BQS OBSP Determination:
4-CHLOROTOLUENE
METHOD: 2021 , TESTIDCODE: 77277GCM66
Open Data Set

Analysis Date = 07/09/99 SpikeMix = ERA 1210-98-04B: 30 µl Pct Recovery = 94% Analysis Date = 11/29/99 SpikeMix = ERA 1210-98-04B: 30 µl Pct Recovery = 99% Analysis Date = 11/09/99 SpikeMix = ERA 1210-98-04B: 30 µl Pct Recovery = 97% Analysis Date = 09/09/99 SpikeMix = ERA 1210-98-04B: 30 µl Pct Recovery = 123% Analysis Date = 12/22/12 SpikeMix = NSI 062112-01VOA: 40 µl & Supelco LB92787: 40 µl Pct Recovery = 99% Analysis Date = 01/19/13 SpikeMix = Accu 212051193: 40 µl & Abs 051712: 40 µl Pct Recovery = 96% Analysis Date = 05/24/99 SpikeMix = ERA 1210-98-04B: 10 µl Pct Recovery = 106% Analysis Date = 07/20/99 SpikeMix = ERA 1210-98-04B: 10 µl Pct Recovery = 130% Analysis Date = 10/13/99 SpikeMix = ERA 1210-98-04B: 10 µl Pct Recovery = 107% Analysis Date = 09/11/12 SpikeMix = NSI 062112-01VOA: 20 µl & Supelco LB92787: 20 µl Pct Recovery = 95% Analysis Date = 07/30/12 SpikeMix = Supelco LB92787: 20 µl & Abs 051712: 20 µl Pct Recovery = 96% Analysis Date = 11/08/12 SpikeMix = Crescent 05BB048: 20 µl & Accu 212051193: 20 µl Pct Recovery = 105% Analysis Date = 11/20/05 SpikeMix = Accu B5070191: 30 µl & Ultra CB-1578: 50 µl Pct Recovery = 94% Analysis Date = 04/07/06 SpikeMix = Accu B5070191: 30 µl & NSI 080405-01VOC: 20 µl Pct Recovery = 112% Analysis Date = 10/28/05 SpikeMix = Supelco LB31918: 30 µl & Accu B5070191: 30 µl Pct Recovery = 108% Analysis Date = 06/23/05 SpikeMix = Crescent 07DD035: 40 µl Pct Recovery = 95% Analysis Date = 04/06/05 SpikeMix = Crescent 07DD035: 40 µl Pct Recovery = 85% Analysis Date = 10/19/01 SpikeMix = ERA 1128-00-06B: 5 µl Pct Recovery = 95% Analysis Date = 07/31/01 SpikeMix = ERA 1128-00-06B: 5 µl Pct Recovery = 89% Analysis Date = 05/25/01 SpikeMix = ERA 1128-00-06B: 5 µl Pct Recovery = 111% Analysis Date = 05/03/01 SpikeMix = ERA 1128-00-06B: 5 µl Pct Recovery = 100% Analysis Date = 02/07/01 SpikeMix = ERA 1128-00-06B: 5 µl Pct Recovery = 101% Analysis Date = 05/03/13 SpikeMix = Supelco LB92787: 10 µl & ChemService 472200: 10 µl Pct Recovery = 81% Analysis Date = 03/29/13 SpikeMix = Supelco LB92787: 10 µl & ChemService 472200: 10 µl Pct Recovery = 84% Analysis Date = 02/28/13 SpikeMix = NSI 062112-01VOA: 10 µl & Accu 212051193: 10 µl Pct Recovery = 100% Analysis Date = 07/19/12 SpikeMix = Crescent 05BB048: 10 µl & Accu 212051193: 10 µl Pct Recovery = 105% Analysis Date = 09/25/03 SpikeMix = ERA 0828-02-09VOC: 40 µl Pct Recovery = 90% Analysis Date = 06/20/03 SpikeMix = ERA 0828-02-09VOC: 40 µl Pct Recovery = 96% Analysis Date = 03/06/03 SpikeMix = ERA 0828-02-09VOC: 40 µl Pct Recovery = 92% Analysis Date = 01/16/03 SpikeMix = ERA 0828-02-09VOC: 40 µl Pct Recovery = 107% Analysis Date = 02/26/99 SpikeMix = NSI Q-16750-50 101497: 25 µl Pct Recovery = 91% Analysis Date = 11/20/98 SpikeMix = NSI Q-16750-50 101497: 25 µl Pct Recovery = 109% Analysis Date = 05/24/02 SpikeMix = NSI Q-3183: 20 µl Pct Recovery = 102% Analysis Date = 02/22/02 SpikeMix = NSI Q-3183: 20 µl Pct Recovery = 93% Analysis Date = 12/16/98 SpikeMix = NSI Q-2002: 40 µl Pct Recovery = 101% Analysis Date = 06/30/09 SpikeMix = Ultra CE-2869: 40 µl Pct Recovery = 80% Analysis Date = 06/17/09 SpikeMix = Ultra CE-2869: 40 µl Pct Recovery = 77% Analysis Date = 04/21/09 SpikeMix = Abs 080408VOC: 40 µl Pct Recovery = 82% Analysis Date = 01/27/09 SpikeMix = Abs 080408VOC: 40 µl Pct Recovery = 90% Analysis Date = 10/04/03 SpikeMix = ERA 0828-02-09VOC: 15 µl Pct Recovery = 101% Analysis Date = 07/19/03 SpikeMix = ERA 0828-02-09VOC: 15 µl Pct Recovery = 94% Analysis Date = 05/12/03 SpikeMix = ERA 0828-02-09VOC: 15 µl Pct Recovery = 93% Analysis Date = 02/20/03 SpikeMix = ERA 0828-02-09VOC: 15 µl Pct Recovery = 90% Analysis Date = 09/05/02 SpikeMix = ERA 0830-01-06.1VOC: 40 µl Pct Recovery = 96% Analysis Date = 07/19/02 SpikeMix = ERA 0830-01-06.1VOC: 40 µl Pct Recovery = 83% Analysis Date = 04/26/02 SpikeMix = ERA 0830-01-06.1VOC: 40 µl Pct Recovery = 101% Analysis Date = 01/11/02 SpikeMix = ERA 0830-01-06.1VOC: 40 µl Pct Recovery = 90% Analysis Date = 03/31/99 SpikeMix = NSI Q-16750-50 101497: 10 µl Pct Recovery = 89% Analysis Date = 01/20/99 SpikeMix = NSI Q-16750-50 101497: 10 µl Pct Recovery = 96% Analysis Date = 11/17/01 SpikeMix = NSI 111700VOC: 25 µl Pct Recovery = 94% Analysis Date = 08/23/01 SpikeMix = NSI 111700VOC: 25 µl Pct Recovery = 87% Analysis Date = 06/01/01 SpikeMix = NSI 111700VOC: 25 µl Pct Recovery = 102% Analysis Date = 03/07/01 SpikeMix = NSI 111700VOC: 25 µl Pct Recovery = 103% Analysis Date = 04/04/02 SpikeMix = NSI Q-3183: 10 µl Pct Recovery = 104% Analysis Date = 01/04/02 SpikeMix = NSI Q-3183: 10 µl Pct Recovery = 94% Analysis Date = 08/11/09 SpikeMix = Ultra CE-2869: 20 µl Pct Recovery = 70% Analysis Date = 05/13/09 SpikeMix = Ultra CE-2869: 20 µl Pct Recovery = 95% Analysis Date = 03/31/09 SpikeMix = Ultra CE-2869: 20 µl Pct Recovery = 90% Analysis Date = 02/18/09 SpikeMix = Ultra CE-2869: 20 µl Pct Recovery = 90% Analysis Date = 05/17/06 SpikeMix = Accu B5070191: 5 µl & NSI 080405-01VOC: 5 µl & Ultra CB-1578: 10 µl Pct Recovery = 96% Analysis Date = 12/08/05 SpikeMix = Accu B5070191: 5 µl & NSI 080405-01VOC: 5 µl & Ultra CB-1578: 10 µl Pct Recovery = 106% Analysis Date = 02/15/06 SpikeMix = Supelco LB31918: 5 µl & Accu B5070191: 5 µl & Ultra CB-1578: 10 µl Pct Recovery = 106% Analysis Date = 11/29/05 SpikeMix = Supelco LB31918: 5 µl & Accu B5070191: 5 µl & Ultra CB-1578: 10 µl Pct Recovery = 127% Analysis Date = 07/28/06 SpikeMix = Accu B5070191: 5 µl & Ultra CB-1578: 10 µl Pct Recovery = 96% Analysis Date = 06/06/06 SpikeMix = Accu B5070191: 5 µl & NSI 080405-01VOC: 5 µl Pct Recovery = 122% Analysis Date = 01/05/06 SpikeMix = Supelco LB31918: 5 µl & Accu B5070191: 5 µl Pct Recovery = 106% Analysis Date = 05/25/12 SpikeMix = NSI 062310-01: 40 µl Pct Recovery = 72% Analysis Date = 05/08/12 SpikeMix = NSI 062310-01: 40 µl Pct Recovery = 72% Analysis Date = 11/24/11 SpikeMix = NSI 062310-01: 40 µl Pct Recovery = 87% Analysis Date = 06/10/11 SpikeMix = NSI 062310-01: 40 µl Pct Recovery = 68% Analysis Date = 04/13/11 SpikeMix = NSI 062310-01: 40 µl Pct Recovery = 58% Analysis Date = 01/22/11 SpikeMix = NSI 062310-01: 40 µl Pct Recovery = 80% Analysis Date = 08/29/09 SpikeMix = Abs 080408VOC: 20 µl Pct Recovery = 76% Analysis Date = 07/17/09 SpikeMix = Abs 080408VOC: 20 µl Pct Recovery = 71% Analysis Date = 06/09/09 SpikeMix = Abs 080408VOC: 20 µl Pct Recovery = 71% Analysis Date = 03/14/09 SpikeMix = Abs 080408VOC: 20 µl Pct Recovery = 82% Analysis Date = 08/15/05 SpikeMix = Protocol R1040726010: 5 µl & Ultra CA-1229: 10 µl Pct Recovery = 100% Analysis Date = 03/04/05 SpikeMix = Protocol R1040726010: 5 µl & Ultra CA-1229: 10 µl Pct Recovery = 94% Analysis Date = 05/11/05 SpikeMix = Protocol R1040726010: 5 µl & NSI 081104-01VOC: 10 µl Pct Recovery = 106% Analysis Date = 08/21/10 SpikeMix = Spex Organics C1090901006: 30 µl Pct Recovery = 82% Analysis Date = 06/09/10 SpikeMix = Spex Organics C1090901006: 30 µl Pct Recovery = 88% Analysis Date = 03/17/10 SpikeMix = Spex Organics C1090901006: 30 µl Pct Recovery = 85% Analysis Date = 12/15/09 SpikeMix = Spex Organics C1090901006: 30 µl Pct Recovery = 94% Analysis Date = 06/22/05 SpikeMix = Protocol R1040726010: 5 µl Pct Recovery = 106% Analysis Date = 04/09/05 SpikeMix = Protocol R1040726010: 5 µl Pct Recovery = 111% Analysis Date = 02/01/05 SpikeMix = Protocol R1040726010: 5 µl Pct Recovery = 117% Analysis Date = 08/11/07 SpikeMix = Crescent 07FF068: 40 µl Pct Recovery = 81% Analysis Date = 06/16/07 SpikeMix = Crescent 07FF068: 40 µl Pct Recovery = 100% Analysis Date = 04/20/07 SpikeMix = Crescent 07FF068: 40 µl Pct Recovery = 88% Analysis Date = 03/01/07 SpikeMix = Crescent 07FF068: 40 µl Pct Recovery = 88% Analysis Date = 07/30/05 SpikeMix = Crescent 07DD035: 5 µl & Ultra CA-1229: 10 µl Pct Recovery = 57% Analysis Date = 01/27/05 SpikeMix = Crescent 07DD035: 5 µl & NSI 081104-01VOC: 10 µl Pct Recovery = 100% Analysis Date = 05/10/05 SpikeMix = Crescent 07DD035: 5 µl Pct Recovery = 71% Analysis Date = 02/25/05 SpikeMix = Crescent 07DD035: 5 µl Pct Recovery = 86% Analysis Date = 03/01/14 SpikeMix = NSI 053013: 20 µl & Supelco LC00154: 20 µl Pct Recovery = 63% Analysis Date = 07/24/13 SpikeMix = NSI 053013: 20 µl & Supelco LC00154: 20 µl Pct Recovery = 73% Analysis Date = 09/17/13 SpikeMix = Crescent 04CC151: 20 µl & Supelco LC00154: 20 µl Pct Recovery = 73% Analysis Date = 01/29/14 SpikeMix = Supelco LC00154: 20 µl & ChemService 1530700: 20 µl Pct Recovery = 81% Analysis Date = 09/17/13 SpikeMix = Supelco LC00154: 20 µl & ChemService 1530700: 20 µl Pct Recovery = 78% Analysis Date = 08/06/13 SpikeMix = Supelco LC00154: 20 µl & Abs 051413: 20 µl Pct Recovery = 65% Analysis Date = 11/01/13 SpikeMix = Accu 213041120: 20 µl & ChemService 1530700: 20 µl Pct Recovery = 74% Analysis Date = 12/12/13 SpikeMix = NSI 053013: 20 µl & Accu 213041120: 20 µl Pct Recovery = 75% Analysis Date = 01/03/03 SpikeMix = ERA 0830-01-06.1VOC: 15 µl Pct Recovery = 108% Analysis Date = 11/07/02 SpikeMix = ERA 0830-01-06.1VOC: 15 µl Pct Recovery = 93% Analysis Date = 10/11/02 SpikeMix = ERA 0830-01-06.1VOC: 15 µl Pct Recovery = 77% Analysis Date = 04/16/03 SpikeMix = ERA 0828-02-09VOC: 5 µl Pct Recovery = 116% Analysis Date = 12/13/02 SpikeMix = ERA 0828-02-09VOC: 5 µl Pct Recovery = 88% Analysis Date = 10/25/02 SpikeMix = ERA 0828-02-09VOC: 5 µl Pct Recovery = 82% Analysis Date = 03/10/12 SpikeMix = NSI 062310-01: 20 µl Pct Recovery = 74% Analysis Date = 10/18/11 SpikeMix = NSI 062310-01: 20 µl Pct Recovery = 72% Analysis Date = 09/17/11 SpikeMix = NSI 062310-01: 20 µl Pct Recovery = 72% Analysis Date = 05/03/11 SpikeMix = NSI 062310-01: 20 µl Pct Recovery = 66% Analysis Date = 03/01/11 SpikeMix = NSI 062310-01: 20 µl Pct Recovery = 74% Analysis Date = 11/05/10 SpikeMix = NSI 062310-01: 20 µl Pct Recovery = 76% Analysis Date = 01/23/07 SpikeMix = Crescent 07FF068: 20 µl Pct Recovery = 100% Analysis Date = 11/07/06 SpikeMix = Crescent 07FF068: 20 µl Pct Recovery = 88% Analysis Date = 08/30/06 SpikeMix = Accu B5070191: 2 µl Pct Recovery = 89% Analysis Date = 12/15/05 SpikeMix = Accu B5070191: 2 µl Pct Recovery = 114% Analysis Date = 10/01/02 SpikeMix = ERA 0830-01-06.1VOC: 10 µl Pct Recovery = 74% Analysis Date = 06/11/02 SpikeMix = ERA 0830-01-06.1VOC: 10 µl Pct Recovery = 109% Analysis Date = 03/04/02 SpikeMix = ERA 0830-01-06.1VOC: 10 µl Pct Recovery = 111% Analysis Date = 11/27/01 SpikeMix = ERA 0830-01-06.1VOC: 10 µl Pct Recovery = 112% Analysis Date = 12/27/00 SpikeMix = NSI 121699: 5 µl Pct Recovery = 117% Analysis Date = 12/14/00 SpikeMix = NSI 121699: 5 µl Pct Recovery = 74% Analysis Date = 09/06/00 SpikeMix = NSI 121699: 5 µl Pct Recovery = 137% Analysis Date = 06/27/00 SpikeMix = NSI 121699: 5 µl Pct Recovery = 77% Analysis Date = 04/18/00 SpikeMix = NSI 121699: 5 µl Pct Recovery = 79% Analysis Date = 09/17/13 SpikeMix = Crescent 04CC151: 10 µl & Supelco LC00154: 10 µl Pct Recovery = 79% Analysis Date = 12/12/13 SpikeMix = Supelco LC00154: 10 µl & Abs 051413: 10 µl Pct Recovery = 78% Analysis Date = 07/09/10 SpikeMix = Spex Organics C1090901006: 10 µl Pct Recovery = 100% Analysis Date = 04/27/10 SpikeMix = Spex Organics C1090901006: 10 µl Pct Recovery = 82% Analysis Date = 02/09/10 SpikeMix = Spex Organics C1090901006: 10 µl Pct Recovery = 77% Analysis Date = 11/04/09 SpikeMix = Spex Organics C1090901006: 10 µl Pct Recovery = 76% Analysis Date = 12/31/13 SpikeMix = Accu 213041120: 10 µl & ChemService 1530700: 10 µl Pct Recovery = 82% Analysis Date = 01/15/14 SpikeMix = Crescent 04CC151: 10 µl & Accu 213041120: 10 µl Pct Recovery = 74% Analysis Date = 05/22/13 SpikeMix = Crescent 04CC151: 10 µl & Accu 213041120: 10 µl Pct Recovery = 85% Analysis Date = 03/19/14 SpikeMix = Accu 213041120: 10 µl & Abs 051413: 10 µl Pct Recovery = 78% Analysis Date = 06/08/13 SpikeMix = Accu 213041120: 10 µl & Abs 051413: 10 µl Pct Recovery = 90% Analysis Date = 12/16/08 SpikeMix = Supelco LB55705: 20 µl Pct Recovery = 107% Analysis Date = 11/18/08 SpikeMix = Supelco LB55705: 20 µl Pct Recovery = 89% Analysis Date = 10/17/08 SpikeMix = Supelco LB55705: 20 µl Pct Recovery = 89% Analysis Date = 08/15/08 SpikeMix = Supelco LB55705: 20 µl Pct Recovery = 89% Analysis Date = 05/09/08 SpikeMix = Supelco LB55705: 20 µl Pct Recovery = 107% Analysis Date = 03/22/08 SpikeMix = Supelco LB55705: 20 µl Pct Recovery = 89% Analysis Date = 09/05/08 SpikeMix = Abs 071107VOC: 20 µl Pct Recovery = 89% Analysis Date = 12/18/07 SpikeMix = Abs 071107VOC: 20 µl Pct Recovery = 107% Analysis Date = 10/19/07 SpikeMix = Abs 071107VOC: 20 µl Pct Recovery = 89% Analysis Date = 09/22/01 SpikeMix = NSI 111700VOC: 5 µl Pct Recovery = 94% Analysis Date = 07/21/01 SpikeMix = NSI 111700VOC: 5 µl Pct Recovery = 90% Analysis Date = 10/14/98 SpikeMix = NSI Q-16750-50 101497: 2 µl Pct Recovery = 45% Analysis Date = 04/11/01 SpikeMix = NSI 111700VOC: 5 µl Pct Recovery = 88% Analysis Date = 01/24/01 SpikeMix = NSI 111700VOC: 5 µl Pct Recovery = 80% Analysis Date = 11/29/00 SpikeMix = NSI 053100-01: 2 µl Pct Recovery = 78% Analysis Date = 09/19/00 SpikeMix = NSI 053100-01: 2 µl Pct Recovery = 96% Analysis Date = 08/02/00 SpikeMix = NSI 053100-01: 2 µl Pct Recovery = 100% Analysis Date = 07/06/00 SpikeMix = NSI 053100-01: 2 µl Pct Recovery = 87% Analysis Date = 03/19/14 Pct Recovery = 79% Analysis Date = 02/18/14 Pct Recovery = 79% Analysis Date = 02/18/14 Pct Recovery = 79% Analysis Date = 01/21/14 Pct Recovery = 79% Analysis Date = 01/21/14 Pct Recovery = 79% Analysis Date = 12/24/13 Pct Recovery = 79% Analysis Date = 12/24/13 Pct Recovery = 79% Analysis Date = 11/26/13 Pct Recovery = 79% Analysis Date = 11/26/13 Pct Recovery = 79% Analysis Date = 10/29/13 Pct Recovery = 79% Analysis Date = 10/29/13 Pct Recovery = 79% Analysis Date = 09/30/13 Pct Recovery = 79% Analysis Date = 09/30/13 Pct Recovery = 79% Analysis Date = 09/02/13 Pct Recovery = 79% Analysis Date = 09/02/13 Pct Recovery = 79% Analysis Date = 08/05/13 Pct Recovery = 79% Analysis Date = 08/05/13 Pct Recovery = 79% Analysis Date = 07/08/13 Pct Recovery = 80% Analysis Date = 07/08/13 Pct Recovery = 80% Analysis Date = 06/10/13 Pct Recovery = 80% Analysis Date = 06/10/13 Pct Recovery = 80% Analysis Date = 05/13/13 Pct Recovery = 80% Analysis Date = 05/13/13 Pct Recovery = 80% Analysis Date = 04/14/13 Pct Recovery = 80% Analysis Date = 04/14/13 Pct Recovery = 80% Analysis Date = 03/17/13 Pct Recovery = 80% Analysis Date = 03/17/13 Pct Recovery = 80% Analysis Date = 02/17/13 Pct Recovery = 80% Analysis Date = 02/17/13 Pct Recovery = 80% Analysis Date = 01/20/13 Pct Recovery = 80% Analysis Date = 01/20/13 Pct Recovery = 80% Analysis Date = 12/23/12 Pct Recovery = 80% Analysis Date = 12/23/12 Pct Recovery = 80% Analysis Date = 11/25/12 Pct Recovery = 80% Analysis Date = 11/25/12 Pct Recovery = 80% Analysis Date = 10/27/12 Pct Recovery = 81% Analysis Date = 10/27/12 Pct Recovery = 81% Analysis Date = 09/29/12 Pct Recovery = 81% Analysis Date = 09/29/12 Pct Recovery = 81% Analysis Date = 09/01/12 Pct Recovery = 81% Analysis Date = 09/01/12 Pct Recovery = 81% Analysis Date = 08/04/12 Pct Recovery = 81% Analysis Date = 08/04/12 Pct Recovery = 81% Analysis Date = 07/07/12 Pct Recovery = 81% Analysis Date = 07/07/12 Pct Recovery = 81% Analysis Date = 06/09/12 Pct Recovery = 81% Analysis Date = 06/09/12 Pct Recovery = 81% Analysis Date = 05/11/12 Pct Recovery = 81% Analysis Date = 05/11/12 Pct Recovery = 81% Analysis Date = 04/13/12 Pct Recovery = 81% Analysis Date = 04/13/12 Pct Recovery = 81% Analysis Date = 03/16/12 Pct Recovery = 81% Analysis Date = 03/16/12 Pct Recovery = 81% Analysis Date = 02/17/12 Pct Recovery = 82% Analysis Date = 02/17/12 Pct Recovery = 82% Analysis Date = 01/20/12 Pct Recovery = 82% Analysis Date = 01/20/12 Pct Recovery = 82% Analysis Date = 12/23/11 Pct Recovery = 82% Analysis Date = 12/23/11 Pct Recovery = 82% Analysis Date = 11/24/11 Pct Recovery = 82% Analysis Date = 11/24/11 Pct Recovery = 82% Analysis Date = 10/27/11 Pct Recovery = 82% Analysis Date = 10/27/11 Pct Recovery = 82% Analysis Date = 09/29/11 Pct Recovery = 82% Analysis Date = 09/29/11 Pct Recovery = 82% Analysis Date = 09/01/11 Pct Recovery = 82% Analysis Date = 09/01/11 Pct Recovery = 82% Analysis Date = 08/04/11 Pct Recovery = 82% Analysis Date = 08/04/11 Pct Recovery = 82% Analysis Date = 07/06/11 Pct Recovery = 83% Analysis Date = 07/06/11 Pct Recovery = 83% Analysis Date = 06/08/11 Pct Recovery = 83% Analysis Date = 06/08/11 Pct Recovery = 83% Analysis Date = 05/11/11 Pct Recovery = 83% Analysis Date = 05/11/11 Pct Recovery = 83% Analysis Date = 04/13/11 Pct Recovery = 83% Analysis Date = 04/13/11 Pct Recovery = 83% Analysis Date = 03/16/11 Pct Recovery = 83% Analysis Date = 03/16/11 Pct Recovery = 83% Analysis Date = 02/16/11 Pct Recovery = 83% Analysis Date = 02/16/11 Pct Recovery = 83% Analysis Date = 01/18/11 Pct Recovery = 83% Analysis Date = 01/18/11 Pct Recovery = 83% Analysis Date = 12/21/10 Pct Recovery = 83% Analysis Date = 12/21/10 Pct Recovery = 83% Analysis Date = 11/23/10 Pct Recovery = 84% Analysis Date = 11/23/10 Pct Recovery = 84% Analysis Date = 10/26/10 Pct Recovery = 84% Analysis Date = 10/26/10 Pct Recovery = 84% Analysis Date = 09/28/10 Pct Recovery = 84% Analysis Date = 09/28/10 Pct Recovery = 84% Analysis Date = 08/31/10 Pct Recovery = 84% Analysis Date = 08/31/10 Pct Recovery = 84% Analysis Date = 08/02/10 Pct Recovery = 84% Analysis Date = 08/02/10 Pct Recovery = 84% Analysis Date = 07/05/10 Pct Recovery = 84% Analysis Date = 07/05/10 Pct Recovery = 84% Analysis Date = 06/07/10 Pct Recovery = 84% Analysis Date = 06/07/10 Pct Recovery = 84% Analysis Date = 05/10/10 Pct Recovery = 85% Analysis Date = 05/10/10 Pct Recovery = 85% Analysis Date = 04/12/10 Pct Recovery = 85% Analysis Date = 04/12/10 Pct Recovery = 85% Analysis Date = 03/15/10 Pct Recovery = 85% Analysis Date = 03/15/10 Pct Recovery = 85% Analysis Date = 02/14/10 Pct Recovery = 85% Analysis Date = 02/14/10 Pct Recovery = 85% Analysis Date = 01/17/10 Pct Recovery = 85% Analysis Date = 01/17/10 Pct Recovery = 85% Analysis Date = 12/20/09 Pct Recovery = 85% Analysis Date = 12/20/09 Pct Recovery = 85% Analysis Date = 11/22/09 Pct Recovery = 85% Analysis Date = 11/22/09 Pct Recovery = 85% Analysis Date = 10/25/09 Pct Recovery = 85% Analysis Date = 10/25/09 Pct Recovery = 85% Analysis Date = 09/27/09 Pct Recovery = 86% Analysis Date = 09/27/09 Pct Recovery = 86% Analysis Date = 08/29/09 Pct Recovery = 86% Analysis Date = 08/29/09 Pct Recovery = 86% Analysis Date = 08/01/09 Pct Recovery = 86% Analysis Date = 08/01/09 Pct Recovery = 86% Analysis Date = 07/04/09 Pct Recovery = 86% Analysis Date = 07/04/09 Pct Recovery = 86% Analysis Date = 06/06/09 Pct Recovery = 86% Analysis Date = 06/06/09 Pct Recovery = 86% Analysis Date = 05/09/09 Pct Recovery = 86% Analysis Date = 05/09/09 Pct Recovery = 86% Analysis Date = 04/10/09 Pct Recovery = 87% Analysis Date = 04/10/09 Pct Recovery = 87% Analysis Date = 03/13/09 Pct Recovery = 87% Analysis Date = 03/13/09 Pct Recovery = 87% Analysis Date = 02/13/09 Pct Recovery = 87% Analysis Date = 02/13/09 Pct Recovery = 87% Analysis Date = 01/16/09 Pct Recovery = 88% Analysis Date = 01/16/09 Pct Recovery = 88% Analysis Date = 12/19/08 Pct Recovery = 88% Analysis Date = 12/19/08 Pct Recovery = 88% Analysis Date = 11/21/08 Pct Recovery = 88% Analysis Date = 11/21/08 Pct Recovery = 88% Analysis Date = 10/23/08 Pct Recovery = 88% Analysis Date = 10/23/08 Pct Recovery = 88% Analysis Date = 09/25/08 Pct Recovery = 89% Analysis Date = 09/25/08 Pct Recovery = 89% Analysis Date = 08/28/08 Pct Recovery = 89% Analysis Date = 08/28/08 Pct Recovery = 89% Analysis Date = 07/31/08 Pct Recovery = 89% Analysis Date = 07/31/08 Pct Recovery = 89% Analysis Date = 07/03/08 Pct Recovery = 89% Analysis Date = 07/03/08 Pct Recovery = 89% Analysis Date = 06/05/08 Pct Recovery = 90% Analysis Date = 06/05/08 Pct Recovery = 90% Analysis Date = 05/07/08 Pct Recovery = 90% Analysis Date = 05/07/08 Pct Recovery = 90% Analysis Date = 04/09/08 Pct Recovery = 90% Analysis Date = 04/09/08 Pct Recovery = 90% Analysis Date = 03/12/08 Pct Recovery = 90% Analysis Date = 03/12/08 Pct Recovery = 90% Analysis Date = 02/13/08 Pct Recovery = 91% Analysis Date = 02/13/08 Pct Recovery = 91% Analysis Date = 01/16/08 Pct Recovery = 91% Analysis Date = 01/16/08 Pct Recovery = 91% Analysis Date = 12/19/07 Pct Recovery = 91% Analysis Date = 12/19/07 Pct Recovery = 91% Analysis Date = 11/20/07 Pct Recovery = 91% Analysis Date = 11/20/07 Pct Recovery = 91% Analysis Date = 10/23/07 Pct Recovery = 92% Analysis Date = 10/23/07 Pct Recovery = 92% Analysis Date = 09/25/07 Pct Recovery = 92% Analysis Date = 09/25/07 Pct Recovery = 92% Analysis Date = 08/28/07 Pct Recovery = 92% Analysis Date = 08/28/07 Pct Recovery = 92% Analysis Date = 07/31/07 Pct Recovery = 92% Analysis Date = 07/31/07 Pct Recovery = 92% Analysis Date = 07/03/07 Pct Recovery = 93% Analysis Date = 07/03/07 Pct Recovery = 93% Analysis Date = 06/04/07 Pct Recovery = 93% Analysis Date = 06/04/07 Pct Recovery = 93% Analysis Date = 05/07/07 Pct Recovery = 93% Analysis Date = 05/07/07 Pct Recovery = 93% Analysis Date = 04/09/07 Pct Recovery = 93% Analysis Date = 04/09/07 Pct Recovery = 93% Analysis Date = 03/12/07 Pct Recovery = 94% Analysis Date = 03/12/07 Pct Recovery = 94% Analysis Date = 02/12/07 Pct Recovery = 94% Analysis Date = 02/12/07 Pct Recovery = 94% Analysis Date = 01/14/07 Pct Recovery = 94% Analysis Date = 01/14/07 Pct Recovery = 94% Analysis Date = 12/17/06 Pct Recovery = 94% Analysis Date = 12/17/06 Pct Recovery = 94% Analysis Date = 11/19/06 Pct Recovery = 94% Analysis Date = 11/19/06 Pct Recovery = 94% Analysis Date = 10/22/06 Pct Recovery = 95% Analysis Date = 10/22/06 Pct Recovery = 95% Analysis Date = 09/24/06 Pct Recovery = 95% Analysis Date = 09/24/06 Pct Recovery = 95% Analysis Date = 08/27/06 Pct Recovery = 95% Analysis Date = 08/27/06 Pct Recovery = 95% Analysis Date = 07/29/06 Pct Recovery = 95% Analysis Date = 07/29/06 Pct Recovery = 95% Analysis Date = 07/01/06 Pct Recovery = 95% Analysis Date = 07/01/06 Pct Recovery = 95% Analysis Date = 06/03/06 Pct Recovery = 95% Analysis Date = 06/03/06 Pct Recovery = 95% Analysis Date = 05/06/06 Pct Recovery = 96% Analysis Date = 05/06/06 Pct Recovery = 96% Analysis Date = 04/08/06 Pct Recovery = 96% Analysis Date = 04/08/06 Pct Recovery = 96% Analysis Date = 03/11/06 Pct Recovery = 96% Analysis Date = 03/11/06 Pct Recovery = 96% Analysis Date = 02/10/06 Pct Recovery = 96% Analysis Date = 02/10/06 Pct Recovery = 96% Analysis Date = 01/13/06 Pct Recovery = 96% Analysis Date = 01/13/06 Pct Recovery = 96% Analysis Date = 12/16/05 Pct Recovery = 97% Analysis Date = 12/16/05 Pct Recovery = 97% Analysis Date = 11/18/05 Pct Recovery = 97% Analysis Date = 11/18/05 Pct Recovery = 97% Analysis Date = 10/21/05 Pct Recovery = 97% Analysis Date = 10/21/05 Pct Recovery = 97% Analysis Date = 09/23/05 Pct Recovery = 97% Analysis Date = 09/23/05 Pct Recovery = 97% Analysis Date = 08/25/05 Pct Recovery = 97% Analysis Date = 08/25/05 Pct Recovery = 97% Analysis Date = 07/28/05 Pct Recovery = 97% Analysis Date = 07/28/05 Pct Recovery = 97% Analysis Date = 06/30/05 Pct Recovery = 97% Analysis Date = 06/30/05 Pct Recovery = 97% Analysis Date = 06/02/05 Pct Recovery = 97% Analysis Date = 06/02/05 Pct Recovery = 97% Analysis Date = 05/05/05 Pct Recovery = 97% Analysis Date = 05/05/05 Pct Recovery = 97% Analysis Date = 04/07/05 Pct Recovery = 97% Analysis Date = 04/07/05 Pct Recovery = 97% Analysis Date = 03/09/05 Pct Recovery = 97% Analysis Date = 03/09/05 Pct Recovery = 97% Analysis Date = 02/09/05 Pct Recovery = 97% Analysis Date = 02/09/05 Pct Recovery = 97% Analysis Date = 01/12/05 Pct Recovery = 97% Analysis Date = 01/12/05 Pct Recovery = 97% Analysis Date = 12/15/04 Pct Recovery = 97% Analysis Date = 12/15/04 Pct Recovery = 97% Analysis Date = 11/17/04 Pct Recovery = 97% Analysis Date = 11/17/04 Pct Recovery = 97% Analysis Date = 10/19/04 Pct Recovery = 97% Analysis Date = 10/19/04 Pct Recovery = 97% Analysis Date = 09/21/04 Pct Recovery = 97% Analysis Date = 09/21/04 Pct Recovery = 97% Analysis Date = 08/24/04 Pct Recovery = 97% Analysis Date = 08/24/04 Pct Recovery = 97% Analysis Date = 07/27/04 Pct Recovery = 97% Analysis Date = 07/27/04 Pct Recovery = 97% Analysis Date = 06/29/04 Pct Recovery = 97% Analysis Date = 06/29/04 Pct Recovery = 97% Analysis Date = 06/01/04 Pct Recovery = 97% Analysis Date = 06/01/04 Pct Recovery = 97% Analysis Date = 05/03/04 Pct Recovery = 97% Analysis Date = 05/03/04 Pct Recovery = 97% Analysis Date = 04/05/04 Pct Recovery = 97% Analysis Date = 04/05/04 Pct Recovery = 97% Analysis Date = 03/08/04 Pct Recovery = 97% Analysis Date = 03/08/04 Pct Recovery = 97% Analysis Date = 02/09/04 Pct Recovery = 97% Analysis Date = 02/09/04 Pct Recovery = 97% Analysis Date = 01/12/04 Pct Recovery = 97% Analysis Date = 01/12/04 Pct Recovery = 97% Analysis Date = 12/15/03 Pct Recovery = 97% Analysis Date = 12/15/03 Pct Recovery = 97% Analysis Date = 11/16/03 Pct Recovery = 97% Analysis Date = 11/16/03 Pct Recovery = 97% Analysis Date = 10/19/03 Pct Recovery = 97% Analysis Date = 10/19/03 Pct Recovery = 97% Analysis Date = 09/21/03 Pct Recovery = 97% Analysis Date = 09/21/03 Pct Recovery = 97% Analysis Date = 08/24/03 Pct Recovery = 97% Analysis Date = 08/24/03 Pct Recovery = 97% Analysis Date = 07/27/03 Pct Recovery = 97% Analysis Date = 07/27/03 Pct Recovery = 97% Analysis Date = 06/29/03 Pct Recovery = 97% Analysis Date = 06/29/03 Pct Recovery = 97% Analysis Date = 05/31/03 Pct Recovery = 97% Analysis Date = 05/31/03 Pct Recovery = 97% Analysis Date = 05/03/03 Pct Recovery = 97% Analysis Date = 05/03/03 Pct Recovery = 97% Analysis Date = 04/05/03 Pct Recovery = 97% Analysis Date = 04/05/03 Pct Recovery = 97% Analysis Date = 03/08/03 Pct Recovery = 97% Analysis Date = 03/08/03 Pct Recovery = 97% Analysis Date = 02/08/03 Pct Recovery = 97% Analysis Date = 02/08/03 Pct Recovery = 97% Analysis Date = 01/11/03 Pct Recovery = 97% Analysis Date = 01/11/03 Pct Recovery = 97% Analysis Date = 12/13/02 Pct Recovery = 97% Analysis Date = 12/13/02 Pct Recovery = 97% Analysis Date = 11/15/02 Pct Recovery = 97% Analysis Date = 11/15/02 Pct Recovery = 97% Analysis Date = 10/18/02 Pct Recovery = 97% Analysis Date = 10/18/02 Pct Recovery = 97% Analysis Date = 09/20/02 Pct Recovery = 97% Analysis Date = 09/20/02 Pct Recovery = 97% Analysis Date = 08/23/02 Pct Recovery = 97% Analysis Date = 08/23/02 Pct Recovery = 97% Analysis Date = 07/25/02 Pct Recovery = 97% Analysis Date = 07/25/02 Pct Recovery = 97% Analysis Date = 06/27/02 Pct Recovery = 97% Analysis Date = 06/27/02 Pct Recovery = 97% Analysis Date = 05/30/02 Pct Recovery = 97% Analysis Date = 05/30/02 Pct Recovery = 97% Analysis Date = 05/02/02 Pct Recovery = 97% Analysis Date = 05/02/02 Pct Recovery = 97% Analysis Date = 04/04/02 Pct Recovery = 97% Analysis Date = 04/04/02 Pct Recovery = 97% Analysis Date = 03/07/02 Pct Recovery = 97% Analysis Date = 03/07/02 Pct Recovery = 97% Analysis Date = 02/06/02 Pct Recovery = 97% Analysis Date = 02/06/02 Pct Recovery = 97% Analysis Date = 01/09/02 Pct Recovery = 97% Analysis Date = 01/09/02 Pct Recovery = 97% Analysis Date = 12/12/01 Pct Recovery = 97% Analysis Date = 12/12/01 Pct Recovery = 97% Analysis Date = 11/14/01 Pct Recovery = 96% Analysis Date = 11/14/01 Pct Recovery = 96% Analysis Date = 10/17/01 Pct Recovery = 96% Analysis Date = 10/17/01 Pct Recovery = 96% Analysis Date = 09/19/01 Pct Recovery = 96% Analysis Date = 09/19/01 Pct Recovery = 96% Analysis Date = 08/21/01 Pct Recovery = 96% Analysis Date = 08/21/01 Pct Recovery = 96% Analysis Date = 07/24/01 Pct Recovery = 96% Analysis Date = 07/24/01 Pct Recovery = 96% Analysis Date = 06/26/01 Pct Recovery = 96% Analysis Date = 06/26/01 Pct Recovery = 96% Analysis Date = 05/29/01 Pct Recovery = 96% Analysis Date = 05/29/01 Pct Recovery = 96% Analysis Date = 05/01/01 Pct Recovery = 96% Analysis Date = 05/01/01 Pct Recovery = 96% Analysis Date = 04/03/01 Pct Recovery = 96% Analysis Date = 04/03/01 Pct Recovery = 96% Analysis Date = 03/05/01 Pct Recovery = 96% Analysis Date = 03/05/01 Pct Recovery = 96% Analysis Date = 02/05/01 Pct Recovery = 96% Analysis Date = 02/05/01 Pct Recovery = 96% Analysis Date = 01/08/01 Pct Recovery = 96% Analysis Date = 01/08/01 Pct Recovery = 96% Analysis Date = 12/11/00 Pct Recovery = 96% Analysis Date = 12/11/00 Pct Recovery = 96% Analysis Date = 11/13/00 Pct Recovery = 96% Analysis Date = 11/13/00 Pct Recovery = 96% Analysis Date = 10/16/00 Pct Recovery = 96% Analysis Date = 10/16/00 Pct Recovery = 96% Analysis Date = 09/17/00 Pct Recovery = 96% Analysis Date = 09/17/00 Pct Recovery = 96% Analysis Date = 08/20/00 Pct Recovery = 96% Analysis Date = 08/20/00 Pct Recovery = 96% Analysis Date = 07/23/00 Pct Recovery = 96% Analysis Date = 07/23/00 Pct Recovery = 96% Analysis Date = 06/25/00 Pct Recovery = 96% Analysis Date = 06/25/00 Pct Recovery = 96% Analysis Date = 05/28/00 Pct Recovery = 96% Analysis Date = 05/28/00 Pct Recovery = 96% Analysis Date = 04/30/00 Pct Recovery = 96% Analysis Date = 04/30/00 Pct Recovery = 96% Analysis Date = 04/01/00 Pct Recovery = 96% Analysis Date = 04/01/00 Pct Recovery = 96% Analysis Date = 03/04/00 Pct Recovery = 96% Analysis Date = 03/04/00 Pct Recovery = 96% Analysis Date = 02/05/00 Pct Recovery = 96% Analysis Date = 02/05/00 Pct Recovery = 96% Analysis Date = 01/08/00 Pct Recovery = 96% Analysis Date = 01/08/00 Pct Recovery = 96% Analysis Date = 12/11/99 Pct Recovery = 96% Analysis Date = 12/11/99 Pct Recovery = 96% Analysis Date = 11/12/99 Pct Recovery = 96% Analysis Date = 11/12/99 Pct Recovery = 96% Analysis Date = 10/15/99 Pct Recovery = 96% Analysis Date = 10/15/99 Pct Recovery = 96% Analysis Date = 09/17/99 Pct Recovery = 96% Analysis Date = 09/17/99 Pct Recovery = 96% Analysis Date = 08/20/99 Pct Recovery = 96% Analysis Date = 08/20/99 Pct Recovery = 96% Analysis Date = 07/23/99 Pct Recovery = 96% Analysis Date = 07/23/99 Pct Recovery = 96% Analysis Date = 06/25/99 Pct Recovery = 96% Analysis Date = 06/25/99 Pct Recovery = 96% Analysis Date = 05/27/99 Pct Recovery = 96% Analysis Date = 05/27/99 Pct Recovery = 96% Analysis Date = 04/29/99 Pct Recovery = 96% Analysis Date = 04/29/99 Pct Recovery = 96% Analysis Date = 04/01/99 Pct Recovery = 96% Analysis Date = 04/01/99 Pct Recovery = 96% Analysis Date = 03/04/99 Pct Recovery = 96% Analysis Date = 03/04/99 Pct Recovery = 96% Analysis Date = 02/04/99 Pct Recovery = 96% Analysis Date = 02/04/99 Pct Recovery = 96% Analysis Date = 01/07/99 Pct Recovery = 96% Analysis Date = 01/07/99 Pct Recovery = 96% Analysis Date = 12/09/98 Pct Recovery = 96% Analysis Date = 12/09/98 Pct Recovery = 96% Analysis Date = 11/11/98 Pct Recovery = 96% Analysis Date = 11/11/98 Pct Recovery = 96% Analysis Date = 10/14/98 Pct Recovery = 96% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
4-CHLOROTOLUENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 7 82% 18% 87% 14%
>= Reporting Level 149 91% 15% 90% 15%
Total 156 91% 15% 90% 15%

Sample Statistics
4-CHLOROTOLUENE

Characteristic N % % Basis
Plotted 156 100% Spiked
Estimated Values 39 25% Spiked
Deleted Values 1 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 157 .  
False Negatives 0 0% 0 out of 156
Not Spiked 319 .  
False Positives 1 0% 1 out of 319