BQS OBSP Determination:
HEXANE
METHOD: 4440 , TESTIDCODE: 81590GCM66
DATES: 07/11/14 - 09/07/17

Expected Conc. = 0.2 Median Pct Recovery = 95% Expected Conc. = 0.1608 Median Pct Recovery = 95% Expected Conc. = 0.1608 Median Pct Recovery = 95% Expected Conc. = 0.1608 Median Pct Recovery = 95% Expected Conc. = 0.1608 Median Pct Recovery = 95% Expected Conc. = 0.1584 Median Pct Recovery = 95% Expected Conc. = 0.1584 Median Pct Recovery = 95% Expected Conc. = 0.1584 Median Pct Recovery = 95% Expected Conc. = 0.1584 Median Pct Recovery = 95% Expected Conc. = 0.1584 Median Pct Recovery = 95% Expected Conc. = 0.1584 Median Pct Recovery = 95% Expected Conc. = 0.1584 Median Pct Recovery = 95% Expected Conc. = 0.1584 Median Pct Recovery = 95% Expected Conc. = 0.1005 Median Pct Recovery = 95% Expected Conc. = 0.1005 Median Pct Recovery = 95% Expected Conc. = 0.1005 Median Pct Recovery = 95% Expected Conc. = 0.1005 Median Pct Recovery = 95% Expected Conc. = 0.1005 Median Pct Recovery = 95% Expected Conc. = 0.1005 Median Pct Recovery = 95% Expected Conc. = 0.1005 Median Pct Recovery = 95% Expected Conc. = 0.1005 Median Pct Recovery = 95% Expected Conc. = 0.1005 Median Pct Recovery = 95% Expected Conc. = 0.1005 Median Pct Recovery = 95% Expected Conc. = 0.1005 Median Pct Recovery = 95% Expected Conc. = 0.1005 Median Pct Recovery = 95% Expected Conc. = 0.1005 Median Pct Recovery = 95% Expected Conc. = 0.1005 Median Pct Recovery = 95% Expected Conc. = 0.1 Median Pct Recovery = 95% Expected Conc. = 0.1 Median Pct Recovery = 95% Expected Conc. = 0.099 Median Pct Recovery = 95% Expected Conc. = 0.099 Median Pct Recovery = 95% Expected Conc. = 0.099 Median Pct Recovery = 95% Expected Conc. = 0.099 Median Pct Recovery = 95% Expected Conc. = 0.099 Median Pct Recovery = 95% Expected Conc. = 0.099 Median Pct Recovery = 95% Expected Conc. = 0.099 Median Pct Recovery = 95% Expected Conc. = 0.099 Median Pct Recovery = 95% Expected Conc. = 0.099 Median Pct Recovery = 95% Expected Conc. = 0.099 Median Pct Recovery = 95% Expected Conc. = 0.099 Median Pct Recovery = 95% Expected Conc. = 0.099 Median Pct Recovery = 95% Expected Conc. = 0.096 Median Pct Recovery = 95% Expected Conc. = 0.096 Median Pct Recovery = 95% Expected Conc. = 0.096 Median Pct Recovery = 95% Expected Conc. = 0.096 Median Pct Recovery = 95% Expected Conc. = 0.096 Median Pct Recovery = 95% Expected Conc. = 0.096 Median Pct Recovery = 95% Expected Conc. = 0.096 Median Pct Recovery = 95% Expected Conc. = 0.096 Median Pct Recovery = 95% Expected Conc. = 0.09 Median Pct Recovery = 95% Expected Conc. = 0.09 Median Pct Recovery = 95% Expected Conc. = 0.09 Median Pct Recovery = 95% Expected Conc. = 0.09 Median Pct Recovery = 95% Expected Conc. = 0.0603 Median Pct Recovery = 95% Expected Conc. = 0.0603 Median Pct Recovery = 95% Expected Conc. = 0.0603 Median Pct Recovery = 95% Expected Conc. = 0.0603 Median Pct Recovery = 95% Expected Conc. = 0.0603 Median Pct Recovery = 95% Expected Conc. = 0.0603 Median Pct Recovery = 95% Expected Conc. = 0.0603 Median Pct Recovery = 95% Expected Conc. = 0.0603 Median Pct Recovery = 95% Expected Conc. = 0.0603 Median Pct Recovery = 95% Expected Conc. = 0.0603 Median Pct Recovery = 95% Expected Conc. = 0.0594 Median Pct Recovery = 95% Expected Conc. = 0.0594 Median Pct Recovery = 95% Expected Conc. = 0.0594 Median Pct Recovery = 95% Expected Conc. = 0.0594 Median Pct Recovery = 95% Expected Conc. = 0.0594 Median Pct Recovery = 95% Expected Conc. = 0.0594 Median Pct Recovery = 95% Expected Conc. = 0.0594 Median Pct Recovery = 95% Expected Conc. = 0.0594 Median Pct Recovery = 95% Expected Conc. = 0.0594 Median Pct Recovery = 95% Expected Conc. = 0.0594 Median Pct Recovery = 95% Expected Conc. = 0.054 Median Pct Recovery = 95% Expected Conc. = 0.054 Median Pct Recovery = 95% Expected Conc. = 0.054 Median Pct Recovery = 95% Expected Conc. = 0.054 Median Pct Recovery = 95% Expected Conc. = 0.054 Median Pct Recovery = 95% Expected Conc. = 0.054 Median Pct Recovery = 95% Expected Conc. = 0.054 Median Pct Recovery = 95% Expected Conc. = 0.054 Median Pct Recovery = 95% Expected Conc. = 0.054 Median Pct Recovery = 95% Expected Conc. = 0.054 Median Pct Recovery = 95% Expected Conc. = 0.054 Median Pct Recovery = 95% Expected Conc. = 0.054 Median Pct Recovery = 95% Expected Conc. = 0.054 Median Pct Recovery = 95% Expected Conc. = 0.054 Median Pct Recovery = 95% Expected Conc. = 0.048 Median Pct Recovery = 95% Expected Conc. = 0.048 Median Pct Recovery = 95% Expected Conc. = 0.048 Median Pct Recovery = 95% Expected Conc. = 0.048 Median Pct Recovery = 95% Expected Conc. = 0.048 Median Pct Recovery = 95% Expected Conc. = 0.048 Median Pct Recovery = 95% Expected Conc. = 0.048 Median Pct Recovery = 95% Expected Conc. = 0.048 Median Pct Recovery = 95% Expected Conc. = 0.036 Median Pct Recovery = 95% Expected Conc. = 0.036 Median Pct Recovery = 95% Expected Conc. = 0.036 Median Pct Recovery = 95% Expected Conc. = 0.036 Median Pct Recovery = 95% Expected Conc. = 0.036 Median Pct Recovery = 95% Expected Conc. = 0.036 Median Pct Recovery = 95% Expected Conc. = 0.036 Median Pct Recovery = 95% Expected Conc. = 0.036 Median Pct Recovery = 95% Expected Conc. = 0.036 Median Pct Recovery = 95% Expected Conc. = 0.036 Median Pct Recovery = 95% Expected Conc. = 0.036 Median Pct Recovery = 95% Expected Conc. = 0.036 Median Pct Recovery = 95% Expected Conc. = 0.036 Median Pct Recovery = 95% Expected Conc. = 0.036 Median Pct Recovery = 95% Expected Conc. = 0.036 Median Pct Recovery = 95% Expected Conc. = 0.036 Median Pct Recovery = 95% Expected Conc. = 0.036 Median Pct Recovery = 95% Expected Conc. = 0.036 Median Pct Recovery = 95% Expected Conc. = 0 Median Pct Recovery = 95% Expected Conc. = 0 Median Pct Recovery = 95% Expected Conc. = 0 Median Pct Recovery = 95% Expected Conc. = 0 Median Pct Recovery = 95% Expected Conc. = 0 Median Pct Recovery = 95% Expected Conc. = 0 Median Pct Recovery = 95% Expected Conc. = 0 Median Pct Recovery = 95% Expected Conc. = 0 Median Pct Recovery = 95% Expected Conc. = 0 Median Pct Recovery = 95% Expected Conc. = 0 Median Pct Recovery = 95% Expected Conc. = 0 Median Pct Recovery = 95% Expected Conc. = 0 Median Pct Recovery = 95% Expected Conc. = 0 Median Pct Recovery = 95% Expected Conc. = 0 Median Pct Recovery = 95% Expected Conc. = 0 Median Pct Recovery = 95% Expected Conc. = 0 Median Pct Recovery = 95% Expected Conc. = 0 Median Pct Recovery = 95% Expected Conc. = 0 Median Pct Recovery = 95% Expected Conc. = 0 Median Pct Recovery = 95% Expected Conc. = 0 Median Pct Recovery = 95% Expected Conc. = 0 Median Pct Recovery = 95% Expected Conc. = 0 Median Pct Recovery = 95% Expected Conc. = 0 Median Pct Recovery = 95% Analysis Date = 08/29/17 SpikeMix = Abs 070717: 20 µl & Abs 070617: 20 µl Pct Recovery = 60% Analysis Date = 03/09/17 SpikeMix = Phenova B20160319: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 118% Analysis Date = 01/04/17 SpikeMix = Phenova B20160319: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 75% Analysis Date = 01/26/17 SpikeMix = ChemService 5082900: 40 µl & Accu 216041125: 40 µl Pct Recovery = 76% Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 88% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 126% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 98% Analysis Date = 06/23/17 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 80% Analysis Date = 06/09/17 SpikeMix = Phenova B20160319: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 80% Analysis Date = 05/17/17 SpikeMix = Phenova B20160319: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 70% Analysis Date = 02/24/17 SpikeMix = Supelco LC20141V: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 119% Analysis Date = 11/14/16 SpikeMix = Phenova B20160319: 25 µl & NSI 041816AVOC: 25 µl Pct Recovery = 100% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 84% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 84% Analysis Date = 09/07/17 SpikeMix = Abs 070717: 10 µl & Abs 070617: 10 µl Pct Recovery = 50% Analysis Date = 06/17/17 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 91% Analysis Date = 04/03/17 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 101% Analysis Date = 02/03/17 SpikeMix = Accu 216041125: 25 µl & NSI 041816AVOC: 25 µl Pct Recovery = 121% Analysis Date = 09/29/16 SpikeMix = ChemService 5082900: 25 µl & Accu 216041125: 25 µl Pct Recovery = 115% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 89% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 71% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 141% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 148% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 167% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 136% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 92% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 79% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 66% Analysis Date = 10/29/16 SpikeMix = Supelco LC20141V: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 100% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 93% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 113% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 86% Analysis Date = 05/25/17 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 101% Analysis Date = 12/24/16 SpikeMix = Supelco LC20141V: 15 µl & Accu 216041125: 15 µl Pct Recovery = 101% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 118% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 107% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 64% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 78% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 87% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 94% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 95% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 98% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 97% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 113% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 133% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 170% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 170% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 148% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 76% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 83% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 121% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 104% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 91% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 86% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 79% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 101% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 90% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Median Pct Recovery = 95% Y = 1
The SGPlot Procedure