OBSP Determination:
FIPRONIL SULFIDE
METHOD: 2033 , TESTIDCODE: 62167GCM29

Analysis Date = 09/20/13 SpikeMix = . Pct Recovery = 95% Analysis Date = 01/30/06 SpikeMix = . Pct Recovery = 78% Analysis Date = 07/14/06 SpikeMix = . Pct Recovery = 76% Analysis Date = 02/19/08 SpikeMix = . Pct Recovery = 73% Analysis Date = 01/25/08 SpikeMix = . Pct Recovery = 96% Analysis Date = 01/24/08 SpikeMix = . Pct Recovery = 76% Analysis Date = 01/24/08 SpikeMix = . Pct Recovery = 90% Analysis Date = 02/06/08 SpikeMix = . Pct Recovery = 86% Analysis Date = 02/13/08 SpikeMix = . Pct Recovery = 85% Analysis Date = 02/23/10 SpikeMix = . Pct Recovery = 79% Analysis Date = 04/03/08 SpikeMix = . Pct Recovery = 98% Analysis Date = 04/18/08 SpikeMix = . Pct Recovery = 93% Analysis Date = 05/28/08 SpikeMix = . Pct Recovery = 79% Analysis Date = 08/20/08 SpikeMix = . Pct Recovery = 124% Analysis Date = 10/24/08 SpikeMix = . Pct Recovery = 91% Analysis Date = 12/06/12 SpikeMix = . Pct Recovery = 115% Analysis Date = 11/20/12 SpikeMix = . Pct Recovery = 89% Analysis Date = 08/19/13 SpikeMix = . Pct Recovery = 95% Analysis Date = 06/05/13 SpikeMix = . Pct Recovery = 114% Analysis Date = 02/12/14 SpikeMix = . Pct Recovery = 79% Analysis Date = 09/24/13 SpikeMix = . Pct Recovery = 90% Analysis Date = 01/20/11 SpikeMix = . Pct Recovery = 110% Analysis Date = 02/22/17 SpikeMix = . Pct Recovery = 75% Analysis Date = 02/22/17 SpikeMix = . Pct Recovery = 94% Analysis Date = 09/09/16 SpikeMix = . Pct Recovery = 109% Analysis Date = 04/20/11 SpikeMix = . Pct Recovery = 92% Analysis Date = 12/03/11 SpikeMix = . Pct Recovery = 78% Analysis Date = 09/13/11 SpikeMix = . Pct Recovery = 94% Analysis Date = 01/13/11 SpikeMix = . Pct Recovery = 98% Analysis Date = 02/28/11 SpikeMix = . Pct Recovery = 79% Analysis Date = 01/21/16 SpikeMix = . Pct Recovery = 88% Analysis Date = 09/24/15 SpikeMix = . Pct Recovery = 91% Analysis Date = 01/27/12 SpikeMix = . Pct Recovery = 86% Analysis Date = 12/21/11 SpikeMix = . Pct Recovery = 110% Analysis Date = 09/29/11 SpikeMix = . Pct Recovery = 93% Analysis Date = 07/07/11 SpikeMix = . Pct Recovery = 97% Analysis Date = 01/09/07 SpikeMix = . Pct Recovery = 72% Analysis Date = 01/11/11 SpikeMix = . Pct Recovery = 104% Analysis Date = 06/13/07 SpikeMix = . Pct Recovery = 97% Analysis Date = 09/12/07 SpikeMix = . Pct Recovery = 82% Analysis Date = 11/19/07 SpikeMix = . Pct Recovery = 89% Analysis Date = 04/27/07 SpikeMix = . Pct Recovery = 86% Analysis Date = 03/10/09 SpikeMix = . Pct Recovery = 114% Analysis Date = 01/29/09 SpikeMix = . Pct Recovery = 122% Analysis Date = 01/28/09 SpikeMix = . Pct Recovery = 114% Analysis Date = 05/13/09 SpikeMix = . Pct Recovery = 127% Analysis Date = 07/10/09 SpikeMix = . Pct Recovery = 60% Analysis Date = 09/09/10 SpikeMix = . Pct Recovery = 99% Analysis Date = 07/23/09 SpikeMix = . Pct Recovery = 133% Analysis Date = 03/21/17 SpikeMix = . Pct Recovery = 86% Analysis Date = 08/19/16 SpikeMix = . Pct Recovery = 103% Analysis Date = 12/14/10 SpikeMix = . Pct Recovery = 107% Analysis Date = 05/11/17 SpikeMix = . Pct Recovery = 80% Analysis Date = 08/27/16 SpikeMix = . Pct Recovery = 73% Analysis Date = 07/21/10 SpikeMix = . Pct Recovery = 75% Analysis Date = 09/15/09 SpikeMix = . Pct Recovery = 88% Analysis Date = 01/14/09 SpikeMix = . Pct Recovery = 102% Analysis Date = 01/10/09 SpikeMix = . Pct Recovery = 92% Analysis Date = 04/22/13 SpikeMix = . Pct Recovery = 96% Analysis Date = 01/15/13 SpikeMix = . Pct Recovery = 80% Analysis Date = 10/12/12 SpikeMix = . Pct Recovery = 120% Analysis Date = 05/27/09 SpikeMix = . Pct Recovery = 115% Analysis Date = 04/17/09 SpikeMix = . Pct Recovery = 120% Analysis Date = 04/02/13 SpikeMix = . Pct Recovery = 91% Analysis Date = 01/17/13 SpikeMix = . Pct Recovery = 101% Analysis Date = 10/18/12 SpikeMix = . Pct Recovery = 93% Analysis Date = 07/13/09 SpikeMix = . Pct Recovery = 110% Analysis Date = 12/14/07 SpikeMix = . Pct Recovery = 106% Analysis Date = 04/09/07 SpikeMix = . Pct Recovery = 72% Analysis Date = 09/03/09 SpikeMix = . Pct Recovery = 91% Analysis Date = 10/23/06 SpikeMix = . Pct Recovery = 106% Analysis Date = 08/15/07 SpikeMix = . Pct Recovery = 82% Analysis Date = 03/04/09 SpikeMix = . Pct Recovery = 90% Analysis Date = 06/22/11 SpikeMix = . Pct Recovery = 96% Analysis Date = 05/29/07 SpikeMix = . Pct Recovery = 108% Analysis Date = 08/27/08 SpikeMix = . Pct Recovery = 119% Analysis Date = 01/09/06 SpikeMix = . Pct Recovery = 77% Analysis Date = 10/24/08 SpikeMix = . Pct Recovery = 84% Analysis Date = 02/21/15 SpikeMix = . Pct Recovery = 90% Analysis Date = 11/19/14 SpikeMix = . Pct Recovery = 79% Analysis Date = 10/04/14 SpikeMix = . Pct Recovery = 87% Analysis Date = 07/09/14 SpikeMix = . Pct Recovery = 86% Analysis Date = 12/04/14 SpikeMix = . Pct Recovery = 99% Analysis Date = 08/27/14 SpikeMix = . Pct Recovery = 79% Analysis Date = 05/20/14 SpikeMix = . Pct Recovery = 105% Analysis Date = 03/03/09 SpikeMix = . Pct Recovery = 82% Analysis Date = 02/11/09 SpikeMix = . Pct Recovery = 102% Analysis Date = 01/30/09 SpikeMix = . Pct Recovery = 175% Analysis Date = 04/15/08 SpikeMix = . Pct Recovery = 101% Analysis Date = 02/16/07 SpikeMix = . Pct Recovery = 104% Analysis Date = 06/03/09 SpikeMix = . Pct Recovery = 116% Analysis Date = 03/05/14 SpikeMix = . Pct Recovery = 73% Analysis Date = 01/08/14 SpikeMix = . Pct Recovery = 92% Analysis Date = 11/23/13 SpikeMix = . Pct Recovery = 112% Analysis Date = 11/09/13 SpikeMix = . Pct Recovery = 85% Analysis Date = 12/30/09 SpikeMix = . Pct Recovery = 98% Analysis Date = 09/03/09 SpikeMix = . Pct Recovery = 111% Analysis Date = 06/23/08 SpikeMix = . Pct Recovery = 71% Analysis Date = 04/28/09 SpikeMix = . Pct Recovery = 125% Analysis Date = 10/30/07 SpikeMix = . Pct Recovery = 87% Analysis Date = 01/10/14 SpikeMix = . Pct Recovery = 73% Analysis Date = 07/11/13 SpikeMix = . Pct Recovery = 67% Analysis Date = 06/11/13 SpikeMix = . Pct Recovery = 106% Analysis Date = 04/13/11 SpikeMix = . Pct Recovery = 68% Analysis Date = 12/08/08 SpikeMix = . Pct Recovery = 98% Analysis Date = 05/08/12 SpikeMix = . Pct Recovery = 144% Analysis Date = 03/05/12 SpikeMix = . Pct Recovery = 92% Analysis Date = 10/25/11 SpikeMix = . Pct Recovery = 99% Analysis Date = 07/28/11 SpikeMix = . Pct Recovery = 115% Analysis Date = 05/14/11 SpikeMix = . Pct Recovery = 88% Analysis Date = 02/19/11 SpikeMix = . Pct Recovery = 72% Analysis Date = 05/19/16 SpikeMix = . Pct Recovery = 87% Analysis Date = 04/19/16 SpikeMix = . Pct Recovery = 89% Analysis Date = 02/09/16 SpikeMix = . Pct Recovery = 81% Analysis Date = 09/05/15 SpikeMix = . Pct Recovery = 68% Analysis Date = 07/21/15 SpikeMix = . Pct Recovery = 101% Analysis Date = 06/17/15 SpikeMix = . Pct Recovery = 92% Analysis Date = 06/02/12 SpikeMix = . Pct Recovery = 99% Analysis Date = 04/05/12 SpikeMix = . Pct Recovery = 134% Analysis Date = 11/17/11 SpikeMix = . Pct Recovery = 110% Analysis Date = 09/19/11 SpikeMix = . Pct Recovery = 102% Analysis Date = 01/21/11 SpikeMix = . Pct Recovery = 107% Analysis Date = 02/08/11 SpikeMix = . Pct Recovery = 69% Analysis Date = 03/23/11 SpikeMix = . Pct Recovery = 141% Analysis Date = 05/07/10 SpikeMix = . Pct Recovery = 108% Analysis Date = 08/25/10 SpikeMix = . Pct Recovery = 133% Analysis Date = 12/16/10 SpikeMix = . Pct Recovery = 124% Analysis Date = 06/03/10 SpikeMix = . Pct Recovery = 52% Analysis Date = 03/16/17 SpikeMix = . Pct Recovery = 113% Analysis Date = 01/18/17 SpikeMix = . Pct Recovery = 92% Analysis Date = 09/14/16 SpikeMix = . Pct Recovery = 89% Analysis Date = 10/19/10 SpikeMix = . Pct Recovery = 117% Analysis Date = 04/24/17 SpikeMix = . Pct Recovery = 85% Analysis Date = 02/27/17 SpikeMix = . Pct Recovery = 84% Analysis Date = 09/20/16 SpikeMix = . Pct Recovery = 94% Analysis Date = 03/24/10 SpikeMix = . Pct Recovery = 101% Analysis Date = 06/30/10 SpikeMix = . Pct Recovery = 71% Analysis Date = 09/22/14 SpikeMix = . Pct Recovery = 107% Analysis Date = 07/17/14 SpikeMix = . Pct Recovery = 82% Analysis Date = 06/30/14 SpikeMix = . Pct Recovery = 78% Analysis Date = 05/28/14 SpikeMix = . Pct Recovery = 69% Analysis Date = 01/31/15 SpikeMix = . Pct Recovery = 98% Analysis Date = 10/21/14 SpikeMix = . Pct Recovery = 104% Analysis Date = 06/26/14 SpikeMix = . Pct Recovery = 114% Analysis Date = 04/29/14 SpikeMix = . Pct Recovery = 98% Analysis Date = 03/07/13 SpikeMix = . Pct Recovery = 97% Analysis Date = 09/17/12 SpikeMix = . Pct Recovery = 112% Analysis Date = 09/05/12 SpikeMix = . Pct Recovery = 114% Analysis Date = 02/22/13 SpikeMix = . Pct Recovery = 90% Analysis Date = 08/14/12 SpikeMix = . Pct Recovery = 153% Analysis Date = 07/14/12 SpikeMix = . Pct Recovery = 110% Analysis Date = 03/05/11 SpikeMix = . Pct Recovery = 114% Analysis Date = 05/04/16 SpikeMix = . Pct Recovery = 102% Analysis Date = 04/14/16 SpikeMix = . Pct Recovery = 110% Analysis Date = 04/06/16 SpikeMix = . Pct Recovery = 97% Analysis Date = 02/09/16 SpikeMix = . Pct Recovery = 104% Analysis Date = 02/02/16 SpikeMix = . Pct Recovery = 85% Analysis Date = 01/26/16 SpikeMix = . Pct Recovery = 88% Analysis Date = 08/19/15 SpikeMix = . Pct Recovery = 75% Analysis Date = 06/10/15 SpikeMix = . Pct Recovery = 101% Analysis Date = 05/30/15 SpikeMix = . Pct Recovery = 98% Analysis Date = 05/12/15 SpikeMix = . Pct Recovery = 97% Analysis Date = 08/31/07 SpikeMix = . Pct Recovery = 112% Analysis Date = 11/13/07 SpikeMix = . Pct Recovery = 96% Analysis Date = 04/19/07 SpikeMix = . Pct Recovery = 85% Analysis Date = 07/06/07 SpikeMix = . Pct Recovery = 143% Analysis Date = 01/04/06 SpikeMix = . Pct Recovery = 95% Analysis Date = 05/10/17 Pct Recovery = 89% Analysis Date = 04/20/17 Pct Recovery = 89% Analysis Date = 04/20/17 Pct Recovery = 89% Analysis Date = 03/30/17 Pct Recovery = 89% Analysis Date = 03/30/17 Pct Recovery = 89% Analysis Date = 03/09/17 Pct Recovery = 89% Analysis Date = 03/09/17 Pct Recovery = 89% Analysis Date = 02/17/17 Pct Recovery = 89% Analysis Date = 02/17/17 Pct Recovery = 89% Analysis Date = 01/27/17 Pct Recovery = 89% Analysis Date = 01/27/17 Pct Recovery = 89% Analysis Date = 01/06/17 Pct Recovery = 90% Analysis Date = 01/06/17 Pct Recovery = 90% Analysis Date = 12/16/16 Pct Recovery = 90% Analysis Date = 12/16/16 Pct Recovery = 90% Analysis Date = 11/26/16 Pct Recovery = 90% Analysis Date = 11/26/16 Pct Recovery = 90% Analysis Date = 11/05/16 Pct Recovery = 90% Analysis Date = 11/05/16 Pct Recovery = 90% Analysis Date = 10/15/16 Pct Recovery = 90% Analysis Date = 10/15/16 Pct Recovery = 90% Analysis Date = 09/25/16 Pct Recovery = 90% Analysis Date = 09/25/16 Pct Recovery = 90% Analysis Date = 09/04/16 Pct Recovery = 90% Analysis Date = 09/04/16 Pct Recovery = 90% Analysis Date = 08/14/16 Pct Recovery = 90% Analysis Date = 08/14/16 Pct Recovery = 90% Analysis Date = 07/24/16 Pct Recovery = 90% Analysis Date = 07/24/16 Pct Recovery = 90% Analysis Date = 07/04/16 Pct Recovery = 90% Analysis Date = 07/04/16 Pct Recovery = 90% Analysis Date = 06/13/16 Pct Recovery = 90% Analysis Date = 06/13/16 Pct Recovery = 90% Analysis Date = 05/23/16 Pct Recovery = 90% Analysis Date = 05/23/16 Pct Recovery = 90% Analysis Date = 05/02/16 Pct Recovery = 91% Analysis Date = 05/02/16 Pct Recovery = 91% Analysis Date = 04/12/16 Pct Recovery = 91% Analysis Date = 04/12/16 Pct Recovery = 91% Analysis Date = 03/22/16 Pct Recovery = 91% Analysis Date = 03/22/16 Pct Recovery = 91% Analysis Date = 03/01/16 Pct Recovery = 91% Analysis Date = 03/01/16 Pct Recovery = 91% Analysis Date = 02/10/16 Pct Recovery = 91% Analysis Date = 02/10/16 Pct Recovery = 91% Analysis Date = 01/20/16 Pct Recovery = 91% Analysis Date = 01/20/16 Pct Recovery = 91% Analysis Date = 12/30/15 Pct Recovery = 91% Analysis Date = 12/30/15 Pct Recovery = 91% Analysis Date = 12/09/15 Pct Recovery = 91% Analysis Date = 12/09/15 Pct Recovery = 91% Analysis Date = 11/19/15 Pct Recovery = 91% Analysis Date = 11/19/15 Pct Recovery = 91% Analysis Date = 10/29/15 Pct Recovery = 91% Analysis Date = 10/29/15 Pct Recovery = 91% Analysis Date = 10/08/15 Pct Recovery = 92% Analysis Date = 10/08/15 Pct Recovery = 92% Analysis Date = 09/17/15 Pct Recovery = 92% Analysis Date = 09/17/15 Pct Recovery = 92% Analysis Date = 08/28/15 Pct Recovery = 92% Analysis Date = 08/28/15 Pct Recovery = 92% Analysis Date = 08/07/15 Pct Recovery = 92% Analysis Date = 08/07/15 Pct Recovery = 92% Analysis Date = 07/17/15 Pct Recovery = 92% Analysis Date = 07/17/15 Pct Recovery = 92% Analysis Date = 06/27/15 Pct Recovery = 92% Analysis Date = 06/27/15 Pct Recovery = 92% Analysis Date = 06/06/15 Pct Recovery = 92% Analysis Date = 06/06/15 Pct Recovery = 92% Analysis Date = 05/16/15 Pct Recovery = 92% Analysis Date = 05/16/15 Pct Recovery = 92% Analysis Date = 04/25/15 Pct Recovery = 92% Analysis Date = 04/25/15 Pct Recovery = 92% Analysis Date = 04/05/15 Pct Recovery = 93% Analysis Date = 04/05/15 Pct Recovery = 93% Analysis Date = 03/15/15 Pct Recovery = 93% Analysis Date = 03/15/15 Pct Recovery = 93% Analysis Date = 02/22/15 Pct Recovery = 93% Analysis Date = 02/22/15 Pct Recovery = 93% Analysis Date = 02/01/15 Pct Recovery = 93% Analysis Date = 02/01/15 Pct Recovery = 93% Analysis Date = 01/12/15 Pct Recovery = 93% Analysis Date = 01/12/15 Pct Recovery = 93% Analysis Date = 12/22/14 Pct Recovery = 93% Analysis Date = 12/22/14 Pct Recovery = 93% Analysis Date = 12/01/14 Pct Recovery = 93% Analysis Date = 12/01/14 Pct Recovery = 93% Analysis Date = 11/11/14 Pct Recovery = 93% Analysis Date = 11/11/14 Pct Recovery = 93% Analysis Date = 10/21/14 Pct Recovery = 94% Analysis Date = 10/21/14 Pct Recovery = 94% Analysis Date = 09/30/14 Pct Recovery = 94% Analysis Date = 09/30/14 Pct Recovery = 94% Analysis Date = 09/09/14 Pct Recovery = 94% Analysis Date = 09/09/14 Pct Recovery = 94% Analysis Date = 08/20/14 Pct Recovery = 94% Analysis Date = 08/20/14 Pct Recovery = 94% Analysis Date = 07/30/14 Pct Recovery = 94% Analysis Date = 07/30/14 Pct Recovery = 94% Analysis Date = 07/09/14 Pct Recovery = 94% Analysis Date = 07/09/14 Pct Recovery = 94% Analysis Date = 06/19/14 Pct Recovery = 94% Analysis Date = 06/19/14 Pct Recovery = 94% Analysis Date = 05/29/14 Pct Recovery = 94% Analysis Date = 05/29/14 Pct Recovery = 94% Analysis Date = 05/08/14 Pct Recovery = 95% Analysis Date = 05/08/14 Pct Recovery = 95% Analysis Date = 04/17/14 Pct Recovery = 95% Analysis Date = 04/17/14 Pct Recovery = 95% Analysis Date = 03/28/14 Pct Recovery = 95% Analysis Date = 03/28/14 Pct Recovery = 95% Analysis Date = 03/07/14 Pct Recovery = 95% Analysis Date = 03/07/14 Pct Recovery = 95% Analysis Date = 02/14/14 Pct Recovery = 95% Analysis Date = 02/14/14 Pct Recovery = 95% Analysis Date = 01/24/14 Pct Recovery = 95% Analysis Date = 01/24/14 Pct Recovery = 95% Analysis Date = 01/04/14 Pct Recovery = 95% Analysis Date = 01/04/14 Pct Recovery = 95% Analysis Date = 12/14/13 Pct Recovery = 96% Analysis Date = 12/14/13 Pct Recovery = 96% Analysis Date = 11/23/13 Pct Recovery = 96% Analysis Date = 11/23/13 Pct Recovery = 96% Analysis Date = 11/03/13 Pct Recovery = 96% Analysis Date = 11/03/13 Pct Recovery = 96% Analysis Date = 10/13/13 Pct Recovery = 96% Analysis Date = 10/13/13 Pct Recovery = 96% Analysis Date = 09/22/13 Pct Recovery = 96% Analysis Date = 09/22/13 Pct Recovery = 96% Analysis Date = 09/01/13 Pct Recovery = 96% Analysis Date = 09/01/13 Pct Recovery = 96% Analysis Date = 08/12/13 Pct Recovery = 96% Analysis Date = 08/12/13 Pct Recovery = 96% Analysis Date = 07/22/13 Pct Recovery = 96% Analysis Date = 07/22/13 Pct Recovery = 96% Analysis Date = 07/01/13 Pct Recovery = 97% Analysis Date = 07/01/13 Pct Recovery = 97% Analysis Date = 06/10/13 Pct Recovery = 97% Analysis Date = 06/10/13 Pct Recovery = 97% Analysis Date = 05/21/13 Pct Recovery = 97% Analysis Date = 05/21/13 Pct Recovery = 97% Analysis Date = 04/30/13 Pct Recovery = 97% Analysis Date = 04/30/13 Pct Recovery = 97% Analysis Date = 04/09/13 Pct Recovery = 97% Analysis Date = 04/09/13 Pct Recovery = 97% Analysis Date = 03/20/13 Pct Recovery = 97% Analysis Date = 03/20/13 Pct Recovery = 97% Analysis Date = 02/27/13 Pct Recovery = 97% Analysis Date = 02/27/13 Pct Recovery = 97% Analysis Date = 02/06/13 Pct Recovery = 97% Analysis Date = 02/06/13 Pct Recovery = 97% Analysis Date = 01/16/13 Pct Recovery = 98% Analysis Date = 01/16/13 Pct Recovery = 98% Analysis Date = 12/27/12 Pct Recovery = 98% Analysis Date = 12/27/12 Pct Recovery = 98% Analysis Date = 12/06/12 Pct Recovery = 98% Analysis Date = 12/06/12 Pct Recovery = 98% Analysis Date = 11/15/12 Pct Recovery = 98% Analysis Date = 11/15/12 Pct Recovery = 98% Analysis Date = 10/25/12 Pct Recovery = 98% Analysis Date = 10/25/12 Pct Recovery = 98% Analysis Date = 10/05/12 Pct Recovery = 98% Analysis Date = 10/05/12 Pct Recovery = 98% Analysis Date = 09/14/12 Pct Recovery = 98% Analysis Date = 09/14/12 Pct Recovery = 98% Analysis Date = 08/24/12 Pct Recovery = 98% Analysis Date = 08/24/12 Pct Recovery = 98% Analysis Date = 08/04/12 Pct Recovery = 99% Analysis Date = 08/04/12 Pct Recovery = 99% Analysis Date = 07/14/12 Pct Recovery = 99% Analysis Date = 07/14/12 Pct Recovery = 99% Analysis Date = 06/23/12 Pct Recovery = 99% Analysis Date = 06/23/12 Pct Recovery = 99% Analysis Date = 06/02/12 Pct Recovery = 99% Analysis Date = 06/02/12 Pct Recovery = 99% Analysis Date = 05/13/12 Pct Recovery = 99% Analysis Date = 05/13/12 Pct Recovery = 99% Analysis Date = 04/22/12 Pct Recovery = 99% Analysis Date = 04/22/12 Pct Recovery = 99% Analysis Date = 04/01/12 Pct Recovery = 99% Analysis Date = 04/01/12 Pct Recovery = 99% Analysis Date = 03/12/12 Pct Recovery = 99% Analysis Date = 03/12/12 Pct Recovery = 99% Analysis Date = 02/20/12 Pct Recovery = 100% Analysis Date = 02/20/12 Pct Recovery = 100% Analysis Date = 01/30/12 Pct Recovery = 100% Analysis Date = 01/30/12 Pct Recovery = 100% Analysis Date = 01/09/12 Pct Recovery = 100% Analysis Date = 01/09/12 Pct Recovery = 100% Analysis Date = 12/20/11 Pct Recovery = 100% Analysis Date = 12/20/11 Pct Recovery = 100% Analysis Date = 11/29/11 Pct Recovery = 100% Analysis Date = 11/29/11 Pct Recovery = 100% Analysis Date = 11/08/11 Pct Recovery = 100% Analysis Date = 11/08/11 Pct Recovery = 100% Analysis Date = 10/18/11 Pct Recovery = 100% Analysis Date = 10/18/11 Pct Recovery = 100% Analysis Date = 09/28/11 Pct Recovery = 100% Analysis Date = 09/28/11 Pct Recovery = 100% Analysis Date = 09/07/11 Pct Recovery = 101% Analysis Date = 09/07/11 Pct Recovery = 101% Analysis Date = 08/17/11 Pct Recovery = 101% Analysis Date = 08/17/11 Pct Recovery = 101% Analysis Date = 07/28/11 Pct Recovery = 101% Analysis Date = 07/28/11 Pct Recovery = 101% Analysis Date = 07/07/11 Pct Recovery = 101% Analysis Date = 07/07/11 Pct Recovery = 101% Analysis Date = 06/16/11 Pct Recovery = 101% Analysis Date = 06/16/11 Pct Recovery = 101% Analysis Date = 05/26/11 Pct Recovery = 101% Analysis Date = 05/26/11 Pct Recovery = 101% Analysis Date = 05/06/11 Pct Recovery = 101% Analysis Date = 05/06/11 Pct Recovery = 101% Analysis Date = 04/15/11 Pct Recovery = 101% Analysis Date = 04/15/11 Pct Recovery = 101% Analysis Date = 03/25/11 Pct Recovery = 101% Analysis Date = 03/25/11 Pct Recovery = 101% Analysis Date = 03/04/11 Pct Recovery = 101% Analysis Date = 03/04/11 Pct Recovery = 101% Analysis Date = 02/12/11 Pct Recovery = 101% Analysis Date = 02/12/11 Pct Recovery = 101% Analysis Date = 01/22/11 Pct Recovery = 101% Analysis Date = 01/22/11 Pct Recovery = 101% Analysis Date = 01/01/11 Pct Recovery = 101% Analysis Date = 01/01/11 Pct Recovery = 101% Analysis Date = 12/12/10 Pct Recovery = 101% Analysis Date = 12/12/10 Pct Recovery = 101% Analysis Date = 11/21/10 Pct Recovery = 101% Analysis Date = 11/21/10 Pct Recovery = 101% Analysis Date = 10/31/10 Pct Recovery = 101% Analysis Date = 10/31/10 Pct Recovery = 101% Analysis Date = 10/10/10 Pct Recovery = 101% Analysis Date = 10/10/10 Pct Recovery = 101% Analysis Date = 09/20/10 Pct Recovery = 101% Analysis Date = 09/20/10 Pct Recovery = 101% Analysis Date = 08/30/10 Pct Recovery = 101% Analysis Date = 08/30/10 Pct Recovery = 101% Analysis Date = 08/09/10 Pct Recovery = 101% Analysis Date = 08/09/10 Pct Recovery = 101% Analysis Date = 07/19/10 Pct Recovery = 101% Analysis Date = 07/19/10 Pct Recovery = 101% Analysis Date = 06/29/10 Pct Recovery = 101% Analysis Date = 06/29/10 Pct Recovery = 101% Analysis Date = 06/08/10 Pct Recovery = 101% Analysis Date = 06/08/10 Pct Recovery = 101% Analysis Date = 05/18/10 Pct Recovery = 101% Analysis Date = 05/18/10 Pct Recovery = 101% Analysis Date = 04/28/10 Pct Recovery = 101% Analysis Date = 04/28/10 Pct Recovery = 101% Analysis Date = 04/07/10 Pct Recovery = 101% Analysis Date = 04/07/10 Pct Recovery = 101% Analysis Date = 03/17/10 Pct Recovery = 101% Analysis Date = 03/17/10 Pct Recovery = 101% Analysis Date = 02/24/10 Pct Recovery = 101% Analysis Date = 02/24/10 Pct Recovery = 101% Analysis Date = 02/04/10 Pct Recovery = 101% Analysis Date = 02/04/10 Pct Recovery = 101% Analysis Date = 01/14/10 Pct Recovery = 100% Analysis Date = 01/14/10 Pct Recovery = 100% Analysis Date = 12/24/09 Pct Recovery = 100% Analysis Date = 12/24/09 Pct Recovery = 100% Analysis Date = 12/04/09 Pct Recovery = 100% Analysis Date = 12/04/09 Pct Recovery = 100% Analysis Date = 11/13/09 Pct Recovery = 100% Analysis Date = 11/13/09 Pct Recovery = 100% Analysis Date = 10/23/09 Pct Recovery = 100% Analysis Date = 10/23/09 Pct Recovery = 100% Analysis Date = 10/02/09 Pct Recovery = 100% Analysis Date = 10/02/09 Pct Recovery = 100% Analysis Date = 09/12/09 Pct Recovery = 100% Analysis Date = 09/12/09 Pct Recovery = 100% Analysis Date = 08/22/09 Pct Recovery = 100% Analysis Date = 08/22/09 Pct Recovery = 100% Analysis Date = 08/01/09 Pct Recovery = 100% Analysis Date = 08/01/09 Pct Recovery = 100% Analysis Date = 07/11/09 Pct Recovery = 100% Analysis Date = 07/11/09 Pct Recovery = 100% Analysis Date = 06/21/09 Pct Recovery = 99% Analysis Date = 06/21/09 Pct Recovery = 99% Analysis Date = 05/31/09 Pct Recovery = 99% Analysis Date = 05/31/09 Pct Recovery = 99% Analysis Date = 05/10/09 Pct Recovery = 99% Analysis Date = 05/10/09 Pct Recovery = 99% Analysis Date = 04/20/09 Pct Recovery = 99% Analysis Date = 04/20/09 Pct Recovery = 99% Analysis Date = 03/30/09 Pct Recovery = 99% Analysis Date = 03/30/09 Pct Recovery = 99% Analysis Date = 03/09/09 Pct Recovery = 99% Analysis Date = 03/09/09 Pct Recovery = 99% Analysis Date = 02/16/09 Pct Recovery = 99% Analysis Date = 02/16/09 Pct Recovery = 99% Analysis Date = 01/27/09 Pct Recovery = 99% Analysis Date = 01/27/09 Pct Recovery = 99% Analysis Date = 01/06/09 Pct Recovery = 99% Analysis Date = 01/06/09 Pct Recovery = 99% Analysis Date = 12/16/08 Pct Recovery = 98% Analysis Date = 12/16/08 Pct Recovery = 98% Analysis Date = 11/25/08 Pct Recovery = 98% Analysis Date = 11/25/08 Pct Recovery = 98% Analysis Date = 11/05/08 Pct Recovery = 98% Analysis Date = 11/05/08 Pct Recovery = 98% Analysis Date = 10/15/08 Pct Recovery = 98% Analysis Date = 10/15/08 Pct Recovery = 98% Analysis Date = 09/24/08 Pct Recovery = 98% Analysis Date = 09/24/08 Pct Recovery = 98% Analysis Date = 09/04/08 Pct Recovery = 98% Analysis Date = 09/04/08 Pct Recovery = 98% Analysis Date = 08/14/08 Pct Recovery = 98% Analysis Date = 08/14/08 Pct Recovery = 98% Analysis Date = 07/24/08 Pct Recovery = 97% Analysis Date = 07/24/08 Pct Recovery = 97% Analysis Date = 07/03/08 Pct Recovery = 97% Analysis Date = 07/03/08 Pct Recovery = 97% Analysis Date = 06/13/08 Pct Recovery = 97% Analysis Date = 06/13/08 Pct Recovery = 97% Analysis Date = 05/23/08 Pct Recovery = 97% Analysis Date = 05/23/08 Pct Recovery = 97% Analysis Date = 05/02/08 Pct Recovery = 97% Analysis Date = 05/02/08 Pct Recovery = 97% Analysis Date = 04/11/08 Pct Recovery = 97% Analysis Date = 04/11/08 Pct Recovery = 97% Analysis Date = 03/22/08 Pct Recovery = 96% Analysis Date = 03/22/08 Pct Recovery = 96% Analysis Date = 03/01/08 Pct Recovery = 96% Analysis Date = 03/01/08 Pct Recovery = 96% Analysis Date = 02/09/08 Pct Recovery = 96% Analysis Date = 02/09/08 Pct Recovery = 96% Analysis Date = 01/20/08 Pct Recovery = 96% Analysis Date = 01/20/08 Pct Recovery = 96% Analysis Date = 12/30/07 Pct Recovery = 96% Analysis Date = 12/30/07 Pct Recovery = 96% Analysis Date = 12/09/07 Pct Recovery = 95% Analysis Date = 12/09/07 Pct Recovery = 95% Analysis Date = 11/18/07 Pct Recovery = 95% Analysis Date = 11/18/07 Pct Recovery = 95% Analysis Date = 10/29/07 Pct Recovery = 95% Analysis Date = 10/29/07 Pct Recovery = 95% Analysis Date = 10/08/07 Pct Recovery = 95% Analysis Date = 10/08/07 Pct Recovery = 95% Analysis Date = 09/17/07 Pct Recovery = 95% Analysis Date = 09/17/07 Pct Recovery = 95% Analysis Date = 08/28/07 Pct Recovery = 94% Analysis Date = 08/28/07 Pct Recovery = 94% Analysis Date = 08/07/07 Pct Recovery = 94% Analysis Date = 08/07/07 Pct Recovery = 94% Analysis Date = 07/17/07 Pct Recovery = 94% Analysis Date = 07/17/07 Pct Recovery = 94% Analysis Date = 06/26/07 Pct Recovery = 94% Analysis Date = 06/26/07 Pct Recovery = 94% Analysis Date = 06/06/07 Pct Recovery = 94% Analysis Date = 06/06/07 Pct Recovery = 94% Analysis Date = 05/16/07 Pct Recovery = 93% Analysis Date = 05/16/07 Pct Recovery = 93% Analysis Date = 04/25/07 Pct Recovery = 93% Analysis Date = 04/25/07 Pct Recovery = 93% Analysis Date = 04/04/07 Pct Recovery = 93% Analysis Date = 04/04/07 Pct Recovery = 93% Analysis Date = 03/15/07 Pct Recovery = 93% Analysis Date = 03/15/07 Pct Recovery = 93% Analysis Date = 02/22/07 Pct Recovery = 93% Analysis Date = 02/22/07 Pct Recovery = 93% Analysis Date = 02/01/07 Pct Recovery = 92% Analysis Date = 02/01/07 Pct Recovery = 92% Analysis Date = 01/12/07 Pct Recovery = 92% Analysis Date = 01/12/07 Pct Recovery = 92% Analysis Date = 12/22/06 Pct Recovery = 92% Analysis Date = 12/22/06 Pct Recovery = 92% Analysis Date = 12/01/06 Pct Recovery = 92% Analysis Date = 12/01/06 Pct Recovery = 92% Analysis Date = 11/10/06 Pct Recovery = 91% Analysis Date = 11/10/06 Pct Recovery = 91% Analysis Date = 10/21/06 Pct Recovery = 91% Analysis Date = 10/21/06 Pct Recovery = 91% Analysis Date = 09/30/06 Pct Recovery = 91% Analysis Date = 09/30/06 Pct Recovery = 91% Analysis Date = 09/09/06 Pct Recovery = 91% Analysis Date = 09/09/06 Pct Recovery = 91% Analysis Date = 08/19/06 Pct Recovery = 91% Analysis Date = 08/19/06 Pct Recovery = 91% Analysis Date = 07/30/06 Pct Recovery = 90% Analysis Date = 07/30/06 Pct Recovery = 90% Analysis Date = 07/09/06 Pct Recovery = 90% Analysis Date = 07/09/06 Pct Recovery = 90% Analysis Date = 06/18/06 Pct Recovery = 90% Analysis Date = 06/18/06 Pct Recovery = 90% Analysis Date = 05/29/06 Pct Recovery = 90% Analysis Date = 05/29/06 Pct Recovery = 90% Analysis Date = 05/08/06 Pct Recovery = 89% Analysis Date = 05/08/06 Pct Recovery = 89% Analysis Date = 04/17/06 Pct Recovery = 89% Analysis Date = 04/17/06 Pct Recovery = 89% Analysis Date = 03/27/06 Pct Recovery = 89% Analysis Date = 03/27/06 Pct Recovery = 89% Analysis Date = 03/07/06 Pct Recovery = 89% Analysis Date = 03/07/06 Pct Recovery = 89% Analysis Date = 02/14/06 Pct Recovery = 89% Analysis Date = 02/14/06 Pct Recovery = 89% Analysis Date = 01/24/06 Pct Recovery = 88% Analysis Date = 01/24/06 Pct Recovery = 88% Analysis Date = 01/04/06 Pct Recovery = 88% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FIPRONIL SULFIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 167 97% 18% 95% 16%
Total 167 97% 18% 95% 16%

Sample Statistics
FIPRONIL SULFIDE

Characteristic N % % Basis
Plotted 167 99% Spiked
Estimated Values 2 1% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 168 .  
False Negatives 1 1% 1 out of 168
Not Spiked 214 .  
False Positives 30 14% 30 out of 214