BQS OBSP Determination:
TIOTROPIUM
METHOD: 2440 , TESTIDCODE: 67508LCM56
DATES: 07/26/14 - 12/10/17

Expected Conc. = 1567.2 Median Pct Recovery = 32% Expected Conc. = 1567.2 Median Pct Recovery = 32% Expected Conc. = 1567.2 Median Pct Recovery = 32% Expected Conc. = 979.5 Median Pct Recovery = 32% Expected Conc. = 979.5 Median Pct Recovery = 32% Expected Conc. = 979.5 Median Pct Recovery = 32% Expected Conc. = 979.5 Median Pct Recovery = 32% Expected Conc. = 979.5 Median Pct Recovery = 32% Expected Conc. = 979.5 Median Pct Recovery = 32% Expected Conc. = 979.5 Median Pct Recovery = 32% Expected Conc. = 979.5 Median Pct Recovery = 32% Expected Conc. = 391.8 Median Pct Recovery = 32% Expected Conc. = 391.8 Median Pct Recovery = 32% Expected Conc. = 391.8 Median Pct Recovery = 32% Expected Conc. = 391.8 Median Pct Recovery = 32% Expected Conc. = 270.5 Median Pct Recovery = 32% Expected Conc. = 270.5 Median Pct Recovery = 32% Expected Conc. = 270.5 Median Pct Recovery = 32% Expected Conc. = 270.5 Median Pct Recovery = 32% Expected Conc. = 260.8 Median Pct Recovery = 32% Expected Conc. = 260.8 Median Pct Recovery = 32% Expected Conc. = 260.8 Median Pct Recovery = 32% Expected Conc. = 260.8 Median Pct Recovery = 32% Expected Conc. = 259.52 Median Pct Recovery = 32% Expected Conc. = 259.52 Median Pct Recovery = 32% Expected Conc. = 259.52 Median Pct Recovery = 32% Expected Conc. = 259.52 Median Pct Recovery = 32% Expected Conc. = 216.4 Median Pct Recovery = 32% Expected Conc. = 216.4 Median Pct Recovery = 32% Expected Conc. = 216.4 Median Pct Recovery = 32% Expected Conc. = 216.4 Median Pct Recovery = 32% Expected Conc. = 216.4 Median Pct Recovery = 32% Expected Conc. = 216.4 Median Pct Recovery = 32% Expected Conc. = 216.4 Median Pct Recovery = 32% Expected Conc. = 216.4 Median Pct Recovery = 32% Expected Conc. = 216.4 Median Pct Recovery = 32% Expected Conc. = 216.4 Median Pct Recovery = 32% Expected Conc. = 216.4 Median Pct Recovery = 32% Expected Conc. = 216.4 Median Pct Recovery = 32% Expected Conc. = 216.4 Median Pct Recovery = 32% Expected Conc. = 216.4 Median Pct Recovery = 32% Expected Conc. = 172.5 Median Pct Recovery = 32% Expected Conc. = 172.5 Median Pct Recovery = 32% Expected Conc. = 172.5 Median Pct Recovery = 32% Expected Conc. = 172.5 Median Pct Recovery = 32% Expected Conc. = 172.5 Median Pct Recovery = 32% Expected Conc. = 172.5 Median Pct Recovery = 32% Expected Conc. = 172.5 Median Pct Recovery = 32% Expected Conc. = 172.5 Median Pct Recovery = 32% Expected Conc. = 172.5 Median Pct Recovery = 32% Expected Conc. = 172.5 Median Pct Recovery = 32% Expected Conc. = 172.5 Median Pct Recovery = 32% Expected Conc. = 172.5 Median Pct Recovery = 32% Expected Conc. = 130.4 Median Pct Recovery = 32% Expected Conc. = 130.4 Median Pct Recovery = 32% Expected Conc. = 130.4 Median Pct Recovery = 32% Expected Conc. = 130.4 Median Pct Recovery = 32% Expected Conc. = 129.76 Median Pct Recovery = 32% Expected Conc. = 129.76 Median Pct Recovery = 32% Expected Conc. = 129.76 Median Pct Recovery = 32% Expected Conc. = 129.76 Median Pct Recovery = 32% Expected Conc. = 129.76 Median Pct Recovery = 32% Expected Conc. = 129.76 Median Pct Recovery = 32% Expected Conc. = 129.76 Median Pct Recovery = 32% Expected Conc. = 129.76 Median Pct Recovery = 32% Expected Conc. = 108.2 Median Pct Recovery = 32% Expected Conc. = 108.2 Median Pct Recovery = 32% Expected Conc. = 108.2 Median Pct Recovery = 32% Expected Conc. = 108.2 Median Pct Recovery = 32% Expected Conc. = 108.2 Median Pct Recovery = 32% Expected Conc. = 108.2 Median Pct Recovery = 32% Expected Conc. = 108.2 Median Pct Recovery = 32% Expected Conc. = 108.2 Median Pct Recovery = 32% Expected Conc. = 108.2 Median Pct Recovery = 32% Expected Conc. = 108.2 Median Pct Recovery = 32% Expected Conc. = 108.2 Median Pct Recovery = 32% Expected Conc. = 108.2 Median Pct Recovery = 32% Expected Conc. = 92 Median Pct Recovery = 32% Expected Conc. = 92 Median Pct Recovery = 32% Expected Conc. = 92 Median Pct Recovery = 32% Expected Conc. = 92 Median Pct Recovery = 32% Expected Conc. = 86.25 Median Pct Recovery = 32% Expected Conc. = 86.25 Median Pct Recovery = 32% Expected Conc. = 65.2 Median Pct Recovery = 32% Expected Conc. = 65.2 Median Pct Recovery = 32% Expected Conc. = 65.2 Median Pct Recovery = 32% Expected Conc. = 65.2 Median Pct Recovery = 32% Expected Conc. = 65.2 Median Pct Recovery = 32% Expected Conc. = 65.2 Median Pct Recovery = 32% Expected Conc. = 65.2 Median Pct Recovery = 32% Expected Conc. = 65.2 Median Pct Recovery = 32% Expected Conc. = 64.88 Median Pct Recovery = 32% Expected Conc. = 64.88 Median Pct Recovery = 32% Expected Conc. = 64.88 Median Pct Recovery = 32% Expected Conc. = 64.88 Median Pct Recovery = 32% Expected Conc. = 64.88 Median Pct Recovery = 32% Expected Conc. = 64.88 Median Pct Recovery = 32% Expected Conc. = 64.88 Median Pct Recovery = 32% Expected Conc. = 64.88 Median Pct Recovery = 32% Expected Conc. = 64.88 Median Pct Recovery = 32% Expected Conc. = 64.88 Median Pct Recovery = 32% Expected Conc. = 64.88 Median Pct Recovery = 32% Expected Conc. = 64.88 Median Pct Recovery = 32% Expected Conc. = 108.2 Median Pct Recovery = 32% Expected Conc. = 108.2 Median Pct Recovery = 32% Expected Conc. = 108.2 Median Pct Recovery = 32% Expected Conc. = 108.2 Median Pct Recovery = 32% Expected Conc. = 108.2 Median Pct Recovery = 32% Expected Conc. = 108.2 Median Pct Recovery = 32% Expected Conc. = 108.2 Median Pct Recovery = 32% Expected Conc. = 108.2 Median Pct Recovery = 32% Expected Conc. = 54.1 Median Pct Recovery = 32% Expected Conc. = 54.1 Median Pct Recovery = 32% Expected Conc. = 32.6 Median Pct Recovery = 32% Expected Conc. = 32.6 Median Pct Recovery = 32% Expected Conc. = 1600 Median Pct Recovery = 32% Expected Conc. = 1600 Median Pct Recovery = 32% Expected Conc. = 1000 Median Pct Recovery = 32% Expected Conc. = 1000 Median Pct Recovery = 32% Expected Conc. = 1000 Median Pct Recovery = 32% Expected Conc. = 1000 Median Pct Recovery = 32% Expected Conc. = 400 Median Pct Recovery = 32% Expected Conc. = 400 Median Pct Recovery = 32% Expected Conc. = 400 Median Pct Recovery = 32% Expected Conc. = 400 Median Pct Recovery = 32% Expected Conc. = 400 Median Pct Recovery = 32% Expected Conc. = 400 Median Pct Recovery = 32% Expected Conc. = 260.8 Median Pct Recovery = 32% Expected Conc. = 260.8 Median Pct Recovery = 32% Expected Conc. = 216.4 Median Pct Recovery = 32% Expected Conc. = 216.4 Median Pct Recovery = 32% Expected Conc. = 172.5 Median Pct Recovery = 32% Expected Conc. = 172.5 Median Pct Recovery = 32% Expected Conc. = 86.25 Median Pct Recovery = 32% Expected Conc. = 86.25 Median Pct Recovery = 32% Expected Conc. = 86.25 Median Pct Recovery = 32% Expected Conc. = 86.25 Median Pct Recovery = 32% Expected Conc. = 65.2 Median Pct Recovery = 32% Expected Conc. = 65.2 Median Pct Recovery = 32% Expected Conc. = 64.88 Median Pct Recovery = 32% Expected Conc. = 64.88 Median Pct Recovery = 32% Expected Conc. = 64.88 Median Pct Recovery = 32% Expected Conc. = 64.88 Median Pct Recovery = 32% Expected Conc. = 32.6 Median Pct Recovery = 32% Expected Conc. = 32.6 Median Pct Recovery = 32% Expected Conc. = 0 Median Pct Recovery = 32% Expected Conc. = 0 Median Pct Recovery = 32% Expected Conc. = 0 Median Pct Recovery = 32% Expected Conc. = 0 Median Pct Recovery = 32% Expected Conc. = 0 Median Pct Recovery = 32% Expected Conc. = 0 Median Pct Recovery = 32% Expected Conc. = 0 Median Pct Recovery = 32% Expected Conc. = 0 Median Pct Recovery = 32% Expected Conc. = 0 Median Pct Recovery = 32% Expected Conc. = 0 Median Pct Recovery = 32% Expected Conc. = 0 Median Pct Recovery = 32% Analysis Date = 12/08/17 SpikeMix = Abs 072517Pharm1: 80 µl & ERA 06281703: 80 µl Pct Recovery = 69% Analysis Date = 09/09/17 SpikeMix = Abs 071817Pharm: 80 µl & Abs 072517Pharm1: 80 µl Pct Recovery = 200% Analysis Date = 12/10/17 SpikeMix = Abs 072517Pharm1: 50 µl & ERA 06281703: 50 µl Pct Recovery = 74% Analysis Date = 09/21/17 SpikeMix = Abs 071817Pharm: 50 µl & Abs 072517Pharm1: 50 µl Pct Recovery = 103% Analysis Date = 08/28/17 SpikeMix = Abs 072517Pharm1: 50 µl & Abs 072517Pharm2: 50 µl Pct Recovery = 111% Analysis Date = 08/26/17 SpikeMix = Abs 072517Pharm1: 50 µl & Abs 071817Pharm: 50 µl Pct Recovery = 43% Analysis Date = 11/08/17 SpikeMix = ERA 06281704: 20 µl & Abs 072517Pharm1: 20 µl Pct Recovery = 32% Analysis Date = 09/23/17 SpikeMix = Abs 072517Pharm1: 20 µl & Abs 072517Pharm2: 20 µl Pct Recovery = 34% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 15% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 17% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 76% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 60% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 14% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 21% Analysis Date = 07/15/17 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 7% Analysis Date = 06/17/17 SpikeMix = Abs 061416: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 39% Analysis Date = 06/08/17 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 30% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 18% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 30% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 23% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 23% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 34% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 55% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 39% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 26% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 10% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 6% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 60% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 49% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 32% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 16% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 19% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 16% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 7% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 16% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 55% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 53% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 3% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 4% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 50% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 53% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 14% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 45% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 23% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 52% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 42% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 29% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 28% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 6% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 32% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 34% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 160% Analysis Date = 02/07/17 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 50% Analysis Date = 02/07/17 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 45% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 36% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 32% Analysis Date = 08/11/17 SpikeMix = Abs 060916PHARM: 20 µl & Abs 071817Pharm: 20 µl Pct Recovery = 57% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 31% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Median Pct Recovery = 32% Y = 1
The SGPlot Procedure