BQS OBSP Determination:
CARBAMAZEPINE
METHOD: 2080 , TESTIDCODE: 6279300021
Open Data Set

Analysis Date = 09/17/09 SpikeMix = Restek A063896: 40 µl Pct Recovery = 82% Analysis Date = 11/04/08 SpikeMix = Protocol T1080910002: 40 µl Pct Recovery = 78% Analysis Date = 06/22/09 SpikeMix = Protocol T1080910002: 40 µl Pct Recovery = 88% Analysis Date = 08/19/09 SpikeMix = NWQL LCL11SP078A: 100 µl Pct Recovery = 101% Analysis Date = 03/10/09 SpikeMix = Restek A063896: 25 µl Pct Recovery = 58% Analysis Date = 05/28/09 SpikeMix = NWQL LCL11SP078A: 80 µl Pct Recovery = 93% Analysis Date = 02/23/09 SpikeMix = Restek A063896: 25 µl Pct Recovery = 86% Analysis Date = 06/25/09 SpikeMix = NWQL LCL11SP078A: 80 µl Pct Recovery = 102% Analysis Date = 03/25/09 SpikeMix = Protocol T1080910002: 25 µl Pct Recovery = 81% Analysis Date = 07/27/09 SpikeMix = NWQL LCL11SP078A: 80 µl Pct Recovery = 97% Analysis Date = 12/16/08 SpikeMix = Restek A063896: 25 µl Pct Recovery = 76% Analysis Date = 11/20/08 SpikeMix = Protocol T1080910002: 25 µl Pct Recovery = 109% Analysis Date = 09/19/08 SpikeMix = Accu B7070261: 50 µl Pct Recovery = 105% Analysis Date = 02/19/08 SpikeMix = Supelco LB50305: 50 µl Pct Recovery = 98% Analysis Date = 07/01/09 SpikeMix = Restek A063896: 25 µl Pct Recovery = 84% Analysis Date = 04/07/08 SpikeMix = Accu B7070261: 50 µl Pct Recovery = 117% Analysis Date = 03/20/08 SpikeMix = Supelco LB50305: 50 µl Pct Recovery = 88% Analysis Date = 05/14/08 SpikeMix = Accu B7070261: 50 µl Pct Recovery = 91% Analysis Date = 07/15/08 SpikeMix = Accu B7070261: 50 µl Pct Recovery = 111% Analysis Date = 10/02/08 SpikeMix = Accu B7070261: 50 µl Pct Recovery = 101% Analysis Date = 05/28/08 SpikeMix = Accu B7070261: 50 µl Pct Recovery = 68% Analysis Date = 08/06/08 SpikeMix = Accu B7070261: 50 µl Pct Recovery = 97% Analysis Date = 06/14/10 SpikeMix = Accu 209081146: 50 µl Pct Recovery = 81% Analysis Date = 09/24/10 SpikeMix = Supelco LB69638: 50 µl Pct Recovery = 79% Analysis Date = 07/14/10 SpikeMix = Supelco LB69638: 50 µl Pct Recovery = 108% Analysis Date = 01/07/10 SpikeMix = Accu 209081146: 50 µl Pct Recovery = 73% Analysis Date = 03/15/11 SpikeMix = Abs 090910Pharm: 80 µl Pct Recovery = 86% Analysis Date = 06/23/11 SpikeMix = Spex Organics T1100628001: 80 µl Pct Recovery = 94% Analysis Date = 09/21/11 SpikeMix = Spex Organics T1100628001: 80 µl Pct Recovery = 97% Analysis Date = 09/15/11 SpikeMix = Abs 090910Pharm: 80 µl Pct Recovery = 84% Analysis Date = 04/07/11 SpikeMix = Spex Organics T1100628001: 80 µl Pct Recovery = 86% Analysis Date = 06/23/10 SpikeMix = NWQL LCL11SP081A: 50 µl Pct Recovery = 116% Analysis Date = 09/10/10 SpikeMix = NWQL LCL11SP081A: 50 µl Pct Recovery = 132% Analysis Date = 04/08/10 SpikeMix = NWQL LCL11SP081A: 50 µl Pct Recovery = 107% Analysis Date = 06/02/10 SpikeMix = NWQL LCL11SP081A: 50 µl Pct Recovery = 79% Analysis Date = 07/21/10 SpikeMix = NWQL LCL11SP081A: 50 µl Pct Recovery = 101% Analysis Date = 12/14/10 SpikeMix = Spex Organics T1100628001: 50 µl Pct Recovery = 89% Analysis Date = 08/03/11 SpikeMix = Spex Organics T1100628001: 50 µl Pct Recovery = 84% Analysis Date = 07/13/11 SpikeMix = Abs 090910Pharm: 50 µl Pct Recovery = 101% Analysis Date = 05/25/11 SpikeMix = Abs 090910Pharm: 50 µl Pct Recovery = 95% Analysis Date = 10/25/10 SpikeMix = Spex Organics T1100628001: 50 µl Pct Recovery = 89% Analysis Date = 11/16/10 SpikeMix = Abs 090910Pharm: 50 µl Pct Recovery = 96% Analysis Date = 05/11/11 SpikeMix = Abs 090910Pharm: 50 µl Pct Recovery = 83% Analysis Date = 05/13/10 SpikeMix = Supelco LB69638: 25 µl Pct Recovery = 108% Analysis Date = 04/28/10 SpikeMix = Accu 209081146: 25 µl Pct Recovery = 88% Analysis Date = 10/22/09 SpikeMix = Accu 209081146: 25 µl Pct Recovery = 73% Analysis Date = 08/05/10 SpikeMix = Accu 209081146: 25 µl Pct Recovery = 89% Analysis Date = 08/17/10 SpikeMix = Supelco LB69638: 25 µl Pct Recovery = 82% Analysis Date = 11/30/09 SpikeMix = Supelco LB69638: 25 µl Pct Recovery = 79% Analysis Date = 03/09/10 SpikeMix = Supelco LB69638: 25 µl Pct Recovery = 85% Analysis Date = 09/20/11 Pct Recovery = 90% Analysis Date = 09/14/11 Pct Recovery = 90% Analysis Date = 09/14/11 Pct Recovery = 90% Analysis Date = 09/07/11 Pct Recovery = 90% Analysis Date = 09/07/11 Pct Recovery = 90% Analysis Date = 09/01/11 Pct Recovery = 90% Analysis Date = 09/01/11 Pct Recovery = 90% Analysis Date = 08/25/11 Pct Recovery = 90% Analysis Date = 08/25/11 Pct Recovery = 90% Analysis Date = 08/19/11 Pct Recovery = 90% Analysis Date = 08/19/11 Pct Recovery = 90% Analysis Date = 08/12/11 Pct Recovery = 90% Analysis Date = 08/12/11 Pct Recovery = 90% Analysis Date = 08/06/11 Pct Recovery = 90% Analysis Date = 08/06/11 Pct Recovery = 90% Analysis Date = 07/30/11 Pct Recovery = 90% Analysis Date = 07/30/11 Pct Recovery = 90% Analysis Date = 07/24/11 Pct Recovery = 90% Analysis Date = 07/24/11 Pct Recovery = 90% Analysis Date = 07/17/11 Pct Recovery = 90% Analysis Date = 07/17/11 Pct Recovery = 90% Analysis Date = 07/10/11 Pct Recovery = 90% Analysis Date = 07/10/11 Pct Recovery = 90% Analysis Date = 07/04/11 Pct Recovery = 91% Analysis Date = 07/04/11 Pct Recovery = 91% Analysis Date = 06/27/11 Pct Recovery = 91% Analysis Date = 06/27/11 Pct Recovery = 91% Analysis Date = 06/21/11 Pct Recovery = 91% Analysis Date = 06/21/11 Pct Recovery = 91% Analysis Date = 06/14/11 Pct Recovery = 91% Analysis Date = 06/14/11 Pct Recovery = 91% Analysis Date = 06/08/11 Pct Recovery = 91% Analysis Date = 06/08/11 Pct Recovery = 91% Analysis Date = 06/01/11 Pct Recovery = 91% Analysis Date = 06/01/11 Pct Recovery = 91% Analysis Date = 05/26/11 Pct Recovery = 91% Analysis Date = 05/26/11 Pct Recovery = 91% Analysis Date = 05/19/11 Pct Recovery = 91% Analysis Date = 05/19/11 Pct Recovery = 91% Analysis Date = 05/12/11 Pct Recovery = 91% Analysis Date = 05/12/11 Pct Recovery = 91% Analysis Date = 05/06/11 Pct Recovery = 91% Analysis Date = 05/06/11 Pct Recovery = 91% Analysis Date = 04/29/11 Pct Recovery = 91% Analysis Date = 04/29/11 Pct Recovery = 91% Analysis Date = 04/23/11 Pct Recovery = 91% Analysis Date = 04/23/11 Pct Recovery = 91% Analysis Date = 04/16/11 Pct Recovery = 91% Analysis Date = 04/16/11 Pct Recovery = 91% Analysis Date = 04/10/11 Pct Recovery = 92% Analysis Date = 04/10/11 Pct Recovery = 92% Analysis Date = 04/03/11 Pct Recovery = 92% Analysis Date = 04/03/11 Pct Recovery = 92% Analysis Date = 03/28/11 Pct Recovery = 92% Analysis Date = 03/28/11 Pct Recovery = 92% Analysis Date = 03/21/11 Pct Recovery = 92% Analysis Date = 03/21/11 Pct Recovery = 92% Analysis Date = 03/15/11 Pct Recovery = 92% Analysis Date = 03/15/11 Pct Recovery = 92% Analysis Date = 03/08/11 Pct Recovery = 92% Analysis Date = 03/08/11 Pct Recovery = 92% Analysis Date = 03/01/11 Pct Recovery = 92% Analysis Date = 03/01/11 Pct Recovery = 92% Analysis Date = 02/23/11 Pct Recovery = 92% Analysis Date = 02/23/11 Pct Recovery = 92% Analysis Date = 02/16/11 Pct Recovery = 92% Analysis Date = 02/16/11 Pct Recovery = 92% Analysis Date = 02/10/11 Pct Recovery = 92% Analysis Date = 02/10/11 Pct Recovery = 92% Analysis Date = 02/03/11 Pct Recovery = 92% Analysis Date = 02/03/11 Pct Recovery = 92% Analysis Date = 01/28/11 Pct Recovery = 92% Analysis Date = 01/28/11 Pct Recovery = 92% Analysis Date = 01/21/11 Pct Recovery = 92% Analysis Date = 01/21/11 Pct Recovery = 92% Analysis Date = 01/15/11 Pct Recovery = 92% Analysis Date = 01/15/11 Pct Recovery = 92% Analysis Date = 01/08/11 Pct Recovery = 92% Analysis Date = 01/08/11 Pct Recovery = 92% Analysis Date = 01/01/11 Pct Recovery = 93% Analysis Date = 01/01/11 Pct Recovery = 93% Analysis Date = 12/26/10 Pct Recovery = 93% Analysis Date = 12/26/10 Pct Recovery = 93% Analysis Date = 12/19/10 Pct Recovery = 93% Analysis Date = 12/19/10 Pct Recovery = 93% Analysis Date = 12/13/10 Pct Recovery = 93% Analysis Date = 12/13/10 Pct Recovery = 93% Analysis Date = 12/06/10 Pct Recovery = 93% Analysis Date = 12/06/10 Pct Recovery = 93% Analysis Date = 11/30/10 Pct Recovery = 93% Analysis Date = 11/30/10 Pct Recovery = 93% Analysis Date = 11/23/10 Pct Recovery = 93% Analysis Date = 11/23/10 Pct Recovery = 93% Analysis Date = 11/17/10 Pct Recovery = 93% Analysis Date = 11/17/10 Pct Recovery = 93% Analysis Date = 11/10/10 Pct Recovery = 93% Analysis Date = 11/10/10 Pct Recovery = 93% Analysis Date = 11/04/10 Pct Recovery = 93% Analysis Date = 11/04/10 Pct Recovery = 93% Analysis Date = 10/28/10 Pct Recovery = 93% Analysis Date = 10/28/10 Pct Recovery = 93% Analysis Date = 10/21/10 Pct Recovery = 93% Analysis Date = 10/21/10 Pct Recovery = 93% Analysis Date = 10/15/10 Pct Recovery = 93% Analysis Date = 10/15/10 Pct Recovery = 93% Analysis Date = 10/08/10 Pct Recovery = 93% Analysis Date = 10/08/10 Pct Recovery = 93% Analysis Date = 10/02/10 Pct Recovery = 94% Analysis Date = 10/02/10 Pct Recovery = 94% Analysis Date = 09/25/10 Pct Recovery = 94% Analysis Date = 09/25/10 Pct Recovery = 94% Analysis Date = 09/19/10 Pct Recovery = 94% Analysis Date = 09/19/10 Pct Recovery = 94% Analysis Date = 09/12/10 Pct Recovery = 94% Analysis Date = 09/12/10 Pct Recovery = 94% Analysis Date = 09/06/10 Pct Recovery = 94% Analysis Date = 09/06/10 Pct Recovery = 94% Analysis Date = 08/30/10 Pct Recovery = 94% Analysis Date = 08/30/10 Pct Recovery = 94% Analysis Date = 08/23/10 Pct Recovery = 93% Analysis Date = 08/23/10 Pct Recovery = 93% Analysis Date = 08/17/10 Pct Recovery = 93% Analysis Date = 08/17/10 Pct Recovery = 93% Analysis Date = 08/10/10 Pct Recovery = 93% Analysis Date = 08/10/10 Pct Recovery = 93% Analysis Date = 08/04/10 Pct Recovery = 93% Analysis Date = 08/04/10 Pct Recovery = 93% Analysis Date = 07/28/10 Pct Recovery = 93% Analysis Date = 07/28/10 Pct Recovery = 93% Analysis Date = 07/22/10 Pct Recovery = 93% Analysis Date = 07/22/10 Pct Recovery = 93% Analysis Date = 07/15/10 Pct Recovery = 93% Analysis Date = 07/15/10 Pct Recovery = 93% Analysis Date = 07/09/10 Pct Recovery = 93% Analysis Date = 07/09/10 Pct Recovery = 93% Analysis Date = 07/02/10 Pct Recovery = 93% Analysis Date = 07/02/10 Pct Recovery = 93% Analysis Date = 06/26/10 Pct Recovery = 93% Analysis Date = 06/26/10 Pct Recovery = 93% Analysis Date = 06/19/10 Pct Recovery = 93% Analysis Date = 06/19/10 Pct Recovery = 93% Analysis Date = 06/12/10 Pct Recovery = 93% Analysis Date = 06/12/10 Pct Recovery = 93% Analysis Date = 06/06/10 Pct Recovery = 93% Analysis Date = 06/06/10 Pct Recovery = 93% Analysis Date = 05/30/10 Pct Recovery = 93% Analysis Date = 05/30/10 Pct Recovery = 93% Analysis Date = 05/24/10 Pct Recovery = 93% Analysis Date = 05/24/10 Pct Recovery = 93% Analysis Date = 05/17/10 Pct Recovery = 92% Analysis Date = 05/17/10 Pct Recovery = 92% Analysis Date = 05/11/10 Pct Recovery = 92% Analysis Date = 05/11/10 Pct Recovery = 92% Analysis Date = 05/04/10 Pct Recovery = 92% Analysis Date = 05/04/10 Pct Recovery = 92% Analysis Date = 04/28/10 Pct Recovery = 92% Analysis Date = 04/28/10 Pct Recovery = 92% Analysis Date = 04/21/10 Pct Recovery = 92% Analysis Date = 04/21/10 Pct Recovery = 92% Analysis Date = 04/14/10 Pct Recovery = 92% Analysis Date = 04/14/10 Pct Recovery = 92% Analysis Date = 04/08/10 Pct Recovery = 92% Analysis Date = 04/08/10 Pct Recovery = 92% Analysis Date = 04/01/10 Pct Recovery = 92% Analysis Date = 04/01/10 Pct Recovery = 92% Analysis Date = 03/26/10 Pct Recovery = 92% Analysis Date = 03/26/10 Pct Recovery = 92% Analysis Date = 03/19/10 Pct Recovery = 91% Analysis Date = 03/19/10 Pct Recovery = 91% Analysis Date = 03/13/10 Pct Recovery = 91% Analysis Date = 03/13/10 Pct Recovery = 91% Analysis Date = 03/06/10 Pct Recovery = 91% Analysis Date = 03/06/10 Pct Recovery = 91% Analysis Date = 02/28/10 Pct Recovery = 91% Analysis Date = 02/28/10 Pct Recovery = 91% Analysis Date = 02/21/10 Pct Recovery = 91% Analysis Date = 02/21/10 Pct Recovery = 91% Analysis Date = 02/15/10 Pct Recovery = 91% Analysis Date = 02/15/10 Pct Recovery = 91% Analysis Date = 02/08/10 Pct Recovery = 91% Analysis Date = 02/08/10 Pct Recovery = 91% Analysis Date = 02/01/10 Pct Recovery = 91% Analysis Date = 02/01/10 Pct Recovery = 91% Analysis Date = 01/26/10 Pct Recovery = 91% Analysis Date = 01/26/10 Pct Recovery = 91% Analysis Date = 01/19/10 Pct Recovery = 91% Analysis Date = 01/19/10 Pct Recovery = 91% Analysis Date = 01/13/10 Pct Recovery = 90% Analysis Date = 01/13/10 Pct Recovery = 90% Analysis Date = 01/06/10 Pct Recovery = 90% Analysis Date = 01/06/10 Pct Recovery = 90% Analysis Date = 12/31/09 Pct Recovery = 90% Analysis Date = 12/31/09 Pct Recovery = 90% Analysis Date = 12/24/09 Pct Recovery = 90% Analysis Date = 12/24/09 Pct Recovery = 90% Analysis Date = 12/18/09 Pct Recovery = 90% Analysis Date = 12/18/09 Pct Recovery = 90% Analysis Date = 12/11/09 Pct Recovery = 90% Analysis Date = 12/11/09 Pct Recovery = 90% Analysis Date = 12/04/09 Pct Recovery = 90% Analysis Date = 12/04/09 Pct Recovery = 90% Analysis Date = 11/28/09 Pct Recovery = 90% Analysis Date = 11/28/09 Pct Recovery = 90% Analysis Date = 11/21/09 Pct Recovery = 89% Analysis Date = 11/21/09 Pct Recovery = 89% Analysis Date = 11/15/09 Pct Recovery = 89% Analysis Date = 11/15/09 Pct Recovery = 89% Analysis Date = 11/08/09 Pct Recovery = 89% Analysis Date = 11/08/09 Pct Recovery = 89% Analysis Date = 11/02/09 Pct Recovery = 89% Analysis Date = 11/02/09 Pct Recovery = 89% Analysis Date = 10/26/09 Pct Recovery = 89% Analysis Date = 10/26/09 Pct Recovery = 89% Analysis Date = 10/20/09 Pct Recovery = 89% Analysis Date = 10/20/09 Pct Recovery = 89% Analysis Date = 10/13/09 Pct Recovery = 89% Analysis Date = 10/13/09 Pct Recovery = 89% Analysis Date = 10/07/09 Pct Recovery = 88% Analysis Date = 10/07/09 Pct Recovery = 88% Analysis Date = 09/30/09 Pct Recovery = 88% Analysis Date = 09/30/09 Pct Recovery = 88% Analysis Date = 09/23/09 Pct Recovery = 88% Analysis Date = 09/23/09 Pct Recovery = 88% Analysis Date = 09/17/09 Pct Recovery = 88% Analysis Date = 09/17/09 Pct Recovery = 88% Analysis Date = 09/10/09 Pct Recovery = 88% Analysis Date = 09/10/09 Pct Recovery = 88% Analysis Date = 09/04/09 Pct Recovery = 88% Analysis Date = 09/04/09 Pct Recovery = 88% Analysis Date = 08/28/09 Pct Recovery = 88% Analysis Date = 08/28/09 Pct Recovery = 88% Analysis Date = 08/22/09 Pct Recovery = 88% Analysis Date = 08/22/09 Pct Recovery = 88% Analysis Date = 08/15/09 Pct Recovery = 87% Analysis Date = 08/15/09 Pct Recovery = 87% Analysis Date = 08/09/09 Pct Recovery = 87% Analysis Date = 08/09/09 Pct Recovery = 87% Analysis Date = 08/02/09 Pct Recovery = 87% Analysis Date = 08/02/09 Pct Recovery = 87% Analysis Date = 07/26/09 Pct Recovery = 87% Analysis Date = 07/26/09 Pct Recovery = 87% Analysis Date = 07/20/09 Pct Recovery = 87% Analysis Date = 07/20/09 Pct Recovery = 87% Analysis Date = 07/13/09 Pct Recovery = 87% Analysis Date = 07/13/09 Pct Recovery = 87% Analysis Date = 07/07/09 Pct Recovery = 87% Analysis Date = 07/07/09 Pct Recovery = 87% Analysis Date = 06/30/09 Pct Recovery = 86% Analysis Date = 06/30/09 Pct Recovery = 86% Analysis Date = 06/24/09 Pct Recovery = 87% Analysis Date = 06/24/09 Pct Recovery = 87% Analysis Date = 06/17/09 Pct Recovery = 87% Analysis Date = 06/17/09 Pct Recovery = 87% Analysis Date = 06/11/09 Pct Recovery = 87% Analysis Date = 06/11/09 Pct Recovery = 87% Analysis Date = 06/04/09 Pct Recovery = 87% Analysis Date = 06/04/09 Pct Recovery = 87% Analysis Date = 05/29/09 Pct Recovery = 87% Analysis Date = 05/29/09 Pct Recovery = 87% Analysis Date = 05/22/09 Pct Recovery = 87% Analysis Date = 05/22/09 Pct Recovery = 87% Analysis Date = 05/15/09 Pct Recovery = 87% Analysis Date = 05/15/09 Pct Recovery = 87% Analysis Date = 05/09/09 Pct Recovery = 88% Analysis Date = 05/09/09 Pct Recovery = 88% Analysis Date = 05/02/09 Pct Recovery = 88% Analysis Date = 05/02/09 Pct Recovery = 88% Analysis Date = 04/26/09 Pct Recovery = 88% Analysis Date = 04/26/09 Pct Recovery = 88% Analysis Date = 04/19/09 Pct Recovery = 88% Analysis Date = 04/19/09 Pct Recovery = 88% Analysis Date = 04/13/09 Pct Recovery = 88% Analysis Date = 04/13/09 Pct Recovery = 88% Analysis Date = 04/06/09 Pct Recovery = 88% Analysis Date = 04/06/09 Pct Recovery = 88% Analysis Date = 03/31/09 Pct Recovery = 88% Analysis Date = 03/31/09 Pct Recovery = 88% Analysis Date = 03/24/09 Pct Recovery = 88% Analysis Date = 03/24/09 Pct Recovery = 88% Analysis Date = 03/17/09 Pct Recovery = 89% Analysis Date = 03/17/09 Pct Recovery = 89% Analysis Date = 03/11/09 Pct Recovery = 89% Analysis Date = 03/11/09 Pct Recovery = 89% Analysis Date = 03/04/09 Pct Recovery = 89% Analysis Date = 03/04/09 Pct Recovery = 89% Analysis Date = 02/26/09 Pct Recovery = 89% Analysis Date = 02/26/09 Pct Recovery = 89% Analysis Date = 02/19/09 Pct Recovery = 89% Analysis Date = 02/19/09 Pct Recovery = 89% Analysis Date = 02/13/09 Pct Recovery = 89% Analysis Date = 02/13/09 Pct Recovery = 89% Analysis Date = 02/06/09 Pct Recovery = 89% Analysis Date = 02/06/09 Pct Recovery = 89% Analysis Date = 01/31/09 Pct Recovery = 90% Analysis Date = 01/31/09 Pct Recovery = 90% Analysis Date = 01/24/09 Pct Recovery = 90% Analysis Date = 01/24/09 Pct Recovery = 90% Analysis Date = 01/18/09 Pct Recovery = 90% Analysis Date = 01/18/09 Pct Recovery = 90% Analysis Date = 01/11/09 Pct Recovery = 90% Analysis Date = 01/11/09 Pct Recovery = 90% Analysis Date = 01/04/09 Pct Recovery = 90% Analysis Date = 01/04/09 Pct Recovery = 90% Analysis Date = 12/29/08 Pct Recovery = 90% Analysis Date = 12/29/08 Pct Recovery = 90% Analysis Date = 12/22/08 Pct Recovery = 90% Analysis Date = 12/22/08 Pct Recovery = 90% Analysis Date = 12/16/08 Pct Recovery = 91% Analysis Date = 12/16/08 Pct Recovery = 91% Analysis Date = 12/09/08 Pct Recovery = 91% Analysis Date = 12/09/08 Pct Recovery = 91% Analysis Date = 12/03/08 Pct Recovery = 91% Analysis Date = 12/03/08 Pct Recovery = 91% Analysis Date = 11/26/08 Pct Recovery = 91% Analysis Date = 11/26/08 Pct Recovery = 91% Analysis Date = 11/20/08 Pct Recovery = 91% Analysis Date = 11/20/08 Pct Recovery = 91% Analysis Date = 11/13/08 Pct Recovery = 91% Analysis Date = 11/13/08 Pct Recovery = 91% Analysis Date = 11/06/08 Pct Recovery = 91% Analysis Date = 11/06/08 Pct Recovery = 91% Analysis Date = 10/31/08 Pct Recovery = 92% Analysis Date = 10/31/08 Pct Recovery = 92% Analysis Date = 10/24/08 Pct Recovery = 92% Analysis Date = 10/24/08 Pct Recovery = 92% Analysis Date = 10/18/08 Pct Recovery = 92% Analysis Date = 10/18/08 Pct Recovery = 92% Analysis Date = 10/11/08 Pct Recovery = 92% Analysis Date = 10/11/08 Pct Recovery = 92% Analysis Date = 10/05/08 Pct Recovery = 92% Analysis Date = 10/05/08 Pct Recovery = 92% Analysis Date = 09/28/08 Pct Recovery = 92% Analysis Date = 09/28/08 Pct Recovery = 92% Analysis Date = 09/22/08 Pct Recovery = 92% Analysis Date = 09/22/08 Pct Recovery = 92% Analysis Date = 09/15/08 Pct Recovery = 93% Analysis Date = 09/15/08 Pct Recovery = 93% Analysis Date = 09/09/08 Pct Recovery = 93% Analysis Date = 09/09/08 Pct Recovery = 93% Analysis Date = 09/02/08 Pct Recovery = 93% Analysis Date = 09/02/08 Pct Recovery = 93% Analysis Date = 08/26/08 Pct Recovery = 93% Analysis Date = 08/26/08 Pct Recovery = 93% Analysis Date = 08/20/08 Pct Recovery = 93% Analysis Date = 08/20/08 Pct Recovery = 93% Analysis Date = 08/13/08 Pct Recovery = 93% Analysis Date = 08/13/08 Pct Recovery = 93% Analysis Date = 08/07/08 Pct Recovery = 93% Analysis Date = 08/07/08 Pct Recovery = 93% Analysis Date = 07/31/08 Pct Recovery = 94% Analysis Date = 07/31/08 Pct Recovery = 94% Analysis Date = 07/25/08 Pct Recovery = 94% Analysis Date = 07/25/08 Pct Recovery = 94% Analysis Date = 07/18/08 Pct Recovery = 94% Analysis Date = 07/18/08 Pct Recovery = 94% Analysis Date = 07/12/08 Pct Recovery = 94% Analysis Date = 07/12/08 Pct Recovery = 94% Analysis Date = 07/05/08 Pct Recovery = 94% Analysis Date = 07/05/08 Pct Recovery = 94% Analysis Date = 06/28/08 Pct Recovery = 94% Analysis Date = 06/28/08 Pct Recovery = 94% Analysis Date = 06/22/08 Pct Recovery = 94% Analysis Date = 06/22/08 Pct Recovery = 94% Analysis Date = 06/15/08 Pct Recovery = 95% Analysis Date = 06/15/08 Pct Recovery = 95% Analysis Date = 06/09/08 Pct Recovery = 95% Analysis Date = 06/09/08 Pct Recovery = 95% Analysis Date = 06/02/08 Pct Recovery = 95% Analysis Date = 06/02/08 Pct Recovery = 95% Analysis Date = 05/27/08 Pct Recovery = 95% Analysis Date = 05/27/08 Pct Recovery = 95% Analysis Date = 05/20/08 Pct Recovery = 95% Analysis Date = 05/20/08 Pct Recovery = 95% Analysis Date = 05/14/08 Pct Recovery = 95% Analysis Date = 05/14/08 Pct Recovery = 95% Analysis Date = 05/07/08 Pct Recovery = 96% Analysis Date = 05/07/08 Pct Recovery = 96% Analysis Date = 05/01/08 Pct Recovery = 96% Analysis Date = 05/01/08 Pct Recovery = 96% Analysis Date = 04/24/08 Pct Recovery = 96% Analysis Date = 04/24/08 Pct Recovery = 96% Analysis Date = 04/17/08 Pct Recovery = 96% Analysis Date = 04/17/08 Pct Recovery = 96% Analysis Date = 04/11/08 Pct Recovery = 96% Analysis Date = 04/11/08 Pct Recovery = 96% Analysis Date = 04/04/08 Pct Recovery = 96% Analysis Date = 04/04/08 Pct Recovery = 96% Analysis Date = 03/29/08 Pct Recovery = 97% Analysis Date = 03/29/08 Pct Recovery = 97% Analysis Date = 03/22/08 Pct Recovery = 97% Analysis Date = 03/22/08 Pct Recovery = 97% Analysis Date = 03/16/08 Pct Recovery = 97% Analysis Date = 03/16/08 Pct Recovery = 97% Analysis Date = 03/09/08 Pct Recovery = 97% Analysis Date = 03/09/08 Pct Recovery = 97% Analysis Date = 03/03/08 Pct Recovery = 97% Analysis Date = 03/03/08 Pct Recovery = 97% Analysis Date = 02/25/08 Pct Recovery = 97% Analysis Date = 02/25/08 Pct Recovery = 97% Analysis Date = 02/19/08 Pct Recovery = 97% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CARBAMAZEPINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 50 91% 14% 89% 13%
Total 50 91% 14% 89% 13%

Sample Statistics
CARBAMAZEPINE

Characteristic N % % Basis
Plotted 50 98% Spiked
Estimated Values 4 8% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 51 .  
False Negatives 1 2% 1 out of 51
Not Spiked 50 .  
False Positives 1 2% 1 out of 49