BQS OBSP Determination:
4-METHYL-2-PENTANONE
METHOD: 4440 , TESTIDCODE: 78133GCM66
DATES: 05/01/14 - 09/07/17

Expected Conc. = 14.576 Median Pct Recovery = 94% Expected Conc. = 14.576 Median Pct Recovery = 94% Expected Conc. = 14.576 Median Pct Recovery = 94% Expected Conc. = 14.576 Median Pct Recovery = 94% Expected Conc. = 14.576 Median Pct Recovery = 94% Expected Conc. = 14.576 Median Pct Recovery = 94% Expected Conc. = 14.576 Median Pct Recovery = 94% Expected Conc. = 9.11 Median Pct Recovery = 94% Expected Conc. = 9.11 Median Pct Recovery = 94% Expected Conc. = 9.11 Median Pct Recovery = 94% Expected Conc. = 9.11 Median Pct Recovery = 94% Expected Conc. = 9.11 Median Pct Recovery = 94% Expected Conc. = 9.11 Median Pct Recovery = 94% Expected Conc. = 9.11 Median Pct Recovery = 94% Expected Conc. = 9.11 Median Pct Recovery = 94% Expected Conc. = 9.11 Median Pct Recovery = 94% Expected Conc. = 9.11 Median Pct Recovery = 94% Expected Conc. = 9.11 Median Pct Recovery = 94% Expected Conc. = 9.11 Median Pct Recovery = 94% Expected Conc. = 9.11 Median Pct Recovery = 94% Expected Conc. = 9.11 Median Pct Recovery = 94% Expected Conc. = 8.27 Median Pct Recovery = 94% Expected Conc. = 8.27 Median Pct Recovery = 94% Expected Conc. = 8.17 Median Pct Recovery = 94% Expected Conc. = 8.17 Median Pct Recovery = 94% Expected Conc. = 8.17 Median Pct Recovery = 94% Expected Conc. = 8.17 Median Pct Recovery = 94% Expected Conc. = 5.466 Median Pct Recovery = 94% Expected Conc. = 5.466 Median Pct Recovery = 94% Expected Conc. = 5.466 Median Pct Recovery = 94% Expected Conc. = 5.466 Median Pct Recovery = 94% Expected Conc. = 5.466 Median Pct Recovery = 94% Expected Conc. = 5.466 Median Pct Recovery = 94% Expected Conc. = 5.466 Median Pct Recovery = 94% Expected Conc. = 5.466 Median Pct Recovery = 94% Expected Conc. = 5.466 Median Pct Recovery = 94% Expected Conc. = 5.466 Median Pct Recovery = 94% Expected Conc. = 4.962 Median Pct Recovery = 94% Expected Conc. = 4.962 Median Pct Recovery = 94% Expected Conc. = 4.962 Median Pct Recovery = 94% Expected Conc. = 4.962 Median Pct Recovery = 94% Expected Conc. = 4.962 Median Pct Recovery = 94% Expected Conc. = 4.962 Median Pct Recovery = 94% Expected Conc. = 4.902 Median Pct Recovery = 94% Expected Conc. = 4.902 Median Pct Recovery = 94% Expected Conc. = 4.902 Median Pct Recovery = 94% Expected Conc. = 4.902 Median Pct Recovery = 94% Expected Conc. = 4.902 Median Pct Recovery = 94% Expected Conc. = 4.902 Median Pct Recovery = 94% Expected Conc. = 3.308 Median Pct Recovery = 94% Expected Conc. = 3.308 Median Pct Recovery = 94% Expected Conc. = 3.308 Median Pct Recovery = 94% Expected Conc. = 3.308 Median Pct Recovery = 94% Expected Conc. = 3.308 Median Pct Recovery = 94% Expected Conc. = 3.308 Median Pct Recovery = 94% Expected Conc. = 3.308 Median Pct Recovery = 94% Expected Conc. = 3.308 Median Pct Recovery = 94% Expected Conc. = 3.268 Median Pct Recovery = 94% Expected Conc. = 3.268 Median Pct Recovery = 94% Expected Conc. = 3.268 Median Pct Recovery = 94% Expected Conc. = 3.268 Median Pct Recovery = 94% Expected Conc. = 3.268 Median Pct Recovery = 94% Expected Conc. = 3.268 Median Pct Recovery = 94% Expected Conc. = 3.268 Median Pct Recovery = 94% Expected Conc. = 3.268 Median Pct Recovery = 94% Expected Conc. = 3.072 Median Pct Recovery = 94% Expected Conc. = 3.072 Median Pct Recovery = 94% Expected Conc. = 1.536 Median Pct Recovery = 94% Expected Conc. = 1.536 Median Pct Recovery = 94% Expected Conc. = 1.28 Median Pct Recovery = 94% Expected Conc. = 1.28 Median Pct Recovery = 94% Expected Conc. = 1.28 Median Pct Recovery = 94% Expected Conc. = 1.28 Median Pct Recovery = 94% Expected Conc. = 1.28 Median Pct Recovery = 94% Expected Conc. = 1.28 Median Pct Recovery = 94% Expected Conc. = 1.264 Median Pct Recovery = 94% Expected Conc. = 1.264 Median Pct Recovery = 94% Expected Conc. = 1.264 Median Pct Recovery = 94% Expected Conc. = 1.264 Median Pct Recovery = 94% Expected Conc. = 0.64 Median Pct Recovery = 94% Expected Conc. = 0.64 Median Pct Recovery = 94% Expected Conc. = 0.64 Median Pct Recovery = 94% Expected Conc. = 0.64 Median Pct Recovery = 94% Expected Conc. = 0.64 Median Pct Recovery = 94% Expected Conc. = 0.64 Median Pct Recovery = 94% Expected Conc. = 0.64 Median Pct Recovery = 94% Expected Conc. = 0.64 Median Pct Recovery = 94% Expected Conc. = 0.632 Median Pct Recovery = 94% Expected Conc. = 0.632 Median Pct Recovery = 94% Expected Conc. = 1.28 Median Pct Recovery = 94% Expected Conc. = 1.28 Median Pct Recovery = 94% Expected Conc. = 1.264 Median Pct Recovery = 94% Expected Conc. = 1.264 Median Pct Recovery = 94% Expected Conc. = 1.264 Median Pct Recovery = 94% Expected Conc. = 1.264 Median Pct Recovery = 94% Expected Conc. = 1.264 Median Pct Recovery = 94% Expected Conc. = 1.264 Median Pct Recovery = 94% Expected Conc. = 0.632 Median Pct Recovery = 94% Expected Conc. = 0.632 Median Pct Recovery = 94% Expected Conc. = 0.632 Median Pct Recovery = 94% Expected Conc. = 0.632 Median Pct Recovery = 94% Expected Conc. = 0.632 Median Pct Recovery = 94% Expected Conc. = 0.632 Median Pct Recovery = 94% Expected Conc. = 0 Median Pct Recovery = 94% Expected Conc. = 0 Median Pct Recovery = 94% Expected Conc. = 0 Median Pct Recovery = 94% Expected Conc. = 0 Median Pct Recovery = 94% Expected Conc. = 0 Median Pct Recovery = 94% Expected Conc. = 0 Median Pct Recovery = 94% Expected Conc. = 0 Median Pct Recovery = 94% Expected Conc. = 0 Median Pct Recovery = 94% Expected Conc. = 0 Median Pct Recovery = 94% Expected Conc. = 0 Median Pct Recovery = 94% Expected Conc. = 0 Median Pct Recovery = 94% Expected Conc. = 0 Median Pct Recovery = 94% Expected Conc. = 0 Median Pct Recovery = 94% Expected Conc. = 0 Median Pct Recovery = 94% Expected Conc. = 0 Median Pct Recovery = 94% Expected Conc. = 0 Median Pct Recovery = 94% Expected Conc. = 0 Median Pct Recovery = 94% Expected Conc. = 0 Median Pct Recovery = 94% Expected Conc. = 0 Median Pct Recovery = 94% Expected Conc. = 0 Median Pct Recovery = 94% Expected Conc. = 0 Median Pct Recovery = 94% Expected Conc. = 0 Median Pct Recovery = 94% Expected Conc. = 0 Median Pct Recovery = 94% Analysis Date = 03/16/17 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 100% Analysis Date = 01/04/17 SpikeMix = Phenova B20160319: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 102% Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 106% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 84% Analysis Date = 06/23/17 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 87% Analysis Date = 06/17/17 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 92% Analysis Date = 04/03/17 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 99% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 95% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 87% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 99% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 105% Analysis Date = 09/29/15 SpikeMix = Accu 215041380: 25 µl & ERA 0406-15-03: 25 µl Pct Recovery = 96% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 99% Analysis Date = 07/13/15 SpikeMix = Crescent 04EE008: 25 µl & NSI 050515AVOC: 25 µl Pct Recovery = 87% Analysis Date = 05/25/17 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 76% Analysis Date = 01/13/17 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 86% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 90% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 80% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 92% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 82% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 85% Analysis Date = 06/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Accu 215041380: 15 µl Pct Recovery = 80% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 98% Analysis Date = 10/17/15 SpikeMix = Crescent 04EE008: 15 µl & NSI 050515AVOC: 15 µl Pct Recovery = 94% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 89% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 90% Analysis Date = 11/20/15 SpikeMix = Accu 215041380: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 90% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 84% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 90% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 102% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 86% Analysis Date = 07/31/15 SpikeMix = Crescent 04EE008: 10 µl & ERA 0406-15-03: 10 µl Pct Recovery = 82% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 84% Analysis Date = 09/01/17 SpikeMix = Abs 070717: 20 µl & Abs 070617: 20 µl Pct Recovery = 102% Analysis Date = 09/07/17 SpikeMix = Abs 070717: 10 µl & Abs 070617: 10 µl Pct Recovery = 77% Analysis Date = 06/10/14 SpikeMix = Crescent 03DD004: 20 µl & NSI 032614: 20 µl Pct Recovery = 93% Analysis Date = 06/10/14 SpikeMix = NSI 032614: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 100% Analysis Date = 05/01/14 SpikeMix = Accu 214031115: 20 µl & NSI 032614: 20 µl Pct Recovery = 88% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 104% Analysis Date = 07/01/14 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 100% Analysis Date = 09/09/14 SpikeMix = Accu 214031115: 10 µl & NSI 032614: 10 µl Pct Recovery = 119% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 114% Analysis Date = 07/29/14 SpikeMix = Crescent 03DD004: 10 µl & NSI 032614: 10 µl Pct Recovery = 112% Analysis Date = 05/30/14 SpikeMix = NSI 032614: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 82% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 106% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 94% Analysis Date = 04/09/15 SpikeMix = Accu 214031115: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 99% Analysis Date = 03/06/15 SpikeMix = ERA 0227-14-06.1A: 20 µl & Supelco LC06438: 20 µl Pct Recovery = 106% Analysis Date = 11/14/14 SpikeMix = Crescent 03DD004: 20 µl & ERA 0227-14-06.1A: 20 µl Pct Recovery = 101% Analysis Date = 01/13/15 SpikeMix = Accu 214031115: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 125% Analysis Date = 10/21/14 SpikeMix = ERA 0227-14-06.1A: 10 µl & Supelco LC06438: 10 µl Pct Recovery = 109% Analysis Date = 10/04/14 SpikeMix = Crescent 03DD004: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 107% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Median Pct Recovery = 94% Y = 1
The SGPlot Procedure