OBSP Determination:
ALACHLOR SULFONIC ACID
METHOD: 2437 , TESTIDCODE: 68871LCM60

Analysis Date = 03/08/17 SpikeMix = Abs 072516: 100 µl & Abs 071216: 100 µl Pct Recovery = 83% Analysis Date = 03/08/17 SpikeMix = Abs 072516: 100 µl & Abs 071216: 100 µl Pct Recovery = 173% Analysis Date = 02/16/17 SpikeMix = Abs 071216: 100 µl & ChemService 5154100: 100 µl Pct Recovery = 82% Analysis Date = 02/16/17 SpikeMix = Abs 071216: 100 µl & ChemService 5154100: 100 µl Pct Recovery = 108% Analysis Date = 08/25/16 SpikeMix = Abs 072516: 100 µl & Abs 071216: 100 µl Pct Recovery = 119% Analysis Date = 08/25/16 SpikeMix = Abs 072516: 100 µl & Abs 071216: 100 µl Pct Recovery = 114% Analysis Date = 07/11/17 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 123% Analysis Date = 06/21/17 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 131% Analysis Date = 04/18/17 SpikeMix = Abs 071216: 80 µl & ChemService 5154100: 80 µl Pct Recovery = 110% Analysis Date = 12/13/16 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 102% Analysis Date = 12/13/16 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 99% Analysis Date = 11/22/16 SpikeMix = Spex Organics TS160603008: 80 µl & Abs 071216: 80 µl Pct Recovery = 146% Analysis Date = 11/22/16 SpikeMix = Spex Organics TS160603008: 80 µl & Abs 071216: 80 µl Pct Recovery = 144% Analysis Date = 05/10/16 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 118% Analysis Date = 05/10/16 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 123% Analysis Date = 02/02/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 92% Analysis Date = 02/02/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 110% Analysis Date = 02/02/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 106% Analysis Date = 03/16/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 69% Analysis Date = 03/16/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 75% Analysis Date = 03/16/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 64% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 109% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 81% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 115% Analysis Date = 07/06/17 SpikeMix = Abs 071216: 40 µl & Abs 072516: 40 µl Pct Recovery = 86% Analysis Date = 05/27/17 SpikeMix = Abs 071216: 40 µl & Abs 071816: 40 µl Pct Recovery = 83% Analysis Date = 11/01/16 SpikeMix = Abs 072516: 40 µl & Abs 071216: 40 µl Pct Recovery = 94% Analysis Date = 10/07/16 SpikeMix = Spex Organics TS160603008: 40 µl & Abs 071216: 40 µl Pct Recovery = 102% Analysis Date = 10/07/16 SpikeMix = Spex Organics TS160603008: 40 µl & Abs 071216: 40 µl Pct Recovery = 69% Analysis Date = 09/21/16 SpikeMix = Abs 071216: 40 µl & ChemService 5154100: 40 µl Pct Recovery = 144% Analysis Date = 09/21/16 SpikeMix = Abs 071216: 40 µl & ChemService 5154100: 40 µl Pct Recovery = 125% Analysis Date = 08/31/16 SpikeMix = Abs 071216: 40 µl & Abs 071816: 40 µl Pct Recovery = 153% Analysis Date = 08/31/16 SpikeMix = Abs 071216: 40 µl & Abs 071816: 40 µl Pct Recovery = 134% Analysis Date = 03/01/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 105% Analysis Date = 03/01/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 119% Analysis Date = 03/01/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 133% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 98% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 121% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 114% Analysis Date = 01/27/16 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 89% Analysis Date = 03/23/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ChemService 4047000: 1 Pct Recovery = 84% Analysis Date = 03/23/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ChemService 4047000: 1 Pct Recovery = 105% Analysis Date = 02/09/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 120% Analysis Date = 02/09/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 87% Analysis Date = 02/09/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 141% Analysis Date = 07/10/17 Pct Recovery = 106% Analysis Date = 07/08/17 Pct Recovery = 106% Analysis Date = 07/08/17 Pct Recovery = 106% Analysis Date = 07/05/17 Pct Recovery = 106% Analysis Date = 07/05/17 Pct Recovery = 106% Analysis Date = 07/03/17 Pct Recovery = 106% Analysis Date = 07/03/17 Pct Recovery = 106% Analysis Date = 06/30/17 Pct Recovery = 106% Analysis Date = 06/30/17 Pct Recovery = 106% Analysis Date = 06/27/17 Pct Recovery = 106% Analysis Date = 06/27/17 Pct Recovery = 106% Analysis Date = 06/25/17 Pct Recovery = 107% Analysis Date = 06/25/17 Pct Recovery = 107% Analysis Date = 06/22/17 Pct Recovery = 107% Analysis Date = 06/22/17 Pct Recovery = 107% Analysis Date = 06/19/17 Pct Recovery = 107% Analysis Date = 06/19/17 Pct Recovery = 107% Analysis Date = 06/17/17 Pct Recovery = 107% Analysis Date = 06/17/17 Pct Recovery = 107% Analysis Date = 06/14/17 Pct Recovery = 107% Analysis Date = 06/14/17 Pct Recovery = 107% Analysis Date = 06/11/17 Pct Recovery = 107% Analysis Date = 06/11/17 Pct Recovery = 107% Analysis Date = 06/09/17 Pct Recovery = 107% Analysis Date = 06/09/17 Pct Recovery = 107% Analysis Date = 06/06/17 Pct Recovery = 107% Analysis Date = 06/06/17 Pct Recovery = 107% Analysis Date = 06/03/17 Pct Recovery = 107% Analysis Date = 06/03/17 Pct Recovery = 107% Analysis Date = 06/01/17 Pct Recovery = 107% Analysis Date = 06/01/17 Pct Recovery = 107% Analysis Date = 05/29/17 Pct Recovery = 108% Analysis Date = 05/29/17 Pct Recovery = 108% Analysis Date = 05/26/17 Pct Recovery = 108% Analysis Date = 05/26/17 Pct Recovery = 108% Analysis Date = 05/24/17 Pct Recovery = 108% Analysis Date = 05/24/17 Pct Recovery = 108% Analysis Date = 05/21/17 Pct Recovery = 108% Analysis Date = 05/21/17 Pct Recovery = 108% Analysis Date = 05/18/17 Pct Recovery = 108% Analysis Date = 05/18/17 Pct Recovery = 108% Analysis Date = 05/16/17 Pct Recovery = 108% Analysis Date = 05/16/17 Pct Recovery = 108% Analysis Date = 05/13/17 Pct Recovery = 108% Analysis Date = 05/13/17 Pct Recovery = 108% Analysis Date = 05/10/17 Pct Recovery = 108% Analysis Date = 05/10/17 Pct Recovery = 108% Analysis Date = 05/08/17 Pct Recovery = 108% Analysis Date = 05/08/17 Pct Recovery = 108% Analysis Date = 05/05/17 Pct Recovery = 109% Analysis Date = 05/05/17 Pct Recovery = 109% Analysis Date = 05/02/17 Pct Recovery = 109% Analysis Date = 05/02/17 Pct Recovery = 109% Analysis Date = 04/30/17 Pct Recovery = 109% Analysis Date = 04/30/17 Pct Recovery = 109% Analysis Date = 04/27/17 Pct Recovery = 109% Analysis Date = 04/27/17 Pct Recovery = 109% Analysis Date = 04/25/17 Pct Recovery = 109% Analysis Date = 04/25/17 Pct Recovery = 109% Analysis Date = 04/22/17 Pct Recovery = 109% Analysis Date = 04/22/17 Pct Recovery = 109% Analysis Date = 04/19/17 Pct Recovery = 109% Analysis Date = 04/19/17 Pct Recovery = 109% Analysis Date = 04/17/17 Pct Recovery = 109% Analysis Date = 04/17/17 Pct Recovery = 109% Analysis Date = 04/14/17 Pct Recovery = 109% Analysis Date = 04/14/17 Pct Recovery = 109% Analysis Date = 04/11/17 Pct Recovery = 110% Analysis Date = 04/11/17 Pct Recovery = 110% Analysis Date = 04/09/17 Pct Recovery = 110% Analysis Date = 04/09/17 Pct Recovery = 110% Analysis Date = 04/06/17 Pct Recovery = 110% Analysis Date = 04/06/17 Pct Recovery = 110% Analysis Date = 04/03/17 Pct Recovery = 110% Analysis Date = 04/03/17 Pct Recovery = 110% Analysis Date = 04/01/17 Pct Recovery = 110% Analysis Date = 04/01/17 Pct Recovery = 110% Analysis Date = 03/29/17 Pct Recovery = 110% Analysis Date = 03/29/17 Pct Recovery = 110% Analysis Date = 03/26/17 Pct Recovery = 110% Analysis Date = 03/26/17 Pct Recovery = 110% Analysis Date = 03/24/17 Pct Recovery = 110% Analysis Date = 03/24/17 Pct Recovery = 110% Analysis Date = 03/21/17 Pct Recovery = 110% Analysis Date = 03/21/17 Pct Recovery = 110% Analysis Date = 03/18/17 Pct Recovery = 111% Analysis Date = 03/18/17 Pct Recovery = 111% Analysis Date = 03/16/17 Pct Recovery = 111% Analysis Date = 03/16/17 Pct Recovery = 111% Analysis Date = 03/13/17 Pct Recovery = 111% Analysis Date = 03/13/17 Pct Recovery = 111% Analysis Date = 03/10/17 Pct Recovery = 111% Analysis Date = 03/10/17 Pct Recovery = 111% Analysis Date = 03/08/17 Pct Recovery = 111% Analysis Date = 03/08/17 Pct Recovery = 111% Analysis Date = 03/05/17 Pct Recovery = 111% Analysis Date = 03/05/17 Pct Recovery = 111% Analysis Date = 03/02/17 Pct Recovery = 111% Analysis Date = 03/02/17 Pct Recovery = 111% Analysis Date = 02/28/17 Pct Recovery = 111% Analysis Date = 02/28/17 Pct Recovery = 111% Analysis Date = 02/25/17 Pct Recovery = 111% Analysis Date = 02/25/17 Pct Recovery = 111% Analysis Date = 02/22/17 Pct Recovery = 112% Analysis Date = 02/22/17 Pct Recovery = 112% Analysis Date = 02/20/17 Pct Recovery = 112% Analysis Date = 02/20/17 Pct Recovery = 112% Analysis Date = 02/17/17 Pct Recovery = 112% Analysis Date = 02/17/17 Pct Recovery = 112% Analysis Date = 02/14/17 Pct Recovery = 112% Analysis Date = 02/14/17 Pct Recovery = 112% Analysis Date = 02/12/17 Pct Recovery = 112% Analysis Date = 02/12/17 Pct Recovery = 112% Analysis Date = 02/09/17 Pct Recovery = 112% Analysis Date = 02/09/17 Pct Recovery = 112% Analysis Date = 02/07/17 Pct Recovery = 112% Analysis Date = 02/07/17 Pct Recovery = 112% Analysis Date = 02/04/17 Pct Recovery = 112% Analysis Date = 02/04/17 Pct Recovery = 112% Analysis Date = 02/01/17 Pct Recovery = 113% Analysis Date = 02/01/17 Pct Recovery = 113% Analysis Date = 01/30/17 Pct Recovery = 113% Analysis Date = 01/30/17 Pct Recovery = 113% Analysis Date = 01/27/17 Pct Recovery = 113% Analysis Date = 01/27/17 Pct Recovery = 113% Analysis Date = 01/24/17 Pct Recovery = 113% Analysis Date = 01/24/17 Pct Recovery = 113% Analysis Date = 01/22/17 Pct Recovery = 113% Analysis Date = 01/22/17 Pct Recovery = 113% Analysis Date = 01/19/17 Pct Recovery = 113% Analysis Date = 01/19/17 Pct Recovery = 113% Analysis Date = 01/16/17 Pct Recovery = 113% Analysis Date = 01/16/17 Pct Recovery = 113% Analysis Date = 01/14/17 Pct Recovery = 113% Analysis Date = 01/14/17 Pct Recovery = 113% Analysis Date = 01/11/17 Pct Recovery = 114% Analysis Date = 01/11/17 Pct Recovery = 114% Analysis Date = 01/08/17 Pct Recovery = 114% Analysis Date = 01/08/17 Pct Recovery = 114% Analysis Date = 01/06/17 Pct Recovery = 114% Analysis Date = 01/06/17 Pct Recovery = 114% Analysis Date = 01/03/17 Pct Recovery = 114% Analysis Date = 01/03/17 Pct Recovery = 114% Analysis Date = 12/31/16 Pct Recovery = 114% Analysis Date = 12/31/16 Pct Recovery = 114% Analysis Date = 12/29/16 Pct Recovery = 114% Analysis Date = 12/29/16 Pct Recovery = 114% Analysis Date = 12/26/16 Pct Recovery = 114% Analysis Date = 12/26/16 Pct Recovery = 114% Analysis Date = 12/23/16 Pct Recovery = 114% Analysis Date = 12/23/16 Pct Recovery = 114% Analysis Date = 12/21/16 Pct Recovery = 115% Analysis Date = 12/21/16 Pct Recovery = 115% Analysis Date = 12/18/16 Pct Recovery = 115% Analysis Date = 12/18/16 Pct Recovery = 115% Analysis Date = 12/15/16 Pct Recovery = 115% Analysis Date = 12/15/16 Pct Recovery = 115% Analysis Date = 12/13/16 Pct Recovery = 115% Analysis Date = 12/13/16 Pct Recovery = 115% Analysis Date = 12/10/16 Pct Recovery = 115% Analysis Date = 12/10/16 Pct Recovery = 115% Analysis Date = 12/07/16 Pct Recovery = 115% Analysis Date = 12/07/16 Pct Recovery = 115% Analysis Date = 12/05/16 Pct Recovery = 115% Analysis Date = 12/05/16 Pct Recovery = 115% Analysis Date = 12/02/16 Pct Recovery = 115% Analysis Date = 12/02/16 Pct Recovery = 115% Analysis Date = 11/29/16 Pct Recovery = 116% Analysis Date = 11/29/16 Pct Recovery = 116% Analysis Date = 11/27/16 Pct Recovery = 116% Analysis Date = 11/27/16 Pct Recovery = 116% Analysis Date = 11/24/16 Pct Recovery = 116% Analysis Date = 11/24/16 Pct Recovery = 116% Analysis Date = 11/22/16 Pct Recovery = 116% Analysis Date = 11/22/16 Pct Recovery = 116% Analysis Date = 11/19/16 Pct Recovery = 116% Analysis Date = 11/19/16 Pct Recovery = 116% Analysis Date = 11/16/16 Pct Recovery = 116% Analysis Date = 11/16/16 Pct Recovery = 116% Analysis Date = 11/14/16 Pct Recovery = 116% Analysis Date = 11/14/16 Pct Recovery = 116% Analysis Date = 11/11/16 Pct Recovery = 116% Analysis Date = 11/11/16 Pct Recovery = 116% Analysis Date = 11/08/16 Pct Recovery = 117% Analysis Date = 11/08/16 Pct Recovery = 117% Analysis Date = 11/06/16 Pct Recovery = 117% Analysis Date = 11/06/16 Pct Recovery = 117% Analysis Date = 11/03/16 Pct Recovery = 117% Analysis Date = 11/03/16 Pct Recovery = 117% Analysis Date = 10/31/16 Pct Recovery = 117% Analysis Date = 10/31/16 Pct Recovery = 117% Analysis Date = 10/29/16 Pct Recovery = 117% Analysis Date = 10/29/16 Pct Recovery = 117% Analysis Date = 10/26/16 Pct Recovery = 117% Analysis Date = 10/26/16 Pct Recovery = 117% Analysis Date = 10/23/16 Pct Recovery = 118% Analysis Date = 10/23/16 Pct Recovery = 118% Analysis Date = 10/21/16 Pct Recovery = 118% Analysis Date = 10/21/16 Pct Recovery = 118% Analysis Date = 10/18/16 Pct Recovery = 118% Analysis Date = 10/18/16 Pct Recovery = 118% Analysis Date = 10/15/16 Pct Recovery = 118% Analysis Date = 10/15/16 Pct Recovery = 118% Analysis Date = 10/13/16 Pct Recovery = 118% Analysis Date = 10/13/16 Pct Recovery = 118% Analysis Date = 10/10/16 Pct Recovery = 118% Analysis Date = 10/10/16 Pct Recovery = 118% Analysis Date = 10/07/16 Pct Recovery = 118% Analysis Date = 10/07/16 Pct Recovery = 118% Analysis Date = 10/05/16 Pct Recovery = 119% Analysis Date = 10/05/16 Pct Recovery = 119% Analysis Date = 10/02/16 Pct Recovery = 119% Analysis Date = 10/02/16 Pct Recovery = 119% Analysis Date = 09/29/16 Pct Recovery = 119% Analysis Date = 09/29/16 Pct Recovery = 119% Analysis Date = 09/27/16 Pct Recovery = 119% Analysis Date = 09/27/16 Pct Recovery = 119% Analysis Date = 09/24/16 Pct Recovery = 119% Analysis Date = 09/24/16 Pct Recovery = 119% Analysis Date = 09/21/16 Pct Recovery = 119% Analysis Date = 09/21/16 Pct Recovery = 119% Analysis Date = 09/19/16 Pct Recovery = 119% Analysis Date = 09/19/16 Pct Recovery = 119% Analysis Date = 09/16/16 Pct Recovery = 120% Analysis Date = 09/16/16 Pct Recovery = 120% Analysis Date = 09/13/16 Pct Recovery = 120% Analysis Date = 09/13/16 Pct Recovery = 120% Analysis Date = 09/11/16 Pct Recovery = 120% Analysis Date = 09/11/16 Pct Recovery = 120% Analysis Date = 09/08/16 Pct Recovery = 120% Analysis Date = 09/08/16 Pct Recovery = 120% Analysis Date = 09/06/16 Pct Recovery = 120% Analysis Date = 09/06/16 Pct Recovery = 120% Analysis Date = 09/03/16 Pct Recovery = 120% Analysis Date = 09/03/16 Pct Recovery = 120% Analysis Date = 08/31/16 Pct Recovery = 120% Analysis Date = 08/31/16 Pct Recovery = 120% Analysis Date = 08/29/16 Pct Recovery = 120% Analysis Date = 08/29/16 Pct Recovery = 120% Analysis Date = 08/26/16 Pct Recovery = 120% Analysis Date = 08/26/16 Pct Recovery = 120% Analysis Date = 08/23/16 Pct Recovery = 120% Analysis Date = 08/23/16 Pct Recovery = 120% Analysis Date = 08/21/16 Pct Recovery = 119% Analysis Date = 08/21/16 Pct Recovery = 119% Analysis Date = 08/18/16 Pct Recovery = 119% Analysis Date = 08/18/16 Pct Recovery = 119% Analysis Date = 08/15/16 Pct Recovery = 119% Analysis Date = 08/15/16 Pct Recovery = 119% Analysis Date = 08/13/16 Pct Recovery = 119% Analysis Date = 08/13/16 Pct Recovery = 119% Analysis Date = 08/10/16 Pct Recovery = 118% Analysis Date = 08/10/16 Pct Recovery = 118% Analysis Date = 08/07/16 Pct Recovery = 118% Analysis Date = 08/07/16 Pct Recovery = 118% Analysis Date = 08/05/16 Pct Recovery = 118% Analysis Date = 08/05/16 Pct Recovery = 118% Analysis Date = 08/02/16 Pct Recovery = 118% Analysis Date = 08/02/16 Pct Recovery = 118% Analysis Date = 07/30/16 Pct Recovery = 117% Analysis Date = 07/30/16 Pct Recovery = 117% Analysis Date = 07/28/16 Pct Recovery = 117% Analysis Date = 07/28/16 Pct Recovery = 117% Analysis Date = 07/25/16 Pct Recovery = 117% Analysis Date = 07/25/16 Pct Recovery = 117% Analysis Date = 07/22/16 Pct Recovery = 117% Analysis Date = 07/22/16 Pct Recovery = 117% Analysis Date = 07/20/16 Pct Recovery = 117% Analysis Date = 07/20/16 Pct Recovery = 117% Analysis Date = 07/17/16 Pct Recovery = 116% Analysis Date = 07/17/16 Pct Recovery = 116% Analysis Date = 07/14/16 Pct Recovery = 116% Analysis Date = 07/14/16 Pct Recovery = 116% Analysis Date = 07/12/16 Pct Recovery = 116% Analysis Date = 07/12/16 Pct Recovery = 116% Analysis Date = 07/09/16 Pct Recovery = 116% Analysis Date = 07/09/16 Pct Recovery = 116% Analysis Date = 07/06/16 Pct Recovery = 115% Analysis Date = 07/06/16 Pct Recovery = 115% Analysis Date = 07/04/16 Pct Recovery = 115% Analysis Date = 07/04/16 Pct Recovery = 115% Analysis Date = 07/01/16 Pct Recovery = 115% Analysis Date = 07/01/16 Pct Recovery = 115% Analysis Date = 06/28/16 Pct Recovery = 115% Analysis Date = 06/28/16 Pct Recovery = 115% Analysis Date = 06/26/16 Pct Recovery = 114% Analysis Date = 06/26/16 Pct Recovery = 114% Analysis Date = 06/23/16 Pct Recovery = 114% Analysis Date = 06/23/16 Pct Recovery = 114% Analysis Date = 06/21/16 Pct Recovery = 114% Analysis Date = 06/21/16 Pct Recovery = 114% Analysis Date = 06/18/16 Pct Recovery = 114% Analysis Date = 06/18/16 Pct Recovery = 114% Analysis Date = 06/15/16 Pct Recovery = 113% Analysis Date = 06/15/16 Pct Recovery = 113% Analysis Date = 06/13/16 Pct Recovery = 113% Analysis Date = 06/13/16 Pct Recovery = 113% Analysis Date = 06/10/16 Pct Recovery = 113% Analysis Date = 06/10/16 Pct Recovery = 113% Analysis Date = 06/07/16 Pct Recovery = 113% Analysis Date = 06/07/16 Pct Recovery = 113% Analysis Date = 06/05/16 Pct Recovery = 112% Analysis Date = 06/05/16 Pct Recovery = 112% Analysis Date = 06/02/16 Pct Recovery = 112% Analysis Date = 06/02/16 Pct Recovery = 112% Analysis Date = 05/30/16 Pct Recovery = 112% Analysis Date = 05/30/16 Pct Recovery = 112% Analysis Date = 05/28/16 Pct Recovery = 112% Analysis Date = 05/28/16 Pct Recovery = 112% Analysis Date = 05/25/16 Pct Recovery = 111% Analysis Date = 05/25/16 Pct Recovery = 111% Analysis Date = 05/22/16 Pct Recovery = 111% Analysis Date = 05/22/16 Pct Recovery = 111% Analysis Date = 05/20/16 Pct Recovery = 111% Analysis Date = 05/20/16 Pct Recovery = 111% Analysis Date = 05/17/16 Pct Recovery = 111% Analysis Date = 05/17/16 Pct Recovery = 111% Analysis Date = 05/14/16 Pct Recovery = 110% Analysis Date = 05/14/16 Pct Recovery = 110% Analysis Date = 05/12/16 Pct Recovery = 110% Analysis Date = 05/12/16 Pct Recovery = 110% Analysis Date = 05/09/16 Pct Recovery = 110% Analysis Date = 05/09/16 Pct Recovery = 110% Analysis Date = 05/06/16 Pct Recovery = 110% Analysis Date = 05/06/16 Pct Recovery = 110% Analysis Date = 05/04/16 Pct Recovery = 109% Analysis Date = 05/04/16 Pct Recovery = 109% Analysis Date = 05/01/16 Pct Recovery = 109% Analysis Date = 05/01/16 Pct Recovery = 109% Analysis Date = 04/28/16 Pct Recovery = 109% Analysis Date = 04/28/16 Pct Recovery = 109% Analysis Date = 04/26/16 Pct Recovery = 108% Analysis Date = 04/26/16 Pct Recovery = 108% Analysis Date = 04/23/16 Pct Recovery = 108% Analysis Date = 04/23/16 Pct Recovery = 108% Analysis Date = 04/20/16 Pct Recovery = 107% Analysis Date = 04/20/16 Pct Recovery = 107% Analysis Date = 04/18/16 Pct Recovery = 107% Analysis Date = 04/18/16 Pct Recovery = 107% Analysis Date = 04/15/16 Pct Recovery = 107% Analysis Date = 04/15/16 Pct Recovery = 107% Analysis Date = 04/12/16 Pct Recovery = 106% Analysis Date = 04/12/16 Pct Recovery = 106% Analysis Date = 04/10/16 Pct Recovery = 106% Analysis Date = 04/10/16 Pct Recovery = 106% Analysis Date = 04/07/16 Pct Recovery = 106% Analysis Date = 04/07/16 Pct Recovery = 106% Analysis Date = 04/05/16 Pct Recovery = 105% Analysis Date = 04/05/16 Pct Recovery = 105% Analysis Date = 04/02/16 Pct Recovery = 105% Analysis Date = 04/02/16 Pct Recovery = 105% Analysis Date = 03/30/16 Pct Recovery = 105% Analysis Date = 03/30/16 Pct Recovery = 105% Analysis Date = 03/28/16 Pct Recovery = 104% Analysis Date = 03/28/16 Pct Recovery = 104% Analysis Date = 03/25/16 Pct Recovery = 104% Analysis Date = 03/25/16 Pct Recovery = 104% Analysis Date = 03/22/16 Pct Recovery = 104% Analysis Date = 03/22/16 Pct Recovery = 104% Analysis Date = 03/20/16 Pct Recovery = 103% Analysis Date = 03/20/16 Pct Recovery = 103% Analysis Date = 03/17/16 Pct Recovery = 103% Analysis Date = 03/17/16 Pct Recovery = 103% Analysis Date = 03/14/16 Pct Recovery = 103% Analysis Date = 03/14/16 Pct Recovery = 103% Analysis Date = 03/12/16 Pct Recovery = 103% Analysis Date = 03/12/16 Pct Recovery = 103% Analysis Date = 03/09/16 Pct Recovery = 103% Analysis Date = 03/09/16 Pct Recovery = 103% Analysis Date = 03/06/16 Pct Recovery = 103% Analysis Date = 03/06/16 Pct Recovery = 103% Analysis Date = 03/04/16 Pct Recovery = 103% Analysis Date = 03/04/16 Pct Recovery = 103% Analysis Date = 03/01/16 Pct Recovery = 103% Analysis Date = 03/01/16 Pct Recovery = 103% Analysis Date = 02/27/16 Pct Recovery = 103% Analysis Date = 02/27/16 Pct Recovery = 103% Analysis Date = 02/25/16 Pct Recovery = 103% Analysis Date = 02/25/16 Pct Recovery = 103% Analysis Date = 02/22/16 Pct Recovery = 103% Analysis Date = 02/22/16 Pct Recovery = 103% Analysis Date = 02/19/16 Pct Recovery = 104% Analysis Date = 02/19/16 Pct Recovery = 104% Analysis Date = 02/17/16 Pct Recovery = 104% Analysis Date = 02/17/16 Pct Recovery = 104% Analysis Date = 02/14/16 Pct Recovery = 104% Analysis Date = 02/14/16 Pct Recovery = 104% Analysis Date = 02/11/16 Pct Recovery = 104% Analysis Date = 02/11/16 Pct Recovery = 104% Analysis Date = 02/09/16 Pct Recovery = 104% Analysis Date = 02/09/16 Pct Recovery = 104% Analysis Date = 02/06/16 Pct Recovery = 104% Analysis Date = 02/06/16 Pct Recovery = 104% Analysis Date = 02/03/16 Pct Recovery = 104% Analysis Date = 02/03/16 Pct Recovery = 104% Analysis Date = 02/01/16 Pct Recovery = 105% Analysis Date = 02/01/16 Pct Recovery = 105% Analysis Date = 01/29/16 Pct Recovery = 105% Analysis Date = 01/29/16 Pct Recovery = 105% Analysis Date = 01/27/16 Pct Recovery = 105% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ALACHLOR SULFONIC ACID

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 12 110% 18% 109% 20%
>= Reporting Level 33 109% 26% 109% 28%
Total 45 109% 24% 109% 25%

Sample Statistics
ALACHLOR SULFONIC ACID

Characteristic N % % Basis
Plotted 45 88% Spiked
Estimated Values 45 88% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 6 12% Spiked
Spiked 51 .  
False Negatives 0 0% 0 out of 51
Not Spiked 68 .  
False Positives 0 0% 0 out of 68