BQS OBSP Determination:
METHYL ACETATE
METHOD: 4437 , TESTIDCODE: 77032GM016
DATES: 05/07/14 - 08/30/17

Expected Conc. = 0.936 Median Pct Recovery = 99% Expected Conc. = 0.936 Median Pct Recovery = 99% Expected Conc. = 0.936 Median Pct Recovery = 99% Expected Conc. = 0.936 Median Pct Recovery = 99% Expected Conc. = 0.936 Median Pct Recovery = 99% Expected Conc. = 0.932 Median Pct Recovery = 99% Expected Conc. = 0.932 Median Pct Recovery = 99% Expected Conc. = 0.585 Median Pct Recovery = 99% Expected Conc. = 0.585 Median Pct Recovery = 99% Expected Conc. = 0.585 Median Pct Recovery = 99% Expected Conc. = 0.585 Median Pct Recovery = 99% Expected Conc. = 0.585 Median Pct Recovery = 99% Expected Conc. = 0.585 Median Pct Recovery = 99% Expected Conc. = 0.585 Median Pct Recovery = 99% Expected Conc. = 0.585 Median Pct Recovery = 99% Expected Conc. = 0.585 Median Pct Recovery = 99% Expected Conc. = 0.585 Median Pct Recovery = 99% Expected Conc. = 0.585 Median Pct Recovery = 99% Expected Conc. = 0.585 Median Pct Recovery = 99% Expected Conc. = 0.585 Median Pct Recovery = 99% Expected Conc. = 0.585 Median Pct Recovery = 99% Expected Conc. = 0.5825 Median Pct Recovery = 99% Expected Conc. = 0.5825 Median Pct Recovery = 99% Expected Conc. = 0.5825 Median Pct Recovery = 99% Expected Conc. = 0.5825 Median Pct Recovery = 99% Expected Conc. = 0.5825 Median Pct Recovery = 99% Expected Conc. = 0.5825 Median Pct Recovery = 99% Expected Conc. = 0.56 Median Pct Recovery = 99% Expected Conc. = 0.56 Median Pct Recovery = 99% Expected Conc. = 0.56 Median Pct Recovery = 99% Expected Conc. = 0.56 Median Pct Recovery = 99% Expected Conc. = 0.56 Median Pct Recovery = 99% Expected Conc. = 0.56 Median Pct Recovery = 99% Expected Conc. = 0.56 Median Pct Recovery = 99% Expected Conc. = 0.56 Median Pct Recovery = 99% Expected Conc. = 0.56 Median Pct Recovery = 99% Expected Conc. = 0.56 Median Pct Recovery = 99% Expected Conc. = 0.56 Median Pct Recovery = 99% Expected Conc. = 0.56 Median Pct Recovery = 99% Expected Conc. = 0.56 Median Pct Recovery = 99% Expected Conc. = 0.56 Median Pct Recovery = 99% Expected Conc. = 0.56 Median Pct Recovery = 99% Expected Conc. = 0.56 Median Pct Recovery = 99% Expected Conc. = 0.525 Median Pct Recovery = 99% Expected Conc. = 0.525 Median Pct Recovery = 99% Expected Conc. = 0.525 Median Pct Recovery = 99% Expected Conc. = 0.525 Median Pct Recovery = 99% Expected Conc. = 0.525 Median Pct Recovery = 99% Expected Conc. = 0.525 Median Pct Recovery = 99% Expected Conc. = 0.525 Median Pct Recovery = 99% Expected Conc. = 0.525 Median Pct Recovery = 99% Expected Conc. = 0.426 Median Pct Recovery = 99% Expected Conc. = 0.426 Median Pct Recovery = 99% Expected Conc. = 0.351 Median Pct Recovery = 99% Expected Conc. = 0.351 Median Pct Recovery = 99% Expected Conc. = 0.351 Median Pct Recovery = 99% Expected Conc. = 0.351 Median Pct Recovery = 99% Expected Conc. = 0.351 Median Pct Recovery = 99% Expected Conc. = 0.351 Median Pct Recovery = 99% Expected Conc. = 0.351 Median Pct Recovery = 99% Expected Conc. = 0.351 Median Pct Recovery = 99% Expected Conc. = 0.3495 Median Pct Recovery = 99% Expected Conc. = 0.3495 Median Pct Recovery = 99% Expected Conc. = 0.3495 Median Pct Recovery = 99% Expected Conc. = 0.3495 Median Pct Recovery = 99% Expected Conc. = 0.3495 Median Pct Recovery = 99% Expected Conc. = 0.3495 Median Pct Recovery = 99% Expected Conc. = 0.3495 Median Pct Recovery = 99% Expected Conc. = 0.3495 Median Pct Recovery = 99% Expected Conc. = 0.3495 Median Pct Recovery = 99% Expected Conc. = 0.3495 Median Pct Recovery = 99% Expected Conc. = 0.3495 Median Pct Recovery = 99% Expected Conc. = 0.3495 Median Pct Recovery = 99% Expected Conc. = 0.3495 Median Pct Recovery = 99% Expected Conc. = 0.3495 Median Pct Recovery = 99% Expected Conc. = 0.3495 Median Pct Recovery = 99% Expected Conc. = 0.3495 Median Pct Recovery = 99% Expected Conc. = 0.3495 Median Pct Recovery = 99% Expected Conc. = 0.3495 Median Pct Recovery = 99% Expected Conc. = 0.315 Median Pct Recovery = 99% Expected Conc. = 0.315 Median Pct Recovery = 99% Expected Conc. = 0.315 Median Pct Recovery = 99% Expected Conc. = 0.315 Median Pct Recovery = 99% Expected Conc. = 0.315 Median Pct Recovery = 99% Expected Conc. = 0.315 Median Pct Recovery = 99% Expected Conc. = 0.315 Median Pct Recovery = 99% Expected Conc. = 0.315 Median Pct Recovery = 99% Expected Conc. = 0.315 Median Pct Recovery = 99% Expected Conc. = 0.315 Median Pct Recovery = 99% Expected Conc. = 0.284 Median Pct Recovery = 99% Expected Conc. = 0.284 Median Pct Recovery = 99% Expected Conc. = 0.284 Median Pct Recovery = 99% Expected Conc. = 0.284 Median Pct Recovery = 99% Expected Conc. = 0.28 Median Pct Recovery = 99% Expected Conc. = 0.28 Median Pct Recovery = 99% Expected Conc. = 0.28 Median Pct Recovery = 99% Expected Conc. = 0.28 Median Pct Recovery = 99% Expected Conc. = 0.28 Median Pct Recovery = 99% Expected Conc. = 0.28 Median Pct Recovery = 99% Expected Conc. = 0.28 Median Pct Recovery = 99% Expected Conc. = 0.28 Median Pct Recovery = 99% Expected Conc. = 0.28 Median Pct Recovery = 99% Expected Conc. = 0.28 Median Pct Recovery = 99% Expected Conc. = 0.28 Median Pct Recovery = 99% Expected Conc. = 0.28 Median Pct Recovery = 99% Expected Conc. = 0.28 Median Pct Recovery = 99% Expected Conc. = 0.28 Median Pct Recovery = 99% Expected Conc. = 0.21 Median Pct Recovery = 99% Expected Conc. = 0.21 Median Pct Recovery = 99% Expected Conc. = 0.21 Median Pct Recovery = 99% Expected Conc. = 0.21 Median Pct Recovery = 99% Expected Conc. = 0.21 Median Pct Recovery = 99% Expected Conc. = 0.21 Median Pct Recovery = 99% Expected Conc. = 0.21 Median Pct Recovery = 99% Expected Conc. = 0.21 Median Pct Recovery = 99% Expected Conc. = 0.21 Median Pct Recovery = 99% Expected Conc. = 0.21 Median Pct Recovery = 99% Expected Conc. = 0.21 Median Pct Recovery = 99% Expected Conc. = 0.21 Median Pct Recovery = 99% Expected Conc. = 0.21 Median Pct Recovery = 99% Expected Conc. = 0.21 Median Pct Recovery = 99% Expected Conc. = 0.21 Median Pct Recovery = 99% Expected Conc. = 0.21 Median Pct Recovery = 99% Expected Conc. = 0.5825 Median Pct Recovery = 99% Analysis Date = 10/21/16 SpikeMix = ChemService 5082800: 40 µl & Supelco LC20145V: 40 µl & NSI 041416HVOC: 40 µl Pct Recovery = 97% Analysis Date = 07/29/16 SpikeMix = Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl Pct Recovery = 88% Analysis Date = 07/06/16 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl Pct Recovery = 74% Analysis Date = 02/02/17 SpikeMix = Abs 060916HVOC: 40 µl & ChemService 5082800: 40 µl & Accu 216041225: 40 µl Pct Recovery = 105% Analysis Date = 06/17/17 SpikeMix = Supelco LC20145V: 25 µl & Phenova B20160303: 25 µl & NSI 041416HVOC: 25 µl Pct Recovery = 81% Analysis Date = 04/13/17 SpikeMix = Accu 216041354: 25 µl & Phenova B20160303: 25 µl & NSI 041416HVOC: 25 µl Pct Recovery = 71% Analysis Date = 12/23/16 SpikeMix = ChemService 5082800: 25 µl & Accu 216041354: 25 µl & NSI 041416HVOC: 25 µl Pct Recovery = 78% Analysis Date = 09/08/16 SpikeMix = Abs 060916HVOC: 25 µl & Phenova B20160303: 25 µl & NSI 041416HVOC: 25 µl Pct Recovery = 98% Analysis Date = 08/11/16 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl Pct Recovery = 75% Analysis Date = 07/14/16 SpikeMix = NSI 041516: 25 µl & ChemService 5082800: 25 µl & NSI 041416HVOC: 25 µl Pct Recovery = 102% Analysis Date = 05/21/16 SpikeMix = Supelco LC20145V: 25 µl & NSI 041516: 25 µl & NSI 041416HVOC: 25 µl Pct Recovery = 94% Analysis Date = 06/24/17 SpikeMix = Supelco LC20145V: 25 µl & Abs 060916HVOC: 25 µl & Accu 216041225: 25 µl Pct Recovery = 108% Analysis Date = 11/10/16 SpikeMix = NSI 041516: 25 µl & Phenova B20160303: 25 µl & Accu 216041225: 25 µl Pct Recovery = 116% Analysis Date = 09/28/16 SpikeMix = Accu 216041354: 25 µl & Abs 060916HVOC: 25 µl & Accu 216041225: 25 µl Pct Recovery = 116% Analysis Date = 03/19/15 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl Pct Recovery = 41% Analysis Date = 01/10/15 SpikeMix = Abs 032014: 20 µl & ERA 0321-14-05A: 20 µl Pct Recovery = 38% Analysis Date = 11/13/14 SpikeMix = NSI 031814: 20 µl & ERA 0321-14-05A: 20 µl Pct Recovery = 32% Analysis Date = 08/20/14 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl Pct Recovery = 41% Analysis Date = 07/23/14 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl Pct Recovery = 39% Analysis Date = 07/03/14 SpikeMix = Abs 032014: 20 µl & ChemService 2615700: 20 µl Pct Recovery = 50% Analysis Date = 06/06/14 SpikeMix = NSI 031814: 20 µl & ChemService 2615700: 20 µl Pct Recovery = 62% Analysis Date = 05/07/14 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl Pct Recovery = 47% Analysis Date = 01/22/16 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl Pct Recovery = 127% Analysis Date = 10/09/15 SpikeMix = ERA 0601-15-05: 25 µl & Accu 215041338: 25 µl Pct Recovery = 109% Analysis Date = 06/26/15 SpikeMix = ChemService 3818700: 25 µl & Accu 215041338: 25 µl Pct Recovery = 113% Analysis Date = 06/25/15 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl Pct Recovery = 94% Analysis Date = 08/16/17 SpikeMix = ChemService 6441300: 15 µl & Spex Organics BW170726021: 15 µl & ChemService 6424 Pct Recovery = 108% Analysis Date = 04/27/17 SpikeMix = Abs 060916HVOC: 15 µl & ChemService 5082800: 15 µl & NSI 041416HVOC: 15 µl Pct Recovery = 78% Analysis Date = 01/03/17 SpikeMix = Supelco LC20145V: 15 µl & Abs 060916HVOC: 15 µl & NSI 041416HVOC: 15 µl Pct Recovery = 74% Analysis Date = 07/06/16 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl Pct Recovery = 77% Analysis Date = 06/03/16 SpikeMix = NSI 041516: 15 µl & Phenova B20160303: 15 µl & NSI 041416HVOC: 15 µl Pct Recovery = 82% Analysis Date = 07/14/17 SpikeMix = Accu 216041354: 15 µl & ChemService 5082800: 15 µl & Accu 216041225: 15 µl Pct Recovery = 98% Analysis Date = 06/01/17 SpikeMix = Accu 216041354: 15 µl & Phenova B20160303: 15 µl & Accu 216041225: 15 µl Pct Recovery = 99% Analysis Date = 03/24/17 SpikeMix = Abs 060916HVOC: 15 µl & Phenova B20160303: 15 µl & Accu 216041225: 15 µl Pct Recovery = 120% Analysis Date = 02/24/17 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & Accu 216041225: 15 µl Pct Recovery = 115% Analysis Date = 02/02/17 SpikeMix = Accu 216041354: 15 µl & NSI 110916: 15 µl & Accu 216041225: 15 µl Pct Recovery = 104% Analysis Date = 11/18/16 SpikeMix = NSI 110916: 15 µl & ChemService 5082800: 15 µl & Accu 216041225: 15 µl Pct Recovery = 104% Analysis Date = 11/02/16 SpikeMix = Supelco LC20145V: 15 µl & Abs 060916HVOC: 15 µl & Accu 216041225: 15 µl Pct Recovery = 101% Analysis Date = 07/27/16 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl Pct Recovery = 98% Analysis Date = 05/20/16 SpikeMix = Accu 216041354: 15 µl & NSI 041516: 15 µl & Accu 216041225: 15 µl Pct Recovery = 112% Analysis Date = 04/28/16 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl Pct Recovery = 142% Analysis Date = 09/24/15 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl Pct Recovery = 119% Analysis Date = 08/24/15 SpikeMix = ERA 0601-15-05: 15 µl & Supelco LC13544: 15 µl Pct Recovery = 130% Analysis Date = 06/16/15 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl Pct Recovery = 99% Analysis Date = 05/14/15 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl Pct Recovery = 103% Analysis Date = 08/30/17 SpikeMix = ChemService 6441300: 10 µl & ChemService 6424500: 10 µl & Spex Organics BW170725 Pct Recovery = 92% Analysis Date = 08/10/17 SpikeMix = ChemService 6441300: 10 µl & ChemService 6441600: 10 µl & ChemService 6424500: 1 Pct Recovery = 102% Analysis Date = 04/25/15 SpikeMix = Abs 032014: 10 µl & ERA 0321-14-05A: 10 µl Pct Recovery = 105% Analysis Date = 12/13/14 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl Pct Recovery = 37% Analysis Date = 11/13/14 SpikeMix = Supelco LC06437: 10 µl & NSI 031814: 10 µl Pct Recovery = 34% Analysis Date = 09/11/14 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl Pct Recovery = 45% Analysis Date = 09/06/14 SpikeMix = NSI 031814: 10 µl & ERA 0321-14-05: 10 µl Pct Recovery = 42% Analysis Date = 07/30/14 SpikeMix = NSI 031814: 10 µl & ChemService 2615700: 10 µl Pct Recovery = 45% Analysis Date = 06/17/14 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl Pct Recovery = 40% Analysis Date = 04/09/16 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl Pct Recovery = 102% Analysis Date = 02/12/16 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl Pct Recovery = 115% Analysis Date = 12/10/15 SpikeMix = ChemService 3818700: 10 µl & Supelco LC13544: 10 µl Pct Recovery = 139% Analysis Date = 12/05/15 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl Pct Recovery = 113% Analysis Date = 11/14/15 SpikeMix = ERA 0601-15-05: 10 µl Pct Recovery = 120% Analysis Date = 10/23/15 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl Pct Recovery = 101% Analysis Date = 08/14/15 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl Pct Recovery = 107% Analysis Date = 05/20/15 SpikeMix = ChemService 3818700: 10 µl & Accu 215041338: 10 µl Pct Recovery = 108% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Median Pct Recovery = 99% Y = 1
The SGPlot Procedure