OBSP Determination:
DEMETHYL FLUOMETURON
METHOD: 2437 , TESTIDCODE: 68591LCM60

Analysis Date = 07/12/17 SpikeMix = Spex Organics TS160511023: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 373% Analysis Date = 05/17/17 SpikeMix = Spex Organics TS160511023: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 361% Analysis Date = 09/22/17 SpikeMix = Abs 071917Pest3: 80 µl & Abs 072417Pest3: 80 µl Pct Recovery = 84% Analysis Date = 10/04/17 SpikeMix = Abs 071917Pest3: 50 µl & Abs 071717Pest3: 50 µl Pct Recovery = 105% Analysis Date = 09/15/17 SpikeMix = Abs 071917Pest3: 50 µl & Abs 072417Pest3: 50 µl Pct Recovery = 95% Analysis Date = 09/06/17 SpikeMix = Abs 072417Pest3: 50 µl & Abs 071917Pest3: 50 µl Pct Recovery = 97% Analysis Date = 03/10/17 SpikeMix = Abs 072516: 100 µl & Abs 071216: 100 µl Pct Recovery = 99% Analysis Date = 03/10/17 SpikeMix = Abs 072516: 100 µl & Abs 071216: 100 µl Pct Recovery = 98% Analysis Date = 09/29/16 SpikeMix = ChemService 5154100: 100 µl & Abs 072516: 100 µl Pct Recovery = 85% Analysis Date = 09/29/16 SpikeMix = ChemService 5154100: 100 µl & Abs 072516: 100 µl Pct Recovery = 93% Analysis Date = 08/24/16 SpikeMix = Abs 072516: 100 µl & Abs 071216: 100 µl Pct Recovery = 107% Analysis Date = 08/24/16 SpikeMix = Abs 072516: 100 µl & Abs 071216: 100 µl Pct Recovery = 103% Analysis Date = 02/01/17 SpikeMix = Spex Organics TS160603008: 100 µl & Spex Organics TS160511023: 100 µl Pct Recovery = 98% Analysis Date = 02/01/17 SpikeMix = Spex Organics TS160603008: 100 µl & Spex Organics TS160511023: 100 µl Pct Recovery = 113% Analysis Date = 01/24/17 SpikeMix = ChemService 5154100: 100 µl & Spex Organics TS160603008: 100 µl Pct Recovery = 108% Analysis Date = 01/24/17 SpikeMix = ChemService 5154100: 100 µl & Spex Organics TS160603008: 100 µl Pct Recovery = 103% Analysis Date = 07/19/17 SpikeMix = Spex Organics TS160511023: 80 µl & Abs 072516: 80 µl Pct Recovery = 121% Analysis Date = 06/21/17 SpikeMix = ChemService 5154100: 80 µl & Abs 072516: 80 µl Pct Recovery = 103% Analysis Date = 03/01/17 SpikeMix = Abs 071816: 80 µl & Abs 072516: 80 µl Pct Recovery = 86% Analysis Date = 03/01/17 SpikeMix = Abs 071816: 80 µl & Abs 072516: 80 µl Pct Recovery = 81% Analysis Date = 09/13/16 SpikeMix = Abs 072516: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 93% Analysis Date = 09/13/16 SpikeMix = Abs 072516: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 79% Analysis Date = 08/21/16 SpikeMix = Abs 071816: 80 µl & Abs 072516: 80 µl Pct Recovery = 83% Analysis Date = 08/21/16 SpikeMix = Abs 071816: 80 µl & Abs 072516: 80 µl Pct Recovery = 88% Analysis Date = 11/22/16 SpikeMix = Spex Organics TS160603008: 80 µl & Abs 071216: 80 µl Pct Recovery = 118% Analysis Date = 11/22/16 SpikeMix = Spex Organics TS160603008: 80 µl & Abs 071216: 80 µl Pct Recovery = 81% Analysis Date = 07/12/16 SpikeMix = Spex Organics TS160603008: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 98% Analysis Date = 07/12/16 SpikeMix = Spex Organics TS160603008: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 99% Analysis Date = 10/11/17 SpikeMix = Abs 071917Pest3: 20 µl & Abs 071717Pest3: 20 µl Pct Recovery = 91% Analysis Date = 08/27/17 SpikeMix = Abs 071917Pest3: 20 µl & Abs 072417Pest3: 20 µl Pct Recovery = 139% Analysis Date = 08/08/17 SpikeMix = Abs 071917Pest3: 20 µl & Abs 071717Pest3: 20 µl Pct Recovery = 121% Analysis Date = 04/20/16 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 77% Analysis Date = 04/20/16 SpikeMix = ERA 0406-15-05: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 79% Analysis Date = 07/08/17 SpikeMix = Abs 071216: 40 µl & Abs 072516: 40 µl Pct Recovery = 109% Analysis Date = 05/25/17 SpikeMix = ChemService 5154100: 40 µl & Abs 072516: 40 µl Pct Recovery = 92% Analysis Date = 05/07/17 SpikeMix = Abs 071816: 40 µl & Abs 072516: 40 µl Pct Recovery = 79% Analysis Date = 01/04/17 SpikeMix = Abs 072516: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 98% Analysis Date = 01/04/17 SpikeMix = Abs 072516: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 102% Analysis Date = 11/17/16 SpikeMix = ChemService 5154100: 40 µl & Abs 072516: 40 µl Pct Recovery = 88% Analysis Date = 11/17/16 SpikeMix = ChemService 5154100: 40 µl & Abs 072516: 40 µl Pct Recovery = 111% Analysis Date = 11/12/16 SpikeMix = Abs 071816: 40 µl & Abs 072516: 40 µl Pct Recovery = 97% Analysis Date = 11/12/16 SpikeMix = Abs 071816: 40 µl & Abs 072516: 40 µl Pct Recovery = 92% Analysis Date = 11/09/16 SpikeMix = Abs 072516: 40 µl & Abs 071216: 40 µl Pct Recovery = 113% Analysis Date = 11/08/16 SpikeMix = Abs 072516: 40 µl & Abs 071216: 40 µl Pct Recovery = 82% Analysis Date = 06/05/17 SpikeMix = Spex Organics TS160511023: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 173% Analysis Date = 01/10/17 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 131% Analysis Date = 01/10/17 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 112% Analysis Date = 10/06/16 SpikeMix = Spex Organics TS160603008: 40 µl & Abs 071216: 40 µl Pct Recovery = 96% Analysis Date = 10/06/16 SpikeMix = Spex Organics TS160603008: 40 µl & Abs 071216: 40 µl Pct Recovery = 115% Analysis Date = 09/07/16 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 68% Analysis Date = 09/07/16 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 87% Analysis Date = 08/03/16 SpikeMix = Spex Organics TS160603008: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 79% Analysis Date = 08/03/16 SpikeMix = Spex Organics TS160603008: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 104% Analysis Date = 07/29/16 SpikeMix = ChemService 5154100: 40 µl & ChemService 5154200: 40 µl & Spex Organics TS160603 Pct Recovery = 115% Analysis Date = 07/29/16 SpikeMix = ChemService 5154100: 40 µl & ChemService 5154200: 40 µl & Spex Organics TS160603 Pct Recovery = 116% Analysis Date = 02/24/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 105% Analysis Date = 02/24/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 115% Analysis Date = 02/24/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 117% Analysis Date = 02/19/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 96% Analysis Date = 02/19/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 65% Analysis Date = 02/19/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 99% Analysis Date = 10/11/17 Pct Recovery = 131% Analysis Date = 10/08/17 Pct Recovery = 131% Analysis Date = 10/08/17 Pct Recovery = 131% Analysis Date = 10/05/17 Pct Recovery = 131% Analysis Date = 10/05/17 Pct Recovery = 131% Analysis Date = 10/02/17 Pct Recovery = 131% Analysis Date = 10/02/17 Pct Recovery = 131% Analysis Date = 09/29/17 Pct Recovery = 131% Analysis Date = 09/29/17 Pct Recovery = 131% Analysis Date = 09/26/17 Pct Recovery = 131% Analysis Date = 09/26/17 Pct Recovery = 131% Analysis Date = 09/23/17 Pct Recovery = 131% Analysis Date = 09/23/17 Pct Recovery = 131% Analysis Date = 09/20/17 Pct Recovery = 131% Analysis Date = 09/20/17 Pct Recovery = 131% Analysis Date = 09/17/17 Pct Recovery = 131% Analysis Date = 09/17/17 Pct Recovery = 131% Analysis Date = 09/14/17 Pct Recovery = 132% Analysis Date = 09/14/17 Pct Recovery = 132% Analysis Date = 09/11/17 Pct Recovery = 132% Analysis Date = 09/11/17 Pct Recovery = 132% Analysis Date = 09/08/17 Pct Recovery = 132% Analysis Date = 09/08/17 Pct Recovery = 132% Analysis Date = 09/05/17 Pct Recovery = 132% Analysis Date = 09/05/17 Pct Recovery = 132% Analysis Date = 09/02/17 Pct Recovery = 132% Analysis Date = 09/02/17 Pct Recovery = 132% Analysis Date = 08/30/17 Pct Recovery = 132% Analysis Date = 08/30/17 Pct Recovery = 132% Analysis Date = 08/27/17 Pct Recovery = 132% Analysis Date = 08/27/17 Pct Recovery = 132% Analysis Date = 08/24/17 Pct Recovery = 132% Analysis Date = 08/24/17 Pct Recovery = 132% Analysis Date = 08/21/17 Pct Recovery = 132% Analysis Date = 08/21/17 Pct Recovery = 132% Analysis Date = 08/18/17 Pct Recovery = 132% Analysis Date = 08/18/17 Pct Recovery = 132% Analysis Date = 08/15/17 Pct Recovery = 132% Analysis Date = 08/15/17 Pct Recovery = 132% Analysis Date = 08/12/17 Pct Recovery = 132% Analysis Date = 08/12/17 Pct Recovery = 132% Analysis Date = 08/09/17 Pct Recovery = 132% Analysis Date = 08/09/17 Pct Recovery = 132% Analysis Date = 08/06/17 Pct Recovery = 132% Analysis Date = 08/06/17 Pct Recovery = 132% Analysis Date = 08/03/17 Pct Recovery = 132% Analysis Date = 08/03/17 Pct Recovery = 132% Analysis Date = 07/31/17 Pct Recovery = 132% Analysis Date = 07/31/17 Pct Recovery = 132% Analysis Date = 07/28/17 Pct Recovery = 132% Analysis Date = 07/28/17 Pct Recovery = 132% Analysis Date = 07/25/17 Pct Recovery = 132% Analysis Date = 07/25/17 Pct Recovery = 132% Analysis Date = 07/22/17 Pct Recovery = 132% Analysis Date = 07/22/17 Pct Recovery = 132% Analysis Date = 07/19/17 Pct Recovery = 132% Analysis Date = 07/19/17 Pct Recovery = 132% Analysis Date = 07/16/17 Pct Recovery = 132% Analysis Date = 07/16/17 Pct Recovery = 132% Analysis Date = 07/13/17 Pct Recovery = 132% Analysis Date = 07/13/17 Pct Recovery = 132% Analysis Date = 07/10/17 Pct Recovery = 132% Analysis Date = 07/10/17 Pct Recovery = 132% Analysis Date = 07/07/17 Pct Recovery = 132% Analysis Date = 07/07/17 Pct Recovery = 132% Analysis Date = 07/04/17 Pct Recovery = 132% Analysis Date = 07/04/17 Pct Recovery = 132% Analysis Date = 07/01/17 Pct Recovery = 132% Analysis Date = 07/01/17 Pct Recovery = 132% Analysis Date = 06/28/17 Pct Recovery = 132% Analysis Date = 06/28/17 Pct Recovery = 132% Analysis Date = 06/25/17 Pct Recovery = 132% Analysis Date = 06/25/17 Pct Recovery = 132% Analysis Date = 06/22/17 Pct Recovery = 132% Analysis Date = 06/22/17 Pct Recovery = 132% Analysis Date = 06/19/17 Pct Recovery = 132% Analysis Date = 06/19/17 Pct Recovery = 132% Analysis Date = 06/16/17 Pct Recovery = 132% Analysis Date = 06/16/17 Pct Recovery = 132% Analysis Date = 06/13/17 Pct Recovery = 132% Analysis Date = 06/13/17 Pct Recovery = 132% Analysis Date = 06/10/17 Pct Recovery = 132% Analysis Date = 06/10/17 Pct Recovery = 132% Analysis Date = 06/07/17 Pct Recovery = 132% Analysis Date = 06/07/17 Pct Recovery = 132% Analysis Date = 06/04/17 Pct Recovery = 132% Analysis Date = 06/04/17 Pct Recovery = 132% Analysis Date = 06/01/17 Pct Recovery = 131% Analysis Date = 06/01/17 Pct Recovery = 131% Analysis Date = 05/29/17 Pct Recovery = 131% Analysis Date = 05/29/17 Pct Recovery = 131% Analysis Date = 05/26/17 Pct Recovery = 131% Analysis Date = 05/26/17 Pct Recovery = 131% Analysis Date = 05/23/17 Pct Recovery = 131% Analysis Date = 05/23/17 Pct Recovery = 131% Analysis Date = 05/20/17 Pct Recovery = 131% Analysis Date = 05/20/17 Pct Recovery = 131% Analysis Date = 05/17/17 Pct Recovery = 130% Analysis Date = 05/17/17 Pct Recovery = 130% Analysis Date = 05/14/17 Pct Recovery = 130% Analysis Date = 05/14/17 Pct Recovery = 130% Analysis Date = 05/11/17 Pct Recovery = 130% Analysis Date = 05/11/17 Pct Recovery = 130% Analysis Date = 05/08/17 Pct Recovery = 130% Analysis Date = 05/08/17 Pct Recovery = 130% Analysis Date = 05/05/17 Pct Recovery = 129% Analysis Date = 05/05/17 Pct Recovery = 129% Analysis Date = 05/02/17 Pct Recovery = 129% Analysis Date = 05/02/17 Pct Recovery = 129% Analysis Date = 04/29/17 Pct Recovery = 129% Analysis Date = 04/29/17 Pct Recovery = 129% Analysis Date = 04/26/17 Pct Recovery = 129% Analysis Date = 04/26/17 Pct Recovery = 129% Analysis Date = 04/23/17 Pct Recovery = 129% Analysis Date = 04/23/17 Pct Recovery = 129% Analysis Date = 04/20/17 Pct Recovery = 128% Analysis Date = 04/20/17 Pct Recovery = 128% Analysis Date = 04/17/17 Pct Recovery = 128% Analysis Date = 04/17/17 Pct Recovery = 128% Analysis Date = 04/14/17 Pct Recovery = 128% Analysis Date = 04/14/17 Pct Recovery = 128% Analysis Date = 04/11/17 Pct Recovery = 128% Analysis Date = 04/11/17 Pct Recovery = 128% Analysis Date = 04/08/17 Pct Recovery = 127% Analysis Date = 04/08/17 Pct Recovery = 127% Analysis Date = 04/05/17 Pct Recovery = 127% Analysis Date = 04/05/17 Pct Recovery = 127% Analysis Date = 04/02/17 Pct Recovery = 127% Analysis Date = 04/02/17 Pct Recovery = 127% Analysis Date = 03/30/17 Pct Recovery = 127% Analysis Date = 03/30/17 Pct Recovery = 127% Analysis Date = 03/27/17 Pct Recovery = 127% Analysis Date = 03/27/17 Pct Recovery = 127% Analysis Date = 03/24/17 Pct Recovery = 126% Analysis Date = 03/24/17 Pct Recovery = 126% Analysis Date = 03/21/17 Pct Recovery = 126% Analysis Date = 03/21/17 Pct Recovery = 126% Analysis Date = 03/18/17 Pct Recovery = 126% Analysis Date = 03/18/17 Pct Recovery = 126% Analysis Date = 03/15/17 Pct Recovery = 126% Analysis Date = 03/15/17 Pct Recovery = 126% Analysis Date = 03/12/17 Pct Recovery = 125% Analysis Date = 03/12/17 Pct Recovery = 125% Analysis Date = 03/09/17 Pct Recovery = 125% Analysis Date = 03/09/17 Pct Recovery = 125% Analysis Date = 03/06/17 Pct Recovery = 124% Analysis Date = 03/06/17 Pct Recovery = 124% Analysis Date = 03/03/17 Pct Recovery = 122% Analysis Date = 03/03/17 Pct Recovery = 122% Analysis Date = 02/28/17 Pct Recovery = 121% Analysis Date = 02/28/17 Pct Recovery = 121% Analysis Date = 02/25/17 Pct Recovery = 120% Analysis Date = 02/25/17 Pct Recovery = 120% Analysis Date = 02/22/17 Pct Recovery = 119% Analysis Date = 02/22/17 Pct Recovery = 119% Analysis Date = 02/19/17 Pct Recovery = 117% Analysis Date = 02/19/17 Pct Recovery = 117% Analysis Date = 02/16/17 Pct Recovery = 116% Analysis Date = 02/16/17 Pct Recovery = 116% Analysis Date = 02/13/17 Pct Recovery = 115% Analysis Date = 02/13/17 Pct Recovery = 115% Analysis Date = 02/10/17 Pct Recovery = 113% Analysis Date = 02/10/17 Pct Recovery = 113% Analysis Date = 02/07/17 Pct Recovery = 112% Analysis Date = 02/07/17 Pct Recovery = 112% Analysis Date = 02/04/17 Pct Recovery = 111% Analysis Date = 02/04/17 Pct Recovery = 111% Analysis Date = 02/01/17 Pct Recovery = 110% Analysis Date = 02/01/17 Pct Recovery = 110% Analysis Date = 01/29/17 Pct Recovery = 108% Analysis Date = 01/29/17 Pct Recovery = 108% Analysis Date = 01/26/17 Pct Recovery = 107% Analysis Date = 01/26/17 Pct Recovery = 107% Analysis Date = 01/23/17 Pct Recovery = 106% Analysis Date = 01/23/17 Pct Recovery = 106% Analysis Date = 01/20/17 Pct Recovery = 105% Analysis Date = 01/20/17 Pct Recovery = 105% Analysis Date = 01/17/17 Pct Recovery = 104% Analysis Date = 01/17/17 Pct Recovery = 104% Analysis Date = 01/14/17 Pct Recovery = 104% Analysis Date = 01/14/17 Pct Recovery = 104% Analysis Date = 01/11/17 Pct Recovery = 103% Analysis Date = 01/11/17 Pct Recovery = 103% Analysis Date = 01/08/17 Pct Recovery = 102% Analysis Date = 01/08/17 Pct Recovery = 102% Analysis Date = 01/05/17 Pct Recovery = 101% Analysis Date = 01/05/17 Pct Recovery = 101% Analysis Date = 01/02/17 Pct Recovery = 101% Analysis Date = 01/02/17 Pct Recovery = 101% Analysis Date = 12/30/16 Pct Recovery = 101% Analysis Date = 12/30/16 Pct Recovery = 101% Analysis Date = 12/27/16 Pct Recovery = 101% Analysis Date = 12/27/16 Pct Recovery = 101% Analysis Date = 12/24/16 Pct Recovery = 101% Analysis Date = 12/24/16 Pct Recovery = 101% Analysis Date = 12/21/16 Pct Recovery = 101% Analysis Date = 12/21/16 Pct Recovery = 101% Analysis Date = 12/18/16 Pct Recovery = 101% Analysis Date = 12/18/16 Pct Recovery = 101% Analysis Date = 12/15/16 Pct Recovery = 101% Analysis Date = 12/15/16 Pct Recovery = 101% Analysis Date = 12/12/16 Pct Recovery = 100% Analysis Date = 12/12/16 Pct Recovery = 100% Analysis Date = 12/09/16 Pct Recovery = 100% Analysis Date = 12/09/16 Pct Recovery = 100% Analysis Date = 12/06/16 Pct Recovery = 100% Analysis Date = 12/06/16 Pct Recovery = 100% Analysis Date = 12/03/16 Pct Recovery = 100% Analysis Date = 12/03/16 Pct Recovery = 100% Analysis Date = 11/30/16 Pct Recovery = 100% Analysis Date = 11/30/16 Pct Recovery = 100% Analysis Date = 11/27/16 Pct Recovery = 100% Analysis Date = 11/27/16 Pct Recovery = 100% Analysis Date = 11/24/16 Pct Recovery = 100% Analysis Date = 11/24/16 Pct Recovery = 100% Analysis Date = 11/21/16 Pct Recovery = 100% Analysis Date = 11/21/16 Pct Recovery = 100% Analysis Date = 11/18/16 Pct Recovery = 100% Analysis Date = 11/18/16 Pct Recovery = 100% Analysis Date = 11/15/16 Pct Recovery = 99% Analysis Date = 11/15/16 Pct Recovery = 99% Analysis Date = 11/12/16 Pct Recovery = 99% Analysis Date = 11/12/16 Pct Recovery = 99% Analysis Date = 11/09/16 Pct Recovery = 99% Analysis Date = 11/09/16 Pct Recovery = 99% Analysis Date = 11/06/16 Pct Recovery = 99% Analysis Date = 11/06/16 Pct Recovery = 99% Analysis Date = 11/03/16 Pct Recovery = 99% Analysis Date = 11/03/16 Pct Recovery = 99% Analysis Date = 10/31/16 Pct Recovery = 98% Analysis Date = 10/31/16 Pct Recovery = 98% Analysis Date = 10/28/16 Pct Recovery = 98% Analysis Date = 10/28/16 Pct Recovery = 98% Analysis Date = 10/25/16 Pct Recovery = 98% Analysis Date = 10/25/16 Pct Recovery = 98% Analysis Date = 10/22/16 Pct Recovery = 98% Analysis Date = 10/22/16 Pct Recovery = 98% Analysis Date = 10/19/16 Pct Recovery = 98% Analysis Date = 10/19/16 Pct Recovery = 98% Analysis Date = 10/16/16 Pct Recovery = 97% Analysis Date = 10/16/16 Pct Recovery = 97% Analysis Date = 10/13/16 Pct Recovery = 97% Analysis Date = 10/13/16 Pct Recovery = 97% Analysis Date = 10/10/16 Pct Recovery = 97% Analysis Date = 10/10/16 Pct Recovery = 97% Analysis Date = 10/07/16 Pct Recovery = 97% Analysis Date = 10/07/16 Pct Recovery = 97% Analysis Date = 10/04/16 Pct Recovery = 97% Analysis Date = 10/04/16 Pct Recovery = 97% Analysis Date = 10/01/16 Pct Recovery = 97% Analysis Date = 10/01/16 Pct Recovery = 97% Analysis Date = 09/28/16 Pct Recovery = 96% Analysis Date = 09/28/16 Pct Recovery = 96% Analysis Date = 09/25/16 Pct Recovery = 96% Analysis Date = 09/25/16 Pct Recovery = 96% Analysis Date = 09/22/16 Pct Recovery = 96% Analysis Date = 09/22/16 Pct Recovery = 96% Analysis Date = 09/19/16 Pct Recovery = 96% Analysis Date = 09/19/16 Pct Recovery = 96% Analysis Date = 09/16/16 Pct Recovery = 96% Analysis Date = 09/16/16 Pct Recovery = 96% Analysis Date = 09/13/16 Pct Recovery = 96% Analysis Date = 09/13/16 Pct Recovery = 96% Analysis Date = 09/10/16 Pct Recovery = 96% Analysis Date = 09/10/16 Pct Recovery = 96% Analysis Date = 09/07/16 Pct Recovery = 96% Analysis Date = 09/07/16 Pct Recovery = 96% Analysis Date = 09/04/16 Pct Recovery = 96% Analysis Date = 09/04/16 Pct Recovery = 96% Analysis Date = 09/01/16 Pct Recovery = 95% Analysis Date = 09/01/16 Pct Recovery = 95% Analysis Date = 08/29/16 Pct Recovery = 95% Analysis Date = 08/29/16 Pct Recovery = 95% Analysis Date = 08/26/16 Pct Recovery = 95% Analysis Date = 08/26/16 Pct Recovery = 95% Analysis Date = 08/23/16 Pct Recovery = 95% Analysis Date = 08/23/16 Pct Recovery = 95% Analysis Date = 08/20/16 Pct Recovery = 95% Analysis Date = 08/20/16 Pct Recovery = 95% Analysis Date = 08/17/16 Pct Recovery = 95% Analysis Date = 08/17/16 Pct Recovery = 95% Analysis Date = 08/14/16 Pct Recovery = 95% Analysis Date = 08/14/16 Pct Recovery = 95% Analysis Date = 08/11/16 Pct Recovery = 95% Analysis Date = 08/11/16 Pct Recovery = 95% Analysis Date = 08/08/16 Pct Recovery = 94% Analysis Date = 08/08/16 Pct Recovery = 94% Analysis Date = 08/05/16 Pct Recovery = 94% Analysis Date = 08/05/16 Pct Recovery = 94% Analysis Date = 08/02/16 Pct Recovery = 94% Analysis Date = 08/02/16 Pct Recovery = 94% Analysis Date = 07/30/16 Pct Recovery = 94% Analysis Date = 07/30/16 Pct Recovery = 94% Analysis Date = 07/27/16 Pct Recovery = 94% Analysis Date = 07/27/16 Pct Recovery = 94% Analysis Date = 07/24/16 Pct Recovery = 94% Analysis Date = 07/24/16 Pct Recovery = 94% Analysis Date = 07/21/16 Pct Recovery = 94% Analysis Date = 07/21/16 Pct Recovery = 94% Analysis Date = 07/18/16 Pct Recovery = 94% Analysis Date = 07/18/16 Pct Recovery = 94% Analysis Date = 07/15/16 Pct Recovery = 94% Analysis Date = 07/15/16 Pct Recovery = 94% Analysis Date = 07/12/16 Pct Recovery = 94% Analysis Date = 07/12/16 Pct Recovery = 94% Analysis Date = 07/09/16 Pct Recovery = 94% Analysis Date = 07/09/16 Pct Recovery = 94% Analysis Date = 07/06/16 Pct Recovery = 94% Analysis Date = 07/06/16 Pct Recovery = 94% Analysis Date = 07/03/16 Pct Recovery = 94% Analysis Date = 07/03/16 Pct Recovery = 94% Analysis Date = 06/30/16 Pct Recovery = 94% Analysis Date = 06/30/16 Pct Recovery = 94% Analysis Date = 06/27/16 Pct Recovery = 94% Analysis Date = 06/27/16 Pct Recovery = 94% Analysis Date = 06/24/16 Pct Recovery = 94% Analysis Date = 06/24/16 Pct Recovery = 94% Analysis Date = 06/21/16 Pct Recovery = 95% Analysis Date = 06/21/16 Pct Recovery = 95% Analysis Date = 06/18/16 Pct Recovery = 95% Analysis Date = 06/18/16 Pct Recovery = 95% Analysis Date = 06/15/16 Pct Recovery = 95% Analysis Date = 06/15/16 Pct Recovery = 95% Analysis Date = 06/12/16 Pct Recovery = 95% Analysis Date = 06/12/16 Pct Recovery = 95% Analysis Date = 06/09/16 Pct Recovery = 95% Analysis Date = 06/09/16 Pct Recovery = 95% Analysis Date = 06/06/16 Pct Recovery = 95% Analysis Date = 06/06/16 Pct Recovery = 95% Analysis Date = 06/03/16 Pct Recovery = 95% Analysis Date = 06/03/16 Pct Recovery = 95% Analysis Date = 05/31/16 Pct Recovery = 95% Analysis Date = 05/31/16 Pct Recovery = 95% Analysis Date = 05/28/16 Pct Recovery = 95% Analysis Date = 05/28/16 Pct Recovery = 95% Analysis Date = 05/25/16 Pct Recovery = 95% Analysis Date = 05/25/16 Pct Recovery = 95% Analysis Date = 05/22/16 Pct Recovery = 95% Analysis Date = 05/22/16 Pct Recovery = 95% Analysis Date = 05/19/16 Pct Recovery = 95% Analysis Date = 05/19/16 Pct Recovery = 95% Analysis Date = 05/16/16 Pct Recovery = 95% Analysis Date = 05/16/16 Pct Recovery = 95% Analysis Date = 05/13/16 Pct Recovery = 95% Analysis Date = 05/13/16 Pct Recovery = 95% Analysis Date = 05/10/16 Pct Recovery = 95% Analysis Date = 05/10/16 Pct Recovery = 95% Analysis Date = 05/07/16 Pct Recovery = 95% Analysis Date = 05/07/16 Pct Recovery = 95% Analysis Date = 05/04/16 Pct Recovery = 95% Analysis Date = 05/04/16 Pct Recovery = 95% Analysis Date = 05/01/16 Pct Recovery = 95% Analysis Date = 05/01/16 Pct Recovery = 95% Analysis Date = 04/28/16 Pct Recovery = 95% Analysis Date = 04/28/16 Pct Recovery = 95% Analysis Date = 04/25/16 Pct Recovery = 96% Analysis Date = 04/25/16 Pct Recovery = 96% Analysis Date = 04/22/16 Pct Recovery = 96% Analysis Date = 04/22/16 Pct Recovery = 96% Analysis Date = 04/19/16 Pct Recovery = 96% Analysis Date = 04/19/16 Pct Recovery = 96% Analysis Date = 04/16/16 Pct Recovery = 96% Analysis Date = 04/16/16 Pct Recovery = 96% Analysis Date = 04/13/16 Pct Recovery = 96% Analysis Date = 04/13/16 Pct Recovery = 96% Analysis Date = 04/10/16 Pct Recovery = 96% Analysis Date = 04/10/16 Pct Recovery = 96% Analysis Date = 04/07/16 Pct Recovery = 96% Analysis Date = 04/07/16 Pct Recovery = 96% Analysis Date = 04/04/16 Pct Recovery = 96% Analysis Date = 04/04/16 Pct Recovery = 96% Analysis Date = 04/01/16 Pct Recovery = 96% Analysis Date = 04/01/16 Pct Recovery = 96% Analysis Date = 03/29/16 Pct Recovery = 96% Analysis Date = 03/29/16 Pct Recovery = 96% Analysis Date = 03/26/16 Pct Recovery = 96% Analysis Date = 03/26/16 Pct Recovery = 96% Analysis Date = 03/23/16 Pct Recovery = 96% Analysis Date = 03/23/16 Pct Recovery = 96% Analysis Date = 03/20/16 Pct Recovery = 96% Analysis Date = 03/20/16 Pct Recovery = 96% Analysis Date = 03/17/16 Pct Recovery = 96% Analysis Date = 03/17/16 Pct Recovery = 96% Analysis Date = 03/14/16 Pct Recovery = 96% Analysis Date = 03/14/16 Pct Recovery = 96% Analysis Date = 03/11/16 Pct Recovery = 96% Analysis Date = 03/11/16 Pct Recovery = 96% Analysis Date = 03/08/16 Pct Recovery = 96% Analysis Date = 03/08/16 Pct Recovery = 96% Analysis Date = 03/05/16 Pct Recovery = 96% Analysis Date = 03/05/16 Pct Recovery = 96% Analysis Date = 03/02/16 Pct Recovery = 96% Analysis Date = 03/02/16 Pct Recovery = 96% Analysis Date = 02/28/16 Pct Recovery = 96% Analysis Date = 02/28/16 Pct Recovery = 96% Analysis Date = 02/25/16 Pct Recovery = 96% Analysis Date = 02/25/16 Pct Recovery = 96% Analysis Date = 02/22/16 Pct Recovery = 96% Analysis Date = 02/22/16 Pct Recovery = 96% Analysis Date = 02/19/16 Pct Recovery = 96% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DEMETHYL FLUOMETURON

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 6 99% 19% 102% 14%
>= Reporting Level 55 109% 53% 98% 19%
Total 61 108% 51% 98% 18%

Sample Statistics
DEMETHYL FLUOMETURON

Characteristic N % % Basis
Plotted 61 95% Spiked
Estimated Values 7 11% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 3 5% Spiked
Spiked 66 .  
False Negatives 0 0% 0 out of 64
Not Spiked 53 .  
False Positives 0 0% 0 out of 53