06/18/16 Pct Recovery = 76% Analysis Date = 06/18/16 Pct Recovery = 76% Analysis Date = 06/15/16 Pct Recovery = 76% Analysis Date = 06/15/16 Pct Recovery = 76% Analysis Date = 06/12/16 Pct Recovery = 76% Analysis Date = 06/12/16 Pct Recovery = 76% Analysis Date = 06/09/16 Pct Recovery = 75% Analysis Date = 06/09/16 Pct Recovery = 75% Analysis Date = 06/06/16 Pct Recovery = 75% Analysis Date = 06/06/16 Pct Recovery = 75% Analysis Date = 06/03/16 Pct Recovery = 75% Analysis Date = 06/03/16 Pct Recovery = 75% Analysis Date = 05/31/16 Pct Recovery = 75% Analysis Date = 05/31/16 Pct Recovery = 75% Analysis Date = 05/28/16 Pct Recovery = 75% Analysis Date = 05/28/16 Pct Recovery = 75% Analysis Date = 05/25/16 Pct Recovery = 75% Analysis Date = 05/25/16 Pct Recovery = 75% Analysis Date = 05/22/16 Pct Recovery = 75% Analysis Date = 05/22/16 Pct Recovery = 75% Analysis Date = 05/19/16 Pct Recovery = 75% Analysis Date = 05/19/16 Pct Recovery = 75% Analysis Date = 05/16/16 Pct Recovery = 75% Analysis Date = 05/16/16 Pct Recovery = 75% Analysis Date = 05/13/16 Pct Recovery = 75% Analysis Date = 05/13/16 Pct Recovery = 75% Analysis Date = 05/10/16 Pct Recovery = 74% Analysis Date = 05/10/16 Pct Recovery = 74% Analysis Date = 05/06/16 Pct Recovery = 74% Analysis Date = 05/06/16 Pct Recovery = 74% Analysis Date = 05/03/16 Pct Recovery = 74% Analysis Date = 05/03/16 Pct Recovery = 74% Analysis Date = 04/30/16 Pct Recovery = 74% Analysis Date = 04/30/16 Pct Recovery = 74% Analysis Date = 04/27/16 Pct Recovery = 74% Analysis Date = 04/27/16 Pct Recovery = 74% Analysis Date = 04/24/16 Pct Recovery = 74% Analysis Date = 04/24/16 Pct Recovery = 74% Analysis Date = 04/21/16 Pct Recovery = 74% Analysis Date = 04/21/16 Pct Recovery = 74% Analysis Date = 04/18/16 Pct Recovery = 74% Analysis Date = 04/18/16 Pct Recovery = 74% Analysis Date = 04/15/16 Pct Recovery = 74% Analysis Date = 04/15/16 Pct Recovery = 74% Analysis Date = 04/12/16 Pct Recovery = 74% Analysis Date = 04/12/16 Pct Recovery = 74% Analysis Date = 04/09/16 Pct Recovery = 73% Analysis Date = 04/09/16 Pct Recovery = 73% Analysis Date = 04/06/16 Pct Recovery = 73% Analysis Date = 04/06/16 Pct Recovery = 73% Analysis Date = 04/03/16 Pct Recovery = 73% Analysis Date = 04/03/16 Pct Recovery = 73% Analysis Date = 03/31/16 Pct Recovery = 73% Analysis Date = 03/31/16 Pct Recovery = 73% Analysis Date = 03/28/16 Pct Recovery = 73% Analysis Date = 03/28/16 Pct Recovery = 73% Analysis Date = 03/25/16 Pct Recovery = 73% Analysis Date = 03/25/16 Pct Recovery = 73% Analysis Date = 03/22/16 Pct Recovery = 73% Analysis Date = 03/22/16 Pct Recovery = 73% Analysis Date = 03/19/16 Pct Recovery = 73% Analysis Date = 03/19/16 Pct Recovery = 73% Analysis Date = 03/16/16 Pct Recovery = 73% Analysis Date = 03/16/16 Pct Recovery = 73% Analysis Date = 03/13/16 Pct Recovery = 73% Analysis Date = 03/13/16 Pct Recovery = 73% Analysis Date = 03/10/16 Pct Recovery = 73% Analysis Date = 03/10/16 Pct Recovery = 73% Analysis Date = 03/07/16 Pct Recovery = 74% Analysis Date = 03/07/16 Pct Recovery = 74% Analysis Date = 03/04/16 Pct Recovery = 74% Analysis Date = 03/04/16 Pct Recovery = 74% Analysis Date = 03/01/16 Pct Recovery = 74% Analysis Date = 03/01/16 Pct Recovery = 74% Analysis Date = 02/27/16 Pct Recovery = 74% Analysis Date = 02/27/16 Pct Recovery = 74% Analysis Date = 02/24/16 Pct Recovery = 74% Analysis Date = 02/24/16 Pct Recovery = 74% Analysis Date = 02/21/16 Pct Recovery = 74% Analysis Date = 02/21/16 Pct Recovery = 74% Analysis Date = 02/18/16 Pct Recovery = 74% Analysis Date = 02/18/16 Pct Recovery = 74% Analysis Date = 02/15/16 Pct Recovery = 75% Analysis Date = 02/15/16 Pct Recovery = 75% Analysis Date = 02/12/16 Pct Recovery = 75% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DISULFOTON OXON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 63 72% 35% 65% 13%
Total 63 72% 35% 65% 13%

Sample Statistics
DISULFOTON OXON

Characteristic N % % Basis
Plotted 63 78% Spiked
Estimated Values 7 9% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 2 2% Spiked
Spiked 81 .  
False Negatives 16 20% 16 out of 81
Not Spiked 38 .  
False Positives 0 0% 0 out of 36