BQS OBSP Determination:
ACETONITRILE
METHOD: 4437 , TESTIDCODE: 76997GM016
DATES: 05/07/14 - 09/09/17

Expected Conc. = 5.4104 Median Pct Recovery = 110% Expected Conc. = 5.4104 Median Pct Recovery = 110% Expected Conc. = 5.4104 Median Pct Recovery = 110% Expected Conc. = 5.4104 Median Pct Recovery = 110% Expected Conc. = 5.4104 Median Pct Recovery = 110% Expected Conc. = 3.3815 Median Pct Recovery = 110% Expected Conc. = 3.3815 Median Pct Recovery = 110% Expected Conc. = 3.3815 Median Pct Recovery = 110% Expected Conc. = 3.3815 Median Pct Recovery = 110% Expected Conc. = 3.2448 Median Pct Recovery = 110% Expected Conc. = 3.2448 Median Pct Recovery = 110% Expected Conc. = 3.2448 Median Pct Recovery = 110% Expected Conc. = 3.2448 Median Pct Recovery = 110% Expected Conc. = 3.2448 Median Pct Recovery = 110% Expected Conc. = 3.2448 Median Pct Recovery = 110% Expected Conc. = 3.2448 Median Pct Recovery = 110% Expected Conc. = 3.2448 Median Pct Recovery = 110% Expected Conc. = 3.2 Median Pct Recovery = 110% Expected Conc. = 3.2 Median Pct Recovery = 110% Expected Conc. = 3.2 Median Pct Recovery = 110% Expected Conc. = 3.2 Median Pct Recovery = 110% Expected Conc. = 3.2 Median Pct Recovery = 110% Expected Conc. = 3.2 Median Pct Recovery = 110% Expected Conc. = 3.2 Median Pct Recovery = 110% Expected Conc. = 3.2 Median Pct Recovery = 110% Expected Conc. = 3 Median Pct Recovery = 110% Expected Conc. = 3 Median Pct Recovery = 110% Expected Conc. = 3 Median Pct Recovery = 110% Expected Conc. = 3 Median Pct Recovery = 110% Expected Conc. = 3 Median Pct Recovery = 110% Expected Conc. = 3 Median Pct Recovery = 110% Expected Conc. = 2.4 Median Pct Recovery = 110% Expected Conc. = 2.4 Median Pct Recovery = 110% Expected Conc. = 2.0289 Median Pct Recovery = 110% Expected Conc. = 2.0289 Median Pct Recovery = 110% Expected Conc. = 2.0289 Median Pct Recovery = 110% Expected Conc. = 2.0289 Median Pct Recovery = 110% Expected Conc. = 2.0289 Median Pct Recovery = 110% Expected Conc. = 2.0289 Median Pct Recovery = 110% Expected Conc. = 2.0289 Median Pct Recovery = 110% Expected Conc. = 2.0289 Median Pct Recovery = 110% Expected Conc. = 1.803 Median Pct Recovery = 110% Expected Conc. = 1.803 Median Pct Recovery = 110% Expected Conc. = 1.803 Median Pct Recovery = 110% Expected Conc. = 1.803 Median Pct Recovery = 110% Expected Conc. = 1.8 Median Pct Recovery = 110% Expected Conc. = 1.8 Median Pct Recovery = 110% Expected Conc. = 1.8 Median Pct Recovery = 110% Expected Conc. = 1.8 Median Pct Recovery = 110% Expected Conc. = 1.8 Median Pct Recovery = 110% Expected Conc. = 1.8 Median Pct Recovery = 110% Expected Conc. = 1.6224 Median Pct Recovery = 110% Expected Conc. = 1.6224 Median Pct Recovery = 110% Expected Conc. = 1.6224 Median Pct Recovery = 110% Expected Conc. = 1.6224 Median Pct Recovery = 110% Expected Conc. = 1.6224 Median Pct Recovery = 110% Expected Conc. = 1.6224 Median Pct Recovery = 110% Expected Conc. = 1.6224 Median Pct Recovery = 110% Expected Conc. = 1.6224 Median Pct Recovery = 110% Expected Conc. = 1.6 Median Pct Recovery = 110% Expected Conc. = 1.6 Median Pct Recovery = 110% Expected Conc. = 1.6 Median Pct Recovery = 110% Expected Conc. = 1.6 Median Pct Recovery = 110% Expected Conc. = 1.6 Median Pct Recovery = 110% Expected Conc. = 1.6 Median Pct Recovery = 110% Expected Conc. = 1.6 Median Pct Recovery = 110% Expected Conc. = 1.6 Median Pct Recovery = 110% Expected Conc. = 1.6 Median Pct Recovery = 110% Expected Conc. = 1.6 Median Pct Recovery = 110% Expected Conc. = 1.202 Median Pct Recovery = 110% Expected Conc. = 1.202 Median Pct Recovery = 110% Expected Conc. = 1.202 Median Pct Recovery = 110% Expected Conc. = 1.202 Median Pct Recovery = 110% Expected Conc. = 1.202 Median Pct Recovery = 110% Expected Conc. = 1.202 Median Pct Recovery = 110% Expected Conc. = 1.202 Median Pct Recovery = 110% Expected Conc. = 1.202 Median Pct Recovery = 110% Expected Conc. = 1.202 Median Pct Recovery = 110% Expected Conc. = 1.202 Median Pct Recovery = 110% Expected Conc. = 1.202 Median Pct Recovery = 110% Expected Conc. = 1.202 Median Pct Recovery = 110% Expected Conc. = 1.2 Median Pct Recovery = 110% Expected Conc. = 1.2 Median Pct Recovery = 110% Expected Conc. = 1.2 Median Pct Recovery = 110% Analysis Date = 11/29/16 SpikeMix = Accu 216041354: 40 µl & Abs 060916HVOC: 40 µl Pct Recovery = 157% Analysis Date = 09/23/16 SpikeMix = Phenova B20160303: 40 µl & Accu 216041354: 40 µl Pct Recovery = 149% Analysis Date = 07/15/16 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl Pct Recovery = 141% Analysis Date = 12/23/16 SpikeMix = ChemService 5082800: 25 µl & Accu 216041354: 25 µl & NSI 041416HVOC: 25 µl Pct Recovery = 165% Analysis Date = 09/28/16 SpikeMix = Accu 216041354: 25 µl & Abs 060916HVOC: 25 µl & Accu 216041225: 25 µl Pct Recovery = 200% Analysis Date = 08/17/14 SpikeMix = ERA 0321-14-05: 20 µl & Accu 214031128: 20 µl Pct Recovery = 200% Analysis Date = 07/23/14 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl Pct Recovery = 110% Analysis Date = 07/11/14 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl Pct Recovery = 101% Analysis Date = 05/07/14 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl Pct Recovery = 114% Analysis Date = 03/19/15 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl Pct Recovery = 116% Analysis Date = 02/26/15 SpikeMix = ERA 0321-14-05A: 20 µl & Supelco LC06437: 20 µl Pct Recovery = 106% Analysis Date = 08/20/14 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl Pct Recovery = 101% Analysis Date = 06/07/14 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl Pct Recovery = 109% Analysis Date = 01/22/16 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl Pct Recovery = 107% Analysis Date = 10/09/15 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl Pct Recovery = 96% Analysis Date = 06/25/15 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl Pct Recovery = 97% Analysis Date = 08/16/17 SpikeMix = ChemService 6441300: 15 µl & Spex Organics BW170726021: 15 µl & ChemService 6424 Pct Recovery = 106% Analysis Date = 07/14/17 SpikeMix = Accu 216041354: 15 µl & ChemService 5082800: 15 µl & Accu 216041225: 15 µl Pct Recovery = 119% Analysis Date = 02/24/17 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & Accu 216041225: 15 µl Pct Recovery = 176% Analysis Date = 08/12/16 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl Pct Recovery = 154% Analysis Date = 07/06/16 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl Pct Recovery = 172% Analysis Date = 11/25/15 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl Pct Recovery = 129% Analysis Date = 09/24/15 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl Pct Recovery = 100% Analysis Date = 09/05/15 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl Pct Recovery = 88% Analysis Date = 07/30/15 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl Pct Recovery = 106% Analysis Date = 06/16/15 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl Pct Recovery = 101% Analysis Date = 12/13/14 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl Pct Recovery = 108% Analysis Date = 10/21/14 SpikeMix = ERA 0321-14-05A: 10 µl & Accu 214031128: 10 µl Pct Recovery = 133% Analysis Date = 09/11/14 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl Pct Recovery = 110% Analysis Date = 05/20/14 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl Pct Recovery = 92% Analysis Date = 09/09/17 SpikeMix = Spex Organics BW170726021: 10 µl & Spex Organics BW170725005: 10 µl Pct Recovery = 110% Analysis Date = 11/22/14 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl Pct Recovery = 103% Analysis Date = 11/13/14 SpikeMix = Supelco LC06437: 10 µl & NSI 031814: 10 µl Pct Recovery = 96% Analysis Date = 09/11/14 SpikeMix = ERA 0321-14-05: 10 µl & Supelco LC06437: 10 µl Pct Recovery = 200% Analysis Date = 06/17/14 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl Pct Recovery = 100% Analysis Date = 04/09/16 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl Pct Recovery = 109% Analysis Date = 01/05/16 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl Pct Recovery = 120% Analysis Date = 10/23/15 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl Pct Recovery = 116% Analysis Date = 08/14/15 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl Pct Recovery = 97% Analysis Date = 06/05/15 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl Pct Recovery = 108% Analysis Date = 05/05/15 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl Pct Recovery = 115% Analysis Date = 03/22/16 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl Pct Recovery = 117% Analysis Date = 12/05/15 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl Pct Recovery = 94% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Median Pct Recovery = 110% Y = 1
The SGPlot Procedure