OBSP Determination:
DEMETHYL NORFLURAZON
METHOD: 2437 , TESTIDCODE: 68567LCM60

Analysis Date = 09/22/17 SpikeMix = Abs 071917Pest3: 80 µl & Abs 072417Pest3: 80 µl Pct Recovery = 89% Analysis Date = 09/15/17 SpikeMix = Abs 071917Pest3: 50 µl & Abs 072417Pest3: 50 µl Pct Recovery = 119% Analysis Date = 09/06/17 SpikeMix = Abs 072417Pest3: 50 µl & Abs 071917Pest3: 50 µl Pct Recovery = 104% Analysis Date = 08/23/17 SpikeMix = Abs 071717Pest3: 50 µl & Abs 072417Pest3: 50 µl Pct Recovery = 77% Analysis Date = 07/11/17 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 91% Analysis Date = 06/24/17 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 88% Analysis Date = 03/01/17 SpikeMix = Abs 071816: 80 µl & Abs 072516: 80 µl Pct Recovery = 83% Analysis Date = 03/01/17 SpikeMix = Abs 071816: 80 µl & Abs 072516: 80 µl Pct Recovery = 110% Analysis Date = 01/18/17 SpikeMix = Spex Organics TS160511023: 80 µl & Abs 071816: 80 µl Pct Recovery = 103% Analysis Date = 01/17/17 SpikeMix = Spex Organics TS160511023: 80 µl & Abs 071816: 80 µl Pct Recovery = 78% Analysis Date = 12/13/16 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 96% Analysis Date = 12/13/16 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 77% Analysis Date = 08/21/16 SpikeMix = Abs 071816: 80 µl & Abs 072516: 80 µl Pct Recovery = 93% Analysis Date = 08/21/16 SpikeMix = Abs 071816: 80 µl & Abs 072516: 80 µl Pct Recovery = 99% Analysis Date = 05/06/16 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 89% Analysis Date = 05/06/16 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 87% Analysis Date = 02/17/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 92% Analysis Date = 02/17/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 84% Analysis Date = 02/17/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 82% Analysis Date = 07/28/17 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 96% Analysis Date = 06/07/17 SpikeMix = Abs 071216: 40 µl & Abs 071816: 40 µl Pct Recovery = 77% Analysis Date = 05/07/17 SpikeMix = Abs 071816: 40 µl & Abs 072516: 40 µl Pct Recovery = 100% Analysis Date = 01/10/17 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 106% Analysis Date = 01/10/17 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 100% Analysis Date = 11/12/16 SpikeMix = Abs 071816: 40 µl & Abs 072516: 40 µl Pct Recovery = 95% Analysis Date = 11/12/16 SpikeMix = Abs 071816: 40 µl & Abs 072516: 40 µl Pct Recovery = 100% Analysis Date = 11/08/16 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 77% Analysis Date = 11/08/16 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 93% Analysis Date = 09/07/16 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 92% Analysis Date = 09/07/16 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 101% Analysis Date = 08/30/16 SpikeMix = Abs 071216: 40 µl & Abs 071816: 40 µl Pct Recovery = 110% Analysis Date = 09/23/17 SpikeMix = Abs 071717Pest3: 20 µl & Abs 072417Pest3: 20 µl Pct Recovery = 125% Analysis Date = 08/27/17 SpikeMix = Abs 071917Pest3: 20 µl & Abs 072417Pest3: 20 µl Pct Recovery = 65% Analysis Date = 03/02/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 105% Analysis Date = 03/02/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 96% Analysis Date = 03/02/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 96% Analysis Date = 02/18/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 83% Analysis Date = 02/18/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 68% Analysis Date = 02/18/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 84% Analysis Date = 02/12/16 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 73% Analysis Date = 02/12/16 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 118% Analysis Date = 11/11/16 SpikeMix = Abs 071216: 10 µl & Abs 071816: 10 µl Pct Recovery = 166% Analysis Date = 11/11/16 SpikeMix = Abs 071216: 10 µl & Abs 071816: 10 µl Pct Recovery = 165% Analysis Date = 09/22/17 Pct Recovery = 96% Analysis Date = 09/20/17 Pct Recovery = 96% Analysis Date = 09/20/17 Pct Recovery = 96% Analysis Date = 09/17/17 Pct Recovery = 96% Analysis Date = 09/17/17 Pct Recovery = 96% Analysis Date = 09/14/17 Pct Recovery = 96% Analysis Date = 09/14/17 Pct Recovery = 96% Analysis Date = 09/11/17 Pct Recovery = 96% Analysis Date = 09/11/17 Pct Recovery = 96% Analysis Date = 09/08/17 Pct Recovery = 96% Analysis Date = 09/08/17 Pct Recovery = 96% Analysis Date = 09/05/17 Pct Recovery = 96% Analysis Date = 09/05/17 Pct Recovery = 96% Analysis Date = 09/02/17 Pct Recovery = 95% Analysis Date = 09/02/17 Pct Recovery = 95% Analysis Date = 08/30/17 Pct Recovery = 95% Analysis Date = 08/30/17 Pct Recovery = 95% Analysis Date = 08/27/17 Pct Recovery = 95% Analysis Date = 08/27/17 Pct Recovery = 95% Analysis Date = 08/24/17 Pct Recovery = 95% Analysis Date = 08/24/17 Pct Recovery = 95% Analysis Date = 08/21/17 Pct Recovery = 95% Analysis Date = 08/21/17 Pct Recovery = 95% Analysis Date = 08/18/17 Pct Recovery = 95% Analysis Date = 08/18/17 Pct Recovery = 95% Analysis Date = 08/15/17 Pct Recovery = 95% Analysis Date = 08/15/17 Pct Recovery = 95% Analysis Date = 08/12/17 Pct Recovery = 95% Analysis Date = 08/12/17 Pct Recovery = 95% Analysis Date = 08/09/17 Pct Recovery = 95% Analysis Date = 08/09/17 Pct Recovery = 95% Analysis Date = 08/06/17 Pct Recovery = 95% Analysis Date = 08/06/17 Pct Recovery = 95% Analysis Date = 08/03/17 Pct Recovery = 95% Analysis Date = 08/03/17 Pct Recovery = 95% Analysis Date = 07/31/17 Pct Recovery = 95% Analysis Date = 07/31/17 Pct Recovery = 95% Analysis Date = 07/29/17 Pct Recovery = 94% Analysis Date = 07/29/17 Pct Recovery = 94% Analysis Date = 07/26/17 Pct Recovery = 94% Analysis Date = 07/26/17 Pct Recovery = 94% Analysis Date = 07/23/17 Pct Recovery = 94% Analysis Date = 07/23/17 Pct Recovery = 94% Analysis Date = 07/20/17 Pct Recovery = 94% Analysis Date = 07/20/17 Pct Recovery = 94% Analysis Date = 07/17/17 Pct Recovery = 94% Analysis Date = 07/17/17 Pct Recovery = 94% Analysis Date = 07/14/17 Pct Recovery = 94% Analysis Date = 07/14/17 Pct Recovery = 94% Analysis Date = 07/11/17 Pct Recovery = 94% Analysis Date = 07/11/17 Pct Recovery = 94% Analysis Date = 07/08/17 Pct Recovery = 94% Analysis Date = 07/08/17 Pct Recovery = 94% Analysis Date = 07/05/17 Pct Recovery = 94% Analysis Date = 07/05/17 Pct Recovery = 94% Analysis Date = 07/02/17 Pct Recovery = 94% Analysis Date = 07/02/17 Pct Recovery = 94% Analysis Date = 06/29/17 Pct Recovery = 94% Analysis Date = 06/29/17 Pct Recovery = 94% Analysis Date = 06/26/17 Pct Recovery = 94% Analysis Date = 06/26/17 Pct Recovery = 94% Analysis Date = 06/23/17 Pct Recovery = 93% Analysis Date = 06/23/17 Pct Recovery = 93% Analysis Date = 06/20/17 Pct Recovery = 93% Analysis Date = 06/20/17 Pct Recovery = 93% Analysis Date = 06/17/17 Pct Recovery = 93% Analysis Date = 06/17/17 Pct Recovery = 93% Analysis Date = 06/14/17 Pct Recovery = 93% Analysis Date = 06/14/17 Pct Recovery = 93% Analysis Date = 06/11/17 Pct Recovery = 93% Analysis Date = 06/11/17 Pct Recovery = 93% Analysis Date = 06/08/17 Pct Recovery = 93% Analysis Date = 06/08/17 Pct Recovery = 93% Analysis Date = 06/06/17 Pct Recovery = 93% Analysis Date = 06/06/17 Pct Recovery = 93% Analysis Date = 06/03/17 Pct Recovery = 93% Analysis Date = 06/03/17 Pct Recovery = 93% Analysis Date = 05/31/17 Pct Recovery = 93% Analysis Date = 05/31/17 Pct Recovery = 93% Analysis Date = 05/28/17 Pct Recovery = 93% Analysis Date = 05/28/17 Pct Recovery = 93% Analysis Date = 05/25/17 Pct Recovery = 93% Analysis Date = 05/25/17 Pct Recovery = 93% Analysis Date = 05/22/17 Pct Recovery = 93% Analysis Date = 05/22/17 Pct Recovery = 93% Analysis Date = 05/19/17 Pct Recovery = 92% Analysis Date = 05/19/17 Pct Recovery = 92% Analysis Date = 05/16/17 Pct Recovery = 92% Analysis Date = 05/16/17 Pct Recovery = 92% Analysis Date = 05/13/17 Pct Recovery = 92% Analysis Date = 05/13/17 Pct Recovery = 92% Analysis Date = 05/10/17 Pct Recovery = 92% Analysis Date = 05/10/17 Pct Recovery = 92% Analysis Date = 05/07/17 Pct Recovery = 92% Analysis Date = 05/07/17 Pct Recovery = 92% Analysis Date = 05/04/17 Pct Recovery = 92% Analysis Date = 05/04/17 Pct Recovery = 92% Analysis Date = 05/01/17 Pct Recovery = 93% Analysis Date = 05/01/17 Pct Recovery = 93% Analysis Date = 04/28/17 Pct Recovery = 93% Analysis Date = 04/28/17 Pct Recovery = 93% Analysis Date = 04/25/17 Pct Recovery = 93% Analysis Date = 04/25/17 Pct Recovery = 93% Analysis Date = 04/22/17 Pct Recovery = 93% Analysis Date = 04/22/17 Pct Recovery = 93% Analysis Date = 04/19/17 Pct Recovery = 93% Analysis Date = 04/19/17 Pct Recovery = 93% Analysis Date = 04/16/17 Pct Recovery = 93% Analysis Date = 04/16/17 Pct Recovery = 93% Analysis Date = 04/14/17 Pct Recovery = 94% Analysis Date = 04/14/17 Pct Recovery = 94% Analysis Date = 04/11/17 Pct Recovery = 94% Analysis Date = 04/11/17 Pct Recovery = 94% Analysis Date = 04/08/17 Pct Recovery = 94% Analysis Date = 04/08/17 Pct Recovery = 94% Analysis Date = 04/05/17 Pct Recovery = 94% Analysis Date = 04/05/17 Pct Recovery = 94% Analysis Date = 04/02/17 Pct Recovery = 94% Analysis Date = 04/02/17 Pct Recovery = 94% Analysis Date = 03/30/17 Pct Recovery = 95% Analysis Date = 03/30/17 Pct Recovery = 95% Analysis Date = 03/27/17 Pct Recovery = 95% Analysis Date = 03/27/17 Pct Recovery = 95% Analysis Date = 03/24/17 Pct Recovery = 95% Analysis Date = 03/24/17 Pct Recovery = 95% Analysis Date = 03/21/17 Pct Recovery = 95% Analysis Date = 03/21/17 Pct Recovery = 95% Analysis Date = 03/18/17 Pct Recovery = 95% Analysis Date = 03/18/17 Pct Recovery = 95% Analysis Date = 03/15/17 Pct Recovery = 96% Analysis Date = 03/15/17 Pct Recovery = 96% Analysis Date = 03/12/17 Pct Recovery = 96% Analysis Date = 03/12/17 Pct Recovery = 96% Analysis Date = 03/09/17 Pct Recovery = 96% Analysis Date = 03/09/17 Pct Recovery = 96% Analysis Date = 03/06/17 Pct Recovery = 96% Analysis Date = 03/06/17 Pct Recovery = 96% Analysis Date = 03/03/17 Pct Recovery = 96% Analysis Date = 03/03/17 Pct Recovery = 96% Analysis Date = 02/28/17 Pct Recovery = 97% Analysis Date = 02/28/17 Pct Recovery = 97% Analysis Date = 02/25/17 Pct Recovery = 97% Analysis Date = 02/25/17 Pct Recovery = 97% Analysis Date = 02/22/17 Pct Recovery = 97% Analysis Date = 02/22/17 Pct Recovery = 97% Analysis Date = 02/20/17 Pct Recovery = 97% Analysis Date = 02/20/17 Pct Recovery = 97% Analysis Date = 02/17/17 Pct Recovery = 97% Analysis Date = 02/17/17 Pct Recovery = 97% Analysis Date = 02/14/17 Pct Recovery = 98% Analysis Date = 02/14/17 Pct Recovery = 98% Analysis Date = 02/11/17 Pct Recovery = 98% Analysis Date = 02/11/17 Pct Recovery = 98% Analysis Date = 02/08/17 Pct Recovery = 98% Analysis Date = 02/08/17 Pct Recovery = 98% Analysis Date = 02/05/17 Pct Recovery = 98% Analysis Date = 02/05/17 Pct Recovery = 98% Analysis Date = 02/02/17 Pct Recovery = 98% Analysis Date = 02/02/17 Pct Recovery = 98% Analysis Date = 01/30/17 Pct Recovery = 99% Analysis Date = 01/30/17 Pct Recovery = 99% Analysis Date = 01/27/17 Pct Recovery = 99% Analysis Date = 01/27/17 Pct Recovery = 99% Analysis Date = 01/24/17 Pct Recovery = 99% Analysis Date = 01/24/17 Pct Recovery = 99% Analysis Date = 01/21/17 Pct Recovery = 99% Analysis Date = 01/21/17 Pct Recovery = 99% Analysis Date = 01/18/17 Pct Recovery = 99% Analysis Date = 01/18/17 Pct Recovery = 99% Analysis Date = 01/15/17 Pct Recovery = 100% Analysis Date = 01/15/17 Pct Recovery = 100% Analysis Date = 01/12/17 Pct Recovery = 100% Analysis Date = 01/12/17 Pct Recovery = 100% Analysis Date = 01/09/17 Pct Recovery = 100% Analysis Date = 01/09/17 Pct Recovery = 100% Analysis Date = 01/06/17 Pct Recovery = 100% Analysis Date = 01/06/17 Pct Recovery = 100% Analysis Date = 01/03/17 Pct Recovery = 100% Analysis Date = 01/03/17 Pct Recovery = 100% Analysis Date = 12/31/16 Pct Recovery = 101% Analysis Date = 12/31/16 Pct Recovery = 101% Analysis Date = 12/29/16 Pct Recovery = 101% Analysis Date = 12/29/16 Pct Recovery = 101% Analysis Date = 12/26/16 Pct Recovery = 101% Analysis Date = 12/26/16 Pct Recovery = 101% Analysis Date = 12/23/16 Pct Recovery = 101% Analysis Date = 12/23/16 Pct Recovery = 101% Analysis Date = 12/20/16 Pct Recovery = 101% Analysis Date = 12/20/16 Pct Recovery = 101% Analysis Date = 12/17/16 Pct Recovery = 101% Analysis Date = 12/17/16 Pct Recovery = 101% Analysis Date = 12/14/16 Pct Recovery = 102% Analysis Date = 12/14/16 Pct Recovery = 102% Analysis Date = 12/11/16 Pct Recovery = 102% Analysis Date = 12/11/16 Pct Recovery = 102% Analysis Date = 12/08/16 Pct Recovery = 102% Analysis Date = 12/08/16 Pct Recovery = 102% Analysis Date = 12/05/16 Pct Recovery = 102% Analysis Date = 12/05/16 Pct Recovery = 102% Analysis Date = 12/02/16 Pct Recovery = 102% Analysis Date = 12/02/16 Pct Recovery = 102% Analysis Date = 11/29/16 Pct Recovery = 102% Analysis Date = 11/29/16 Pct Recovery = 102% Analysis Date = 11/26/16 Pct Recovery = 102% Analysis Date = 11/26/16 Pct Recovery = 102% Analysis Date = 11/23/16 Pct Recovery = 102% Analysis Date = 11/23/16 Pct Recovery = 102% Analysis Date = 11/20/16 Pct Recovery = 102% Analysis Date = 11/20/16 Pct Recovery = 102% Analysis Date = 11/17/16 Pct Recovery = 102% Analysis Date = 11/17/16 Pct Recovery = 102% Analysis Date = 11/14/16 Pct Recovery = 102% Analysis Date = 11/14/16 Pct Recovery = 102% Analysis Date = 11/11/16 Pct Recovery = 102% Analysis Date = 11/11/16 Pct Recovery = 102% Analysis Date = 11/08/16 Pct Recovery = 102% Analysis Date = 11/08/16 Pct Recovery = 102% Analysis Date = 11/05/16 Pct Recovery = 102% Analysis Date = 11/05/16 Pct Recovery = 102% Analysis Date = 11/03/16 Pct Recovery = 102% Analysis Date = 11/03/16 Pct Recovery = 102% Analysis Date = 10/31/16 Pct Recovery = 102% Analysis Date = 10/31/16 Pct Recovery = 102% Analysis Date = 10/28/16 Pct Recovery = 102% Analysis Date = 10/28/16 Pct Recovery = 102% Analysis Date = 10/25/16 Pct Recovery = 102% Analysis Date = 10/25/16 Pct Recovery = 102% Analysis Date = 10/22/16 Pct Recovery = 102% Analysis Date = 10/22/16 Pct Recovery = 102% Analysis Date = 10/19/16 Pct Recovery = 102% Analysis Date = 10/19/16 Pct Recovery = 102% Analysis Date = 10/16/16 Pct Recovery = 102% Analysis Date = 10/16/16 Pct Recovery = 102% Analysis Date = 10/13/16 Pct Recovery = 102% Analysis Date = 10/13/16 Pct Recovery = 102% Analysis Date = 10/10/16 Pct Recovery = 102% Analysis Date = 10/10/16 Pct Recovery = 102% Analysis Date = 10/07/16 Pct Recovery = 102% Analysis Date = 10/07/16 Pct Recovery = 102% Analysis Date = 10/04/16 Pct Recovery = 102% Analysis Date = 10/04/16 Pct Recovery = 102% Analysis Date = 10/01/16 Pct Recovery = 102% Analysis Date = 10/01/16 Pct Recovery = 102% Analysis Date = 09/28/16 Pct Recovery = 102% Analysis Date = 09/28/16 Pct Recovery = 102% Analysis Date = 09/25/16 Pct Recovery = 102% Analysis Date = 09/25/16 Pct Recovery = 102% Analysis Date = 09/22/16 Pct Recovery = 102% Analysis Date = 09/22/16 Pct Recovery = 102% Analysis Date = 09/19/16 Pct Recovery = 102% Analysis Date = 09/19/16 Pct Recovery = 102% Analysis Date = 09/16/16 Pct Recovery = 102% Analysis Date = 09/16/16 Pct Recovery = 102% Analysis Date = 09/13/16 Pct Recovery = 101% Analysis Date = 09/13/16 Pct Recovery = 101% Analysis Date = 09/11/16 Pct Recovery = 101% Analysis Date = 09/11/16 Pct Recovery = 101% Analysis Date = 09/08/16 Pct Recovery = 101% Analysis Date = 09/08/16 Pct Recovery = 101% Analysis Date = 09/05/16 Pct Recovery = 101% Analysis Date = 09/05/16 Pct Recovery = 101% Analysis Date = 09/02/16 Pct Recovery = 101% Analysis Date = 09/02/16 Pct Recovery = 101% Analysis Date = 08/30/16 Pct Recovery = 101% Analysis Date = 08/30/16 Pct Recovery = 101% Analysis Date = 08/27/16 Pct Recovery = 100% Analysis Date = 08/27/16 Pct Recovery = 100% Analysis Date = 08/24/16 Pct Recovery = 100% Analysis Date = 08/24/16 Pct Recovery = 100% Analysis Date = 08/21/16 Pct Recovery = 100% Analysis Date = 08/21/16 Pct Recovery = 100% Analysis Date = 08/18/16 Pct Recovery = 100% Analysis Date = 08/18/16 Pct Recovery = 100% Analysis Date = 08/15/16 Pct Recovery = 100% Analysis Date = 08/15/16 Pct Recovery = 100% Analysis Date = 08/12/16 Pct Recovery = 99% Analysis Date = 08/12/16 Pct Recovery = 99% Analysis Date = 08/09/16 Pct Recovery = 99% Analysis Date = 08/09/16 Pct Recovery = 99% Analysis Date = 08/06/16 Pct Recovery = 99% Analysis Date = 08/06/16 Pct Recovery = 99% Analysis Date = 08/03/16 Pct Recovery = 99% Analysis Date = 08/03/16 Pct Recovery = 99% Analysis Date = 07/31/16 Pct Recovery = 99% Analysis Date = 07/31/16 Pct Recovery = 99% Analysis Date = 07/28/16 Pct Recovery = 98% Analysis Date = 07/28/16 Pct Recovery = 98% Analysis Date = 07/25/16 Pct Recovery = 98% Analysis Date = 07/25/16 Pct Recovery = 98% Analysis Date = 07/22/16 Pct Recovery = 98% Analysis Date = 07/22/16 Pct Recovery = 98% Analysis Date = 07/20/16 Pct Recovery = 98% Analysis Date = 07/20/16 Pct Recovery = 98% Analysis Date = 07/17/16 Pct Recovery = 98% Analysis Date = 07/17/16 Pct Recovery = 98% Analysis Date = 07/14/16 Pct Recovery = 98% Analysis Date = 07/14/16 Pct Recovery = 98% Analysis Date = 07/11/16 Pct Recovery = 97% Analysis Date = 07/11/16 Pct Recovery = 97% Analysis Date = 07/08/16 Pct Recovery = 97% Analysis Date = 07/08/16 Pct Recovery = 97% Analysis Date = 07/05/16 Pct Recovery = 97% Analysis Date = 07/05/16 Pct Recovery = 97% Analysis Date = 07/02/16 Pct Recovery = 97% Analysis Date = 07/02/16 Pct Recovery = 97% Analysis Date = 06/29/16 Pct Recovery = 97% Analysis Date = 06/29/16 Pct Recovery = 97% Analysis Date = 06/26/16 Pct Recovery = 96% Analysis Date = 06/26/16 Pct Recovery = 96% Analysis Date = 06/23/16 Pct Recovery = 96% Analysis Date = 06/23/16 Pct Recovery = 96% Analysis Date = 06/20/16 Pct Recovery = 96% Analysis Date = 06/20/16 Pct Recovery = 96% Analysis Date = 06/17/16 Pct Recovery = 96% Analysis Date = 06/17/16 Pct Recovery = 96% Analysis Date = 06/14/16 Pct Recovery = 96% Analysis Date = 06/14/16 Pct Recovery = 96% Analysis Date = 06/11/16 Pct Recovery = 96% Analysis Date = 06/11/16 Pct Recovery = 96% Analysis Date = 06/08/16 Pct Recovery = 95% Analysis Date = 06/08/16 Pct Recovery = 95% Analysis Date = 06/05/16 Pct Recovery = 95% Analysis Date = 06/05/16 Pct Recovery = 95% Analysis Date = 06/02/16 Pct Recovery = 95% Analysis Date = 06/02/16 Pct Recovery = 95% Analysis Date = 05/30/16 Pct Recovery = 95% Analysis Date = 05/30/16 Pct Recovery = 95% Analysis Date = 05/28/16 Pct Recovery = 95% Analysis Date = 05/28/16 Pct Recovery = 95% Analysis Date = 05/25/16 Pct Recovery = 94% Analysis Date = 05/25/16 Pct Recovery = 94% Analysis Date = 05/22/16 Pct Recovery = 94% Analysis Date = 05/22/16 Pct Recovery = 94% Analysis Date = 05/19/16 Pct Recovery = 94% Analysis Date = 05/19/16 Pct Recovery = 94% Analysis Date = 05/16/16 Pct Recovery = 94% Analysis Date = 05/16/16 Pct Recovery = 94% Analysis Date = 05/13/16 Pct Recovery = 94% Analysis Date = 05/13/16 Pct Recovery = 94% Analysis Date = 05/10/16 Pct Recovery = 93% Analysis Date = 05/10/16 Pct Recovery = 93% Analysis Date = 05/07/16 Pct Recovery = 93% Analysis Date = 05/07/16 Pct Recovery = 93% Analysis Date = 05/04/16 Pct Recovery = 93% Analysis Date = 05/04/16 Pct Recovery = 93% Analysis Date = 05/01/16 Pct Recovery = 93% Analysis Date = 05/01/16 Pct Recovery = 93% Analysis Date = 04/28/16 Pct Recovery = 93% Analysis Date = 04/28/16 Pct Recovery = 93% Analysis Date = 04/25/16 Pct Recovery = 93% Analysis Date = 04/25/16 Pct Recovery = 93% Analysis Date = 04/22/16 Pct Recovery = 92% Analysis Date = 04/22/16 Pct Recovery = 92% Analysis Date = 04/19/16 Pct Recovery = 92% Analysis Date = 04/19/16 Pct Recovery = 92% Analysis Date = 04/16/16 Pct Recovery = 92% Analysis Date = 04/16/16 Pct Recovery = 92% Analysis Date = 04/13/16 Pct Recovery = 92% Analysis Date = 04/13/16 Pct Recovery = 92% Analysis Date = 04/10/16 Pct Recovery = 92% Analysis Date = 04/10/16 Pct Recovery = 92% Analysis Date = 04/07/16 Pct Recovery = 91% Analysis Date = 04/07/16 Pct Recovery = 91% Analysis Date = 04/05/16 Pct Recovery = 91% Analysis Date = 04/05/16 Pct Recovery = 91% Analysis Date = 04/02/16 Pct Recovery = 91% Analysis Date = 04/02/16 Pct Recovery = 91% Analysis Date = 03/30/16 Pct Recovery = 91% Analysis Date = 03/30/16 Pct Recovery = 91% Analysis Date = 03/27/16 Pct Recovery = 91% Analysis Date = 03/27/16 Pct Recovery = 91% Analysis Date = 03/24/16 Pct Recovery = 91% Analysis Date = 03/24/16 Pct Recovery = 91% Analysis Date = 03/21/16 Pct Recovery = 90% Analysis Date = 03/21/16 Pct Recovery = 90% Analysis Date = 03/18/16 Pct Recovery = 90% Analysis Date = 03/18/16 Pct Recovery = 90% Analysis Date = 03/15/16 Pct Recovery = 90% Analysis Date = 03/15/16 Pct Recovery = 90% Analysis Date = 03/12/16 Pct Recovery = 90% Analysis Date = 03/12/16 Pct Recovery = 90% Analysis Date = 03/09/16 Pct Recovery = 90% Analysis Date = 03/09/16 Pct Recovery = 90% Analysis Date = 03/06/16 Pct Recovery = 89% Analysis Date = 03/06/16 Pct Recovery = 89% Analysis Date = 03/03/16 Pct Recovery = 89% Analysis Date = 03/03/16 Pct Recovery = 89% Analysis Date = 02/29/16 Pct Recovery = 89% Analysis Date = 02/29/16 Pct Recovery = 89% Analysis Date = 02/26/16 Pct Recovery = 89% Analysis Date = 02/26/16 Pct Recovery = 89% Analysis Date = 02/23/16 Pct Recovery = 89% Analysis Date = 02/23/16 Pct Recovery = 89% Analysis Date = 02/20/16 Pct Recovery = 89% Analysis Date = 02/20/16 Pct Recovery = 89% Analysis Date = 02/17/16 Pct Recovery = 88% Analysis Date = 02/17/16 Pct Recovery = 88% Analysis Date = 02/14/16 Pct Recovery = 88% Analysis Date = 02/14/16 Pct Recovery = 88% Analysis Date = 02/12/16 Pct Recovery = 88% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DEMETHYL NORFLURAZON

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 166% 1% 166% 1%
>= Reporting Level 41 93% 13% 93% 12%
Total 43 96% 20% 93% 14%

Sample Statistics
DEMETHYL NORFLURAZON

Characteristic N % % Basis
Plotted 43 96% Spiked
Estimated Values 2 4% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 45 .  
False Negatives 2 4% 2 out of 45
Not Spiked 74 .  
False Positives 0 0% 0 out of 72