Organic Blind Sample Project
False Positive and Negative Report for
Method: 4437

Analyte TestIDCode CASNumber # Samples
Spiked
# False
Negatives
# Samples
Not Spiked
# False
Positives
1,1-DICHLORO-2-PROPANONE 80336GM016 513-88-2 19 0 30 1
1,2,3-TRICHLOROPROPANE 77443GM016 96-18-4 32 0 17 1
1,2-DIBROMO-3-CHLOROPROPANE 82625GM016 96-12-8 27 0 18 0
1,2-DIBROMOETHANE 77651GM016 106-93-4 33 0 16 1
1,2-DICHLOROPROPANE 34541GM016 78-87-5 21 0 16 0
1,3-DIOXOLANE 81583GM016 646-06-0 19 0 18 0
1,4-DIOXANE 81582GM016 123-91-1 24 0 21 0
1-OCTANOL 77310GM016 111-87-5 35 0 18 0
1METHOXY-4(2-PROPENYL)BENZENE 68066GM016 140-67-0 32 0 17 1
2-ETHOXYETHYL_ACETATE 68728GM016 111-15-9 20 1 33 1
2-HEXANONE,_5-METHYL- 77179GM016 110-12-3 23 0 22 0
2-NITROPROPANE 77076GM016 79-46-9 17 0 20 0
2-PENTANOL,_4-METHYL- 77113GM016 108-11-2 23 0 22 3
2-PROPEN-1-OL 68729GM016 107-18-6 34 0 19 0
4-HEPTANONE,_2,6-DIMETHYL- 77419GM016 108-83-8 32 0 17 3
ACETATE,_ETHYL 81585GM016 141-78-6 26 1 12 1
ACETATE,_ISOBUTYL 77201GM016 110-19-0 34 1 19 1
ACETATE,_ISOPROPYL 45013GM016 108-21-4 35 1 18 1
ACETATE,_PROPYL 45022GM016 109-60-4 35 1 18 1
ACETONITRILE 76997GM016 75-05-8 13 0 14 3
ACROLEIN 34210GM016 107-02-8 2 0 1 0
ALPHA-TERPINEOL 68730GM016 98-55-5 19 0 18 0
BUTANAL 68732GM016 123-72-8 24 1 22 1
BUTANOL 77034GM016 71-36-3 19 0 17 5
CHLOROPICRIN 77548GM016 76-06-2 34 0 19 0
CYCLOHEXANONE 77097GM016 108-94-1 32 0 17 1
DIETHYLAMINE,_N-NITROSO- 78200GM016 55-18-5 32 0 17 1
DIMETHOXYMETHANE 81578GM016 109-87-5 20 0 16 0
HEXACHLOROCYCLOPENTADIENE 34386GM016 77-47-4 18 0 31 12
HEXANOL,_2-ETHYL- 77311GM016 104-76-7 31 2 22 0
ISOPHORONE 34408GM016 78-59-1 21 0 19 1
ISOPROPYL_ALCOHOL 77015GM016 67-63-0 17 0 10 1
METHYL_ACETATE 77032GM016 79-20-9 35 1 18 1
N-PENTANAL 77061GM016 110-62-3 17 0 32 1
NITROBENZENE 34447GM016 98-95-3 33 0 16 1
TERT-BUTYL_ALCOHOL 77035GM016 75-65-0 23 0 22 1
TERT-BUTYL_METHYL_ETHER_(MTBE) 78032GM016 1634-04-4 17 0 12 0
TRANS-CROTONALDEHYDE 68733GM016 123-73-9 26 0 19 0

back to table
Organic Blind Sample Program
False Positives & False Negatives
1,1-DICHLORO-2-PROPANONE
Method: 4437 Testid: 80336GM016
Link to Individual Chart

 newdate = 06/24/17 
 falsepos = 0.986  newdate = 08/30/17 
 CENC_VAL = 0.353  newdate = 08/10/17 
 CENC_VAL = 0.455  newdate = 08/01/17 
 CENC_VAL = 0.582  newdate = 03/24/17 
 CENC_VAL = 0.684  newdate = 03/10/17 
 CENC_VAL = 1.110  newdate = 03/09/17 
 CENC_VAL = 1.510  newdate = 02/24/17 
 CENC_VAL = 0.734  newdate = 01/14/17 
 CENC_VAL = 0.612  newdate = 12/05/16 
 CENC_VAL = 1.510  newdate = 11/10/16 
 CENC_VAL = 1.200  newdate = 09/23/16 
 CENC_VAL = 1.780  newdate = 09/08/16 
 CENC_VAL = 1.050  newdate = 08/11/16 
 CENC_VAL = 0.884  newdate = 07/06/16 
 CENC_VAL = 0.490  newdate = 06/03/16 
 CENC_VAL = 0.555  newdate = 04/28/16 
 CENC_VAL = 0.565  newdate = 04/09/16 
 CENC_VAL = 0.336  newdate = 02/12/16 
 CENC_VAL = 0.309  newdate = 01/22/16 
 CENC_VAL = 0.879  newdate = 08/30/17 
 REPORTING LEVEL = 0.24  newdate = 08/10/17 
 REPORTING LEVEL = 0.24  newdate = 08/10/17 
 REPORTING LEVEL = 0.24  newdate = 08/01/17 
 REPORTING LEVEL = 0.24  newdate = 08/01/17 
 REPORTING LEVEL = 0.24  newdate = 06/24/17 
 REPORTING LEVEL = 0.24  newdate = 06/24/17 
 REPORTING LEVEL = 0.24  newdate = 03/24/17 
 REPORTING LEVEL = 0.24  newdate = 03/24/17 
 REPORTING LEVEL = 0.24  newdate = 03/10/17 
 REPORTING LEVEL = 0.24  newdate = 03/10/17 
 REPORTING LEVEL = 0.24  newdate = 03/09/17 
 REPORTING LEVEL = 0.24  newdate = 03/09/17 
 REPORTING LEVEL = 0.24  newdate = 02/24/17 
 REPORTING LEVEL = 0.24  newdate = 02/24/17 
 REPORTING LEVEL = 0.24  newdate = 01/14/17 
 REPORTING LEVEL = 0.24  newdate = 01/14/17 
 REPORTING LEVEL = 0.24  newdate = 12/05/16 
 REPORTING LEVEL = 0.24  newdate = 12/05/16 
 REPORTING LEVEL = 0.24  newdate = 11/10/16 
 REPORTING LEVEL = 0.24  newdate = 11/10/16 
 REPORTING LEVEL = 0.24  newdate = 09/23/16 
 REPORTING LEVEL = 0.24  newdate = 09/23/16 
 REPORTING LEVEL = 0.24  newdate = 09/08/16 
 REPORTING LEVEL = 0.24  newdate = 09/08/16 
 REPORTING LEVEL = 0.24  newdate = 08/11/16 
 REPORTING LEVEL = 0.24  newdate = 08/11/16 
 REPORTING LEVEL = 0.24  newdate = 07/06/16 
 REPORTING LEVEL = 0.24  newdate = 07/06/16 
 REPORTING LEVEL = 0.24  newdate = 06/03/16 
 REPORTING LEVEL = 0.24  newdate = 06/03/16 
 REPORTING LEVEL = 0.24  newdate = 04/28/16 
 REPORTING LEVEL = 0.24  newdate = 04/28/16 
 REPORTING LEVEL = 0.24  newdate = 04/09/16 
 REPORTING LEVEL = 0.24  newdate = 04/09/16 
 REPORTING LEVEL = 0.24  newdate = 02/12/16 
 REPORTING LEVEL = 0.24  newdate = 02/12/16 
 REPORTING LEVEL = 0.24  newdate = 01/22/16 
 REPORTING LEVEL = 0.24
The SGPlot Procedure

False Positive & Negative Listing for 1,1-DICHLORO-2-PROPANONE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Positive 20171720144 Supelco LC20145V: 25 µl & Abs 060916HVOC: 25 µl & Accu 216041225: 25 µl 0.24 06/24/17 0.986 0

Updated 04/25/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
1,2,3-TRICHLOROPROPANE
Method: 4437 Testid: 77443GM016
Link to Individual Chart

 newdate = 06/24/17 
 falsepos = 0.0251  newdate = 08/16/17 
 CENC_VAL = 0.020  newdate = 08/01/17 
 CENC_VAL = 0.014  newdate = 07/14/17 
 CENC_VAL = 0.014  newdate = 06/13/17 
 CENC_VAL = 0.024  newdate = 04/27/17 
 CENC_VAL = 0.014  newdate = 03/24/17 
 CENC_VAL = 0.018  newdate = 03/10/17 
 CENC_VAL = 0.027  newdate = 03/09/17 
 CENC_VAL = 0.043  newdate = 02/24/17 
 CENC_VAL = 0.014  newdate = 02/02/17 
 CENC_VAL = 0.043  newdate = 01/24/17 
 CENC_VAL = 0.039  newdate = 01/14/17 
 CENC_VAL = 0.014  newdate = 12/23/16 
 CENC_VAL = 0.026  newdate = 12/05/16 
 CENC_VAL = 0.038  newdate = 11/18/16 
 CENC_VAL = 0.016  newdate = 11/10/16 
 CENC_VAL = 0.023  newdate = 10/21/16 
 CENC_VAL = 0.033  newdate = 10/07/16 
 CENC_VAL = 0.015  newdate = 09/23/16 
 CENC_VAL = 0.040  newdate = 09/08/16 
 CENC_VAL = 0.025  newdate = 08/31/16 
 CENC_VAL = 0.026  newdate = 08/18/16 
 CENC_VAL = 0.015  newdate = 08/11/16 
 CENC_VAL = 0.024  newdate = 07/27/16 
 CENC_VAL = 0.014  newdate = 07/14/16 
 CENC_VAL = 0.026  newdate = 07/06/16 
 CENC_VAL = 0.015  newdate = 06/29/16 
 CENC_VAL = 0.037  newdate = 06/23/16 
 CENC_VAL = 0.016  newdate = 06/03/16 
 CENC_VAL = 0.017  newdate = 04/09/16 
 CENC_VAL = 0.009  newdate = 03/22/16 
 CENC_VAL = 0.012  newdate = 01/22/16 
 CENC_VAL = 0.025  newdate = 08/16/17 
 REPORTING LEVEL = 0.006  newdate = 08/01/17 
 REPORTING LEVEL = 0.006  newdate = 08/01/17 
 REPORTING LEVEL = 0.006  newdate = 07/14/17 
 REPORTING LEVEL = 0.006  newdate = 07/14/17 
 REPORTING LEVEL = 0.006  newdate = 06/24/17 
 REPORTING LEVEL = 0.006  newdate = 06/24/17 
 REPORTING LEVEL = 0.006  newdate = 06/13/17 
 REPORTING LEVEL = 0.006  newdate = 06/13/17 
 REPORTING LEVEL = 0.006  newdate = 04/27/17 
 REPORTING LEVEL = 0.006  newdate = 04/27/17 
 REPORTING LEVEL = 0.006  newdate = 03/24/17 
 REPORTING LEVEL = 0.006  newdate = 03/24/17 
 REPORTING LEVEL = 0.006  newdate = 03/10/17 
 REPORTING LEVEL = 0.006  newdate = 03/10/17 
 REPORTING LEVEL = 0.006  newdate = 03/09/17 
 REPORTING LEVEL = 0.006  newdate = 03/09/17 
 REPORTING LEVEL = 0.006  newdate = 02/24/17 
 REPORTING LEVEL = 0.006  newdate = 02/24/17 
 REPORTING LEVEL = 0.006  newdate = 02/02/17 
 REPORTING LEVEL = 0.006  newdate = 02/02/17 
 REPORTING LEVEL = 0.006  newdate = 01/24/17 
 REPORTING LEVEL = 0.006  newdate = 01/24/17 
 REPORTING LEVEL = 0.006  newdate = 01/14/17 
 REPORTING LEVEL = 0.006  newdate = 01/14/17 
 REPORTING LEVEL = 0.006  newdate = 12/23/16 
 REPORTING LEVEL = 0.006  newdate = 12/23/16 
 REPORTING LEVEL = 0.006  newdate = 12/05/16 
 REPORTING LEVEL = 0.006  newdate = 12/05/16 
 REPORTING LEVEL = 0.006  newdate = 11/18/16 
 REPORTING LEVEL = 0.006  newdate = 11/18/16 
 REPORTING LEVEL = 0.006  newdate = 11/10/16 
 REPORTING LEVEL = 0.006  newdate = 11/10/16 
 REPORTING LEVEL = 0.006  newdate = 10/21/16 
 REPORTING LEVEL = 0.006  newdate = 10/21/16 
 REPORTING LEVEL = 0.006  newdate = 10/07/16 
 REPORTING LEVEL = 0.006  newdate = 10/07/16 
 REPORTING LEVEL = 0.006  newdate = 09/23/16 
 REPORTING LEVEL = 0.006  newdate = 09/23/16 
 REPORTING LEVEL = 0.006  newdate = 09/08/16 
 REPORTING LEVEL = 0.006  newdate = 09/08/16 
 REPORTING LEVEL = 0.006  newdate = 08/31/16 
 REPORTING LEVEL = 0.006  newdate = 08/31/16 
 REPORTING LEVEL = 0.006  newdate = 08/18/16 
 REPORTING LEVEL = 0.006  newdate = 08/18/16 
 REPORTING LEVEL = 0.006  newdate = 08/11/16 
 REPORTING LEVEL = 0.006  newdate = 08/11/16 
 REPORTING LEVEL = 0.006  newdate = 07/27/16 
 REPORTING LEVEL = 0.006  newdate = 07/27/16 
 REPORTING LEVEL = 0.006  newdate = 07/14/16 
 REPORTING LEVEL = 0.006  newdate = 07/14/16 
 REPORTING LEVEL = 0.006  newdate = 07/06/16 
 REPORTING LEVEL = 0.006  newdate = 07/06/16 
 REPORTING LEVEL = 0.006  newdate = 06/29/16 
 REPORTING LEVEL = 0.006  newdate = 06/29/16 
 REPORTING LEVEL = 0.006  newdate = 06/23/16 
 REPORTING LEVEL = 0.006  newdate = 06/23/16 
 REPORTING LEVEL = 0.006  newdate = 06/03/16 
 REPORTING LEVEL = 0.006  newdate = 06/03/16 
 REPORTING LEVEL = 0.006  newdate = 04/09/16 
 REPORTING LEVEL = 0.006  newdate = 04/09/16 
 REPORTING LEVEL = 0.006  newdate = 03/22/16 
 REPORTING LEVEL = 0.006  newdate = 03/22/16 
 REPORTING LEVEL = 0.006  newdate = 01/22/16 
 REPORTING LEVEL = 0.006
The SGPlot Procedure

False Positive & Negative Listing for 1,2,3-TRICHLOROPROPANE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Positive 20171720144 Supelco LC20145V: 25 µl & Abs 060916HVOC: 25 µl & Accu 216041225: 25 µl 0.006 06/24/17 0.0251 0

Updated 04/25/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
1,2-DIBROMO-3-CHLOROPROPANE
Method: 4437 Testid: 82625GM016
Link to Individual Chart

 newdate = 08/30/17 
 CENC_VAL = 0.033  newdate = 08/16/17 
 CENC_VAL = 0.053  newdate = 08/16/17 
 CENC_VAL = 0.035  newdate = 08/01/17 
 CENC_VAL = 0.061  newdate = 06/24/17 
 CENC_VAL = 0.081  newdate = 06/13/17 
 CENC_VAL = 0.074  newdate = 04/27/17 
 CENC_VAL = 0.034  newdate = 03/24/17 
 CENC_VAL = 0.051  newdate = 03/09/17 
 CENC_VAL = 0.120  newdate = 02/24/17 
 CENC_VAL = 0.068  newdate = 02/02/17 
 CENC_VAL = 0.130  newdate = 02/02/17 
 CENC_VAL = 0.044  newdate = 01/03/17 
 CENC_VAL = 0.047  newdate = 12/05/16 
 CENC_VAL = 0.128  newdate = 11/29/16 
 CENC_VAL = 0.124  newdate = 11/18/16 
 CENC_VAL = 0.040  newdate = 11/02/16 
 CENC_VAL = 0.053  newdate = 10/07/16 
 CENC_VAL = 0.049  newdate = 09/28/16 
 CENC_VAL = 0.084  newdate = 09/08/16 
 CENC_VAL = 0.083  newdate = 09/08/16 
 CENC_VAL = 0.078  newdate = 08/18/16 
 CENC_VAL = 0.045  newdate = 08/12/16 
 CENC_VAL = 0.044  newdate = 04/28/16 
 CENC_VAL = 0.044  newdate = 04/09/16 
 CENC_VAL = 0.027  newdate = 02/12/16 
 CENC_VAL = 0.032  newdate = 01/22/16 
 CENC_VAL = 0.070  newdate = 08/30/17 
 REPORTING LEVEL = 0.02  newdate = 08/16/17 
 REPORTING LEVEL = 0.02  newdate = 08/16/17 
 REPORTING LEVEL = 0.02  newdate = 08/16/17 
 REPORTING LEVEL = 0.02  newdate = 08/16/17 
 REPORTING LEVEL = 0.02  newdate = 08/01/17 
 REPORTING LEVEL = 0.02  newdate = 08/01/17 
 REPORTING LEVEL = 0.02  newdate = 06/24/17 
 REPORTING LEVEL = 0.02  newdate = 06/24/17 
 REPORTING LEVEL = 0.02  newdate = 06/13/17 
 REPORTING LEVEL = 0.02  newdate = 06/13/17 
 REPORTING LEVEL = 0.02  newdate = 04/27/17 
 REPORTING LEVEL = 0.02  newdate = 04/27/17 
 REPORTING LEVEL = 0.02  newdate = 03/24/17 
 REPORTING LEVEL = 0.02  newdate = 03/24/17 
 REPORTING LEVEL = 0.02  newdate = 03/09/17 
 REPORTING LEVEL = 0.02  newdate = 03/09/17 
 REPORTING LEVEL = 0.02  newdate = 02/24/17 
 REPORTING LEVEL = 0.02  newdate = 02/24/17 
 REPORTING LEVEL = 0.02  newdate = 02/02/17 
 REPORTING LEVEL = 0.02  newdate = 02/02/17 
 REPORTING LEVEL = 0.02  newdate = 02/02/17 
 REPORTING LEVEL = 0.02  newdate = 02/02/17 
 REPORTING LEVEL = 0.02  newdate = 01/03/17 
 REPORTING LEVEL = 0.02  newdate = 01/03/17 
 REPORTING LEVEL = 0.02  newdate = 12/05/16 
 REPORTING LEVEL = 0.02  newdate = 12/05/16 
 REPORTING LEVEL = 0.02  newdate = 11/29/16 
 REPORTING LEVEL = 0.02  newdate = 11/29/16 
 REPORTING LEVEL = 0.02  newdate = 11/18/16 
 REPORTING LEVEL = 0.02  newdate = 11/18/16 
 REPORTING LEVEL = 0.02  newdate = 11/02/16 
 REPORTING LEVEL = 0.02  newdate = 11/02/16 
 REPORTING LEVEL = 0.02  newdate = 10/07/16 
 REPORTING LEVEL = 0.02  newdate = 10/07/16 
 REPORTING LEVEL = 0.02  newdate = 09/28/16 
 REPORTING LEVEL = 0.02  newdate = 09/28/16 
 REPORTING LEVEL = 0.02  newdate = 09/08/16 
 REPORTING LEVEL = 0.02  newdate = 09/08/16 
 REPORTING LEVEL = 0.02  newdate = 09/08/16 
 REPORTING LEVEL = 0.02  newdate = 09/08/16 
 REPORTING LEVEL = 0.02  newdate = 08/18/16 
 REPORTING LEVEL = 0.02  newdate = 08/18/16 
 REPORTING LEVEL = 0.02  newdate = 08/12/16 
 REPORTING LEVEL = 0.02  newdate = 08/12/16 
 REPORTING LEVEL = 0.02  newdate = 04/28/16 
 REPORTING LEVEL = 0.02  newdate = 04/28/16 
 REPORTING LEVEL = 0.02  newdate = 04/09/16 
 REPORTING LEVEL = 0.02  newdate = 04/09/16 
 REPORTING LEVEL = 0.02  newdate = 02/12/16 
 REPORTING LEVEL = 0.02  newdate = 02/12/16 
 REPORTING LEVEL = 0.02  newdate = 01/22/16 
 REPORTING LEVEL = 0.02
The SGPlot Procedure

back to table
Organic Blind Sample Program
False Positives & False Negatives
1,2-DIBROMOETHANE
Method: 4437 Testid: 77651GM016
Link to Individual Chart

 newdate = 06/24/17 
 falsepos = 0.016  newdate = 08/30/17 
 CENC_VAL = 0.009  newdate = 08/10/17 
 CENC_VAL = 0.008  newdate = 08/01/17 
 CENC_VAL = 0.009  newdate = 07/14/17 
 CENC_VAL = 0.009  newdate = 06/13/17 
 CENC_VAL = 0.015  newdate = 04/27/17 
 CENC_VAL = 0.009  newdate = 03/24/17 
 CENC_VAL = 0.010  newdate = 03/10/17 
 CENC_VAL = 0.017  newdate = 03/09/17 
 CENC_VAL = 0.029  newdate = 02/24/17 
 CENC_VAL = 0.010  newdate = 02/02/17 
 CENC_VAL = 0.026  newdate = 01/24/17 
 CENC_VAL = 0.023  newdate = 01/14/17 
 CENC_VAL = 0.010  newdate = 12/23/16 
 CENC_VAL = 0.016  newdate = 12/05/16 
 CENC_VAL = 0.025  newdate = 11/18/16 
 CENC_VAL = 0.009  newdate = 11/10/16 
 CENC_VAL = 0.015  newdate = 10/21/16 
 CENC_VAL = 0.020  newdate = 10/07/16 
 CENC_VAL = 0.008  newdate = 09/23/16 
 CENC_VAL = 0.024  newdate = 09/08/16 
 CENC_VAL = 0.015  newdate = 08/31/16 
 CENC_VAL = 0.014  newdate = 08/18/16 
 CENC_VAL = 0.008  newdate = 08/11/16 
 CENC_VAL = 0.014  newdate = 07/27/16 
 CENC_VAL = 0.008  newdate = 07/14/16 
 CENC_VAL = 0.017  newdate = 07/06/16 
 CENC_VAL = 0.008  newdate = 06/29/16 
 CENC_VAL = 0.024  newdate = 06/23/16 
 CENC_VAL = 0.008  newdate = 06/03/16 
 CENC_VAL = 0.009  newdate = 04/28/16 
 CENC_VAL = 0.010  newdate = 03/22/16 
 CENC_VAL = 0.006  newdate = 02/12/16 
 CENC_VAL = 0.006  newdate = 08/30/17 
 REPORTING LEVEL = 0.004  newdate = 08/10/17 
 REPORTING LEVEL = 0.004  newdate = 08/10/17 
 REPORTING LEVEL = 0.004  newdate = 08/01/17 
 REPORTING LEVEL = 0.004  newdate = 08/01/17 
 REPORTING LEVEL = 0.004  newdate = 07/14/17 
 REPORTING LEVEL = 0.004  newdate = 07/14/17 
 REPORTING LEVEL = 0.004  newdate = 06/24/17 
 REPORTING LEVEL = 0.004  newdate = 06/24/17 
 REPORTING LEVEL = 0.004  newdate = 06/13/17 
 REPORTING LEVEL = 0.004  newdate = 06/13/17 
 REPORTING LEVEL = 0.004  newdate = 04/27/17 
 REPORTING LEVEL = 0.004  newdate = 04/27/17 
 REPORTING LEVEL = 0.004  newdate = 03/24/17 
 REPORTING LEVEL = 0.004  newdate = 03/24/17 
 REPORTING LEVEL = 0.004  newdate = 03/10/17 
 REPORTING LEVEL = 0.004  newdate = 03/10/17 
 REPORTING LEVEL = 0.004  newdate = 03/09/17 
 REPORTING LEVEL = 0.004  newdate = 03/09/17 
 REPORTING LEVEL = 0.004  newdate = 02/24/17 
 REPORTING LEVEL = 0.004  newdate = 02/24/17 
 REPORTING LEVEL = 0.004  newdate = 02/02/17 
 REPORTING LEVEL = 0.004  newdate = 02/02/17 
 REPORTING LEVEL = 0.004  newdate = 01/24/17 
 REPORTING LEVEL = 0.004  newdate = 01/24/17 
 REPORTING LEVEL = 0.004  newdate = 01/14/17 
 REPORTING LEVEL = 0.004  newdate = 01/14/17 
 REPORTING LEVEL = 0.004  newdate = 12/23/16 
 REPORTING LEVEL = 0.004  newdate = 12/23/16 
 REPORTING LEVEL = 0.004  newdate = 12/05/16 
 REPORTING LEVEL = 0.004  newdate = 12/05/16 
 REPORTING LEVEL = 0.004  newdate = 11/18/16 
 REPORTING LEVEL = 0.004  newdate = 11/18/16 
 REPORTING LEVEL = 0.004  newdate = 11/10/16 
 REPORTING LEVEL = 0.004  newdate = 11/10/16 
 REPORTING LEVEL = 0.004  newdate = 10/21/16 
 REPORTING LEVEL = 0.004  newdate = 10/21/16 
 REPORTING LEVEL = 0.004  newdate = 10/07/16 
 REPORTING LEVEL = 0.004  newdate = 10/07/16 
 REPORTING LEVEL = 0.004  newdate = 09/23/16 
 REPORTING LEVEL = 0.004  newdate = 09/23/16 
 REPORTING LEVEL = 0.004  newdate = 09/08/16 
 REPORTING LEVEL = 0.004  newdate = 09/08/16 
 REPORTING LEVEL = 0.004  newdate = 08/31/16 
 REPORTING LEVEL = 0.004  newdate = 08/31/16 
 REPORTING LEVEL = 0.004  newdate = 08/18/16 
 REPORTING LEVEL = 0.004  newdate = 08/18/16 
 REPORTING LEVEL = 0.004  newdate = 08/11/16 
 REPORTING LEVEL = 0.004  newdate = 08/11/16 
 REPORTING LEVEL = 0.004  newdate = 07/27/16 
 REPORTING LEVEL = 0.004  newdate = 07/27/16 
 REPORTING LEVEL = 0.004  newdate = 07/14/16 
 REPORTING LEVEL = 0.004  newdate = 07/14/16 
 REPORTING LEVEL = 0.004  newdate = 07/06/16 
 REPORTING LEVEL = 0.004  newdate = 07/06/16 
 REPORTING LEVEL = 0.004  newdate = 06/29/16 
 REPORTING LEVEL = 0.004  newdate = 06/29/16 
 REPORTING LEVEL = 0.004  newdate = 06/23/16 
 REPORTING LEVEL = 0.004  newdate = 06/23/16 
 REPORTING LEVEL = 0.004  newdate = 06/03/16 
 REPORTING LEVEL = 0.004  newdate = 06/03/16 
 REPORTING LEVEL = 0.004  newdate = 04/28/16 
 REPORTING LEVEL = 0.004  newdate = 04/28/16 
 REPORTING LEVEL = 0.004  newdate = 03/22/16 
 REPORTING LEVEL = 0.004  newdate = 03/22/16 
 REPORTING LEVEL = 0.004  newdate = 02/12/16 
 REPORTING LEVEL = 0.004
The SGPlot Procedure

False Positive & Negative Listing for 1,2-DIBROMOETHANE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Positive 20171720144 Supelco LC20145V: 25 µl & Abs 060916HVOC: 25 µl & Accu 216041225: 25 µl 0.004 06/24/17 0.016 0

Updated 04/25/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
1,2-DICHLOROPROPANE
Method: 4437 Testid: 34541GM016
Link to Individual Chart

 newdate = 08/30/17 
 CENC_VAL = 0.008  newdate = 08/16/17 
 CENC_VAL = 0.011  newdate = 08/10/17 
 CENC_VAL = 0.008  newdate = 08/01/17 
 CENC_VAL = 0.013  newdate = 07/14/17 
 CENC_VAL = 0.009  newdate = 02/24/17 
 CENC_VAL = 0.008  newdate = 02/02/17 
 CENC_VAL = 0.009  newdate = 12/23/16 
 CENC_VAL = 0.017  newdate = 11/29/16 
 CENC_VAL = 0.027  newdate = 09/28/16 
 CENC_VAL = 0.016  newdate = 09/23/16 
 CENC_VAL = 0.024  newdate = 08/31/16 
 CENC_VAL = 0.015  newdate = 08/12/16 
 CENC_VAL = 0.009  newdate = 07/06/16 
 CENC_VAL = 0.027  newdate = 07/06/16 
 CENC_VAL = 0.010  newdate = 06/23/16 
 CENC_VAL = 0.009  newdate = 05/20/16 
 CENC_VAL = 0.009  newdate = 04/28/16 
 CENC_VAL = 0.009  newdate = 04/09/16 
 CENC_VAL = 0.007  newdate = 02/12/16 
 CENC_VAL = 0.006  newdate = 01/22/16 
 CENC_VAL = 0.014  newdate = 08/30/17 
 REPORTING LEVEL = 0.004  newdate = 08/16/17 
 REPORTING LEVEL = 0.004  newdate = 08/16/17 
 REPORTING LEVEL = 0.004  newdate = 08/10/17 
 REPORTING LEVEL = 0.004  newdate = 08/10/17 
 REPORTING LEVEL = 0.004  newdate = 08/01/17 
 REPORTING LEVEL = 0.004  newdate = 08/01/17 
 REPORTING LEVEL = 0.004  newdate = 07/14/17 
 REPORTING LEVEL = 0.004  newdate = 07/14/17 
 REPORTING LEVEL = 0.004  newdate = 02/24/17 
 REPORTING LEVEL = 0.004  newdate = 02/24/17 
 REPORTING LEVEL = 0.004  newdate = 02/02/17 
 REPORTING LEVEL = 0.004  newdate = 02/02/17 
 REPORTING LEVEL = 0.004  newdate = 12/23/16 
 REPORTING LEVEL = 0.004  newdate = 12/23/16 
 REPORTING LEVEL = 0.004  newdate = 11/29/16 
 REPORTING LEVEL = 0.004  newdate = 11/29/16 
 REPORTING LEVEL = 0.004  newdate = 09/28/16 
 REPORTING LEVEL = 0.004  newdate = 09/28/16 
 REPORTING LEVEL = 0.004  newdate = 09/23/16 
 REPORTING LEVEL = 0.004  newdate = 09/23/16 
 REPORTING LEVEL = 0.004  newdate = 08/31/16 
 REPORTING LEVEL = 0.004  newdate = 08/31/16 
 REPORTING LEVEL = 0.004  newdate = 08/12/16 
 REPORTING LEVEL = 0.004  newdate = 08/12/16 
 REPORTING LEVEL = 0.004  newdate = 07/06/16 
 REPORTING LEVEL = 0.004  newdate = 07/06/16 
 REPORTING LEVEL = 0.004  newdate = 07/06/16 
 REPORTING LEVEL = 0.004  newdate = 07/06/16 
 REPORTING LEVEL = 0.004  newdate = 06/23/16 
 REPORTING LEVEL = 0.004  newdate = 06/23/16 
 REPORTING LEVEL = 0.004  newdate = 05/20/16 
 REPORTING LEVEL = 0.004  newdate = 05/20/16 
 REPORTING LEVEL = 0.004  newdate = 04/28/16 
 REPORTING LEVEL = 0.004  newdate = 04/28/16 
 REPORTING LEVEL = 0.004  newdate = 04/09/16 
 REPORTING LEVEL = 0.004  newdate = 04/09/16 
 REPORTING LEVEL = 0.004  newdate = 02/12/16 
 REPORTING LEVEL = 0.004  newdate = 02/12/16 
 REPORTING LEVEL = 0.004  newdate = 01/22/16 
 REPORTING LEVEL = 0.004
The SGPlot Procedure

back to table
Organic Blind Sample Program
False Positives & False Negatives
1,3-DIOXOLANE
Method: 4437 Testid: 81583GM016
Link to Individual Chart

 newdate = 08/30/17 
 CENC_VAL = 0.715  newdate = 08/10/17 
 CENC_VAL = 0.775  newdate = 07/14/17 
 CENC_VAL = 1.000  newdate = 02/24/17 
 CENC_VAL = 1.050  newdate = 02/02/17 
 CENC_VAL = 0.978  newdate = 12/23/16 
 CENC_VAL = 1.320  newdate = 11/29/16 
 CENC_VAL = 2.520  newdate = 09/28/16 
 CENC_VAL = 1.580  newdate = 09/23/16 
 CENC_VAL = 2.230  newdate = 08/31/16 
 CENC_VAL = 1.390  newdate = 08/12/16 
 CENC_VAL = 0.950  newdate = 07/06/16 
 CENC_VAL = 3.050  newdate = 07/06/16 
 CENC_VAL = 0.906  newdate = 06/23/16 
 CENC_VAL = 0.765  newdate = 05/20/16 
 CENC_VAL = 1.330  newdate = 04/28/16 
 CENC_VAL = 0.904  newdate = 04/09/16 
 CENC_VAL = 0.677  newdate = 02/12/16 
 CENC_VAL = 0.555  newdate = 01/22/16 
 CENC_VAL = 1.420  newdate = 08/30/17 
 REPORTING LEVEL = 0.38  newdate = 08/10/17 
 REPORTING LEVEL = 0.38  newdate = 08/10/17 
 REPORTING LEVEL = 0.38  newdate = 07/14/17 
 REPORTING LEVEL = 0.38  newdate = 07/14/17 
 REPORTING LEVEL = 0.38  newdate = 02/24/17 
 REPORTING LEVEL = 0.38  newdate = 02/24/17 
 REPORTING LEVEL = 0.38  newdate = 02/02/17 
 REPORTING LEVEL = 0.38  newdate = 02/02/17 
 REPORTING LEVEL = 0.38  newdate = 12/23/16 
 REPORTING LEVEL = 0.38  newdate = 12/23/16 
 REPORTING LEVEL = 0.38  newdate = 11/29/16 
 REPORTING LEVEL = 0.38  newdate = 11/29/16 
 REPORTING LEVEL = 0.38  newdate = 09/28/16 
 REPORTING LEVEL = 0.38  newdate = 09/28/16 
 REPORTING LEVEL = 0.38  newdate = 09/23/16 
 REPORTING LEVEL = 0.38  newdate = 09/23/16 
 REPORTING LEVEL = 0.38  newdate = 08/31/16 
 REPORTING LEVEL = 0.38  newdate = 08/31/16 
 REPORTING LEVEL = 0.38  newdate = 08/12/16 
 REPORTING LEVEL = 0.38  newdate = 08/12/16 
 REPORTING LEVEL = 0.38  newdate = 07/06/16 
 REPORTING LEVEL = 0.38  newdate = 07/06/16 
 REPORTING LEVEL = 0.38  newdate = 07/06/16 
 REPORTING LEVEL = 0.38  newdate = 07/06/16 
 REPORTING LEVEL = 0.38  newdate = 06/23/16 
 REPORTING LEVEL = 0.38  newdate = 06/23/16 
 REPORTING LEVEL = 0.38  newdate = 05/20/16 
 REPORTING LEVEL = 0.38  newdate = 05/20/16 
 REPORTING LEVEL = 0.38  newdate = 04/28/16 
 REPORTING LEVEL = 0.38  newdate = 04/28/16 
 REPORTING LEVEL = 0.38  newdate = 04/09/16 
 REPORTING LEVEL = 0.38  newdate = 04/09/16 
 REPORTING LEVEL = 0.38  newdate = 02/12/16 
 REPORTING LEVEL = 0.38  newdate = 02/12/16 
 REPORTING LEVEL = 0.38  newdate = 01/22/16 
 REPORTING LEVEL = 0.38
The SGPlot Procedure

back to table
Organic Blind Sample Program
False Positives & False Negatives
1,4-DIOXANE
Method: 4437 Testid: 81582GM016
Link to Individual Chart

 newdate = 08/30/17 
 CENC_VAL = 1.340  newdate = 08/16/17 
 CENC_VAL = 1.250  newdate = 06/24/17 
 CENC_VAL = 2.640  newdate = 06/13/17 
 CENC_VAL = 2.840  newdate = 04/27/17 
 CENC_VAL = 1.540  newdate = 03/24/17 
 CENC_VAL = 1.780  newdate = 03/09/17 
 CENC_VAL = 4.120  newdate = 02/24/17 
 CENC_VAL = 2.520  newdate = 02/02/17 
 CENC_VAL = 4.760  newdate = 02/02/17 
 CENC_VAL = 1.600  newdate = 01/03/17 
 CENC_VAL = 1.510  newdate = 12/05/16 
 CENC_VAL = 4.550  newdate = 11/29/16 
 CENC_VAL = 4.340  newdate = 11/18/16 
 CENC_VAL = 1.490  newdate = 11/02/16 
 CENC_VAL = 2.030  newdate = 10/07/16 
 CENC_VAL = 1.720  newdate = 09/28/16 
 CENC_VAL = 2.910  newdate = 09/08/16 
 CENC_VAL = 2.900  newdate = 09/08/16 
 CENC_VAL = 2.810  newdate = 08/18/16 
 CENC_VAL = 1.760  newdate = 08/12/16 
 CENC_VAL = 1.840  newdate = 04/28/16 
 CENC_VAL = 1.500  newdate = 03/22/16 
 CENC_VAL = 1.000  newdate = 02/12/16 
 CENC_VAL = 1.000  newdate = 08/30/17 
 REPORTING LEVEL = 0.7  newdate = 08/16/17 
 REPORTING LEVEL = 0.7  newdate = 08/16/17 
 REPORTING LEVEL = 0.7  newdate = 06/24/17 
 REPORTING LEVEL = 0.7  newdate = 06/24/17 
 REPORTING LEVEL = 0.7  newdate = 06/13/17 
 REPORTING LEVEL = 0.7  newdate = 06/13/17 
 REPORTING LEVEL = 0.7  newdate = 04/27/17 
 REPORTING LEVEL = 0.7  newdate = 04/27/17 
 REPORTING LEVEL = 0.7  newdate = 03/24/17 
 REPORTING LEVEL = 0.7  newdate = 03/24/17 
 REPORTING LEVEL = 0.7  newdate = 03/09/17 
 REPORTING LEVEL = 0.7  newdate = 03/09/17 
 REPORTING LEVEL = 0.7  newdate = 02/24/17 
 REPORTING LEVEL = 0.7  newdate = 02/24/17 
 REPORTING LEVEL = 0.7  newdate = 02/02/17 
 REPORTING LEVEL = 0.7  newdate = 02/02/17 
 REPORTING LEVEL = 0.7  newdate = 02/02/17 
 REPORTING LEVEL = 0.7  newdate = 02/02/17 
 REPORTING LEVEL = 0.7  newdate = 01/03/17 
 REPORTING LEVEL = 0.7  newdate = 01/03/17 
 REPORTING LEVEL = 0.7  newdate = 12/05/16 
 REPORTING LEVEL = 0.7  newdate = 12/05/16 
 REPORTING LEVEL = 0.7  newdate = 11/29/16 
 REPORTING LEVEL = 0.7  newdate = 11/29/16 
 REPORTING LEVEL = 0.7  newdate = 11/18/16 
 REPORTING LEVEL = 0.7  newdate = 11/18/16 
 REPORTING LEVEL = 0.7  newdate = 11/02/16 
 REPORTING LEVEL = 0.7  newdate = 11/02/16 
 REPORTING LEVEL = 0.7  newdate = 10/07/16 
 REPORTING LEVEL = 0.7  newdate = 10/07/16 
 REPORTING LEVEL = 0.7  newdate = 09/28/16 
 REPORTING LEVEL = 0.7  newdate = 09/28/16 
 REPORTING LEVEL = 0.7  newdate = 09/08/16 
 REPORTING LEVEL = 0.7  newdate = 09/08/16 
 REPORTING LEVEL = 0.7  newdate = 09/08/16 
 REPORTING LEVEL = 0.7  newdate = 09/08/16 
 REPORTING LEVEL = 0.7  newdate = 08/18/16 
 REPORTING LEVEL = 0.7  newdate = 08/18/16 
 REPORTING LEVEL = 0.7  newdate = 08/12/16 
 REPORTING LEVEL = 0.7  newdate = 08/12/16 
 REPORTING LEVEL = 0.7  newdate = 04/28/16 
 REPORTING LEVEL = 0.7  newdate = 04/28/16 
 REPORTING LEVEL = 0.7  newdate = 03/22/16 
 REPORTING LEVEL = 0.7  newdate = 03/22/16 
 REPORTING LEVEL = 0.7  newdate = 02/12/16 
 REPORTING LEVEL = 0.7
The SGPlot Procedure

back to table
Organic Blind Sample Program
False Positives & False Negatives
1-OCTANOL
Method: 4437 Testid: 77310GM016
Link to Individual Chart

 newdate = 08/30/17 
 CENC_VAL = 2.810  newdate = 08/16/17 
 CENC_VAL = 4.500  newdate = 08/16/17 
 CENC_VAL = 2.960  newdate = 08/01/17 
 CENC_VAL = 4.700  newdate = 06/24/17 
 CENC_VAL = 6.980  newdate = 06/13/17 
 CENC_VAL = 5.970  newdate = 04/27/17 
 CENC_VAL = 3.770  newdate = 03/24/17 
 CENC_VAL = 4.150  newdate = 03/09/17 
 CENC_VAL = 11.600  newdate = 02/24/17 
 CENC_VAL = 5.960  newdate = 02/02/17 
 CENC_VAL = 9.490  newdate = 02/02/17 
 CENC_VAL = 3.550  newdate = 01/03/17 
 CENC_VAL = 3.830  newdate = 12/05/16 
 CENC_VAL = 10.300  newdate = 11/29/16 
 CENC_VAL = 9.650  newdate = 11/18/16 
 CENC_VAL = 3.760  newdate = 11/10/16 
 CENC_VAL = 6.770  newdate = 11/02/16 
 CENC_VAL = 3.620  newdate = 10/07/16 
 CENC_VAL = 4.310  newdate = 09/28/16 
 CENC_VAL = 6.350  newdate = 09/08/16 
 CENC_VAL = 6.520  newdate = 09/08/16 
 CENC_VAL = 6.360  newdate = 08/18/16 
 CENC_VAL = 4.310  newdate = 08/12/16 
 CENC_VAL = 3.940  newdate = 07/29/16 
 CENC_VAL = 10.200  newdate = 07/14/16 
 CENC_VAL = 4.990  newdate = 07/06/16 
 CENC_VAL = 9.120  newdate = 06/29/16 
 CENC_VAL = 9.760  newdate = 06/03/16 
 CENC_VAL = 3.750  newdate = 05/21/16 
 CENC_VAL = 5.980  newdate = 05/20/16 
 CENC_VAL = 3.540  newdate = 04/28/16 
 CENC_VAL = 3.680  newdate = 04/09/16 
 CENC_VAL = 2.150  newdate = 02/12/16 
 CENC_VAL = 2.270  newdate = 01/22/16 
 CENC_VAL = 4.950  newdate = 08/30/17 
 REPORTING LEVEL = 1.8  newdate = 08/16/17 
 REPORTING LEVEL = 1.8  newdate = 08/16/17 
 REPORTING LEVEL = 1.8  newdate = 08/16/17 
 REPORTING LEVEL = 1.8  newdate = 08/16/17 
 REPORTING LEVEL = 1.8  newdate = 08/01/17 
 REPORTING LEVEL = 1.8  newdate = 08/01/17 
 REPORTING LEVEL = 1.8  newdate = 06/24/17 
 REPORTING LEVEL = 1.8  newdate = 06/24/17 
 REPORTING LEVEL = 1.8  newdate = 06/13/17 
 REPORTING LEVEL = 1.8  newdate = 06/13/17 
 REPORTING LEVEL = 1.8  newdate = 04/27/17 
 REPORTING LEVEL = 1.8  newdate = 04/27/17 
 REPORTING LEVEL = 1.8  newdate = 03/24/17 
 REPORTING LEVEL = 1.8  newdate = 03/24/17 
 REPORTING LEVEL = 1.8  newdate = 03/09/17 
 REPORTING LEVEL = 1.8  newdate = 03/09/17 
 REPORTING LEVEL = 1.8  newdate = 02/24/17 
 REPORTING LEVEL = 1.8  newdate = 02/24/17 
 REPORTING LEVEL = 1.8  newdate = 02/02/17 
 REPORTING LEVEL = 1.8  newdate = 02/02/17 
 REPORTING LEVEL = 1.8  newdate = 02/02/17 
 REPORTING LEVEL = 1.8  newdate = 02/02/17 
 REPORTING LEVEL = 1.8  newdate = 01/03/17 
 REPORTING LEVEL = 1.8  newdate = 01/03/17 
 REPORTING LEVEL = 1.8  newdate = 12/05/16 
 REPORTING LEVEL = 1.8  newdate = 12/05/16 
 REPORTING LEVEL = 1.8  newdate = 11/29/16 
 REPORTING LEVEL = 1.8  newdate = 11/29/16 
 REPORTING LEVEL = 1.8  newdate = 11/18/16 
 REPORTING LEVEL = 1.8  newdate = 11/18/16 
 REPORTING LEVEL = 1.8  newdate = 11/10/16 
 REPORTING LEVEL = 1.8  newdate = 11/10/16 
 REPORTING LEVEL = 1.8  newdate = 11/02/16 
 REPORTING LEVEL = 1.8  newdate = 11/02/16 
 REPORTING LEVEL = 1.8  newdate = 10/07/16 
 REPORTING LEVEL = 1.8  newdate = 10/07/16 
 REPORTING LEVEL = 1.8  newdate = 09/28/16 
 REPORTING LEVEL = 1.8  newdate = 09/28/16 
 REPORTING LEVEL = 1.8  newdate = 09/08/16 
 REPORTING LEVEL = 1.8  newdate = 09/08/16 
 REPORTING LEVEL = 1.8  newdate = 09/08/16 
 REPORTING LEVEL = 1.8  newdate = 09/08/16 
 REPORTING LEVEL = 1.8  newdate = 08/18/16 
 REPORTING LEVEL = 1.8  newdate = 08/18/16 
 REPORTING LEVEL = 1.8  newdate = 08/12/16 
 REPORTING LEVEL = 1.8  newdate = 08/12/16 
 REPORTING LEVEL = 1.8  newdate = 07/29/16 
 REPORTING LEVEL = 1.8  newdate = 07/29/16 
 REPORTING LEVEL = 1.8  newdate = 07/14/16 
 REPORTING LEVEL = 1.8  newdate = 07/14/16 
 REPORTING LEVEL = 1.8  newdate = 07/06/16 
 REPORTING LEVEL = 1.8  newdate = 07/06/16 
 REPORTING LEVEL = 1.8  newdate = 06/29/16 
 REPORTING LEVEL = 1.8  newdate = 06/29/16 
 REPORTING LEVEL = 1.8  newdate = 06/03/16 
 REPORTING LEVEL = 1.8  newdate = 06/03/16 
 REPORTING LEVEL = 1.8  newdate = 05/21/16 
 REPORTING LEVEL = 1.8  newdate = 05/21/16 
 REPORTING LEVEL = 1.8  newdate = 05/20/16 
 REPORTING LEVEL = 1.8  newdate = 05/20/16 
 REPORTING LEVEL = 1.8  newdate = 04/28/16 
 REPORTING LEVEL = 1.8  newdate = 04/28/16 
 REPORTING LEVEL = 1.8  newdate = 04/09/16 
 REPORTING LEVEL = 1.8  newdate = 04/09/16 
 REPORTING LEVEL = 1.8  newdate = 02/12/16 
 REPORTING LEVEL = 1.8  newdate = 02/12/16 
 REPORTING LEVEL = 1.8  newdate = 01/22/16 
 REPORTING LEVEL = 1.8
The SGPlot Procedure

back to table
Organic Blind Sample Program
False Positives & False Negatives
1METHOXY-4(2-PROPENYL)BENZENE
Method: 4437 Testid: 68066GM016
Link to Individual Chart

 newdate = 06/24/17 
 falsepos = 1.2  newdate = 08/16/17 
 CENC_VAL = 0.726  newdate = 08/01/17 
 CENC_VAL = 0.866  newdate = 07/14/17 
 CENC_VAL = 0.545  newdate = 06/13/17 
 CENC_VAL = 0.924  newdate = 04/27/17 
 CENC_VAL = 0.604  newdate = 03/24/17 
 CENC_VAL = 0.659  newdate = 03/10/17 
 CENC_VAL = 0.879  newdate = 03/09/17 
 CENC_VAL = 1.470  newdate = 02/24/17 
 CENC_VAL = 0.610  newdate = 02/02/17 
 CENC_VAL = 1.290  newdate = 01/24/17 
 CENC_VAL = 1.340  newdate = 01/14/17 
 CENC_VAL = 0.476  newdate = 12/23/16 
 CENC_VAL = 0.881  newdate = 12/05/16 
 CENC_VAL = 1.590  newdate = 11/18/16 
 CENC_VAL = 0.908  newdate = 11/18/16 
 CENC_VAL = 0.546  newdate = 10/21/16 
 CENC_VAL = 1.740  newdate = 10/07/16 
 CENC_VAL = 0.744  newdate = 09/23/16 
 CENC_VAL = 1.530  newdate = 09/08/16 
 CENC_VAL = 1.000  newdate = 08/31/16 
 CENC_VAL = 0.851  newdate = 08/18/16 
 CENC_VAL = 0.568  newdate = 08/11/16 
 CENC_VAL = 0.987  newdate = 07/27/16 
 CENC_VAL = 0.529  newdate = 07/14/16 
 CENC_VAL = 1.130  newdate = 07/06/16 
 CENC_VAL = 0.563  newdate = 06/29/16 
 CENC_VAL = 1.660  newdate = 06/23/16 
 CENC_VAL = 0.633  newdate = 06/03/16 
 CENC_VAL = 0.698  newdate = 04/28/16 
 CENC_VAL = 0.626  newdate = 03/22/16 
 CENC_VAL = 0.384  newdate = 02/12/16 
 CENC_VAL = 0.330  newdate = 08/16/17 
 REPORTING LEVEL = 0.3  newdate = 08/01/17 
 REPORTING LEVEL = 0.3  newdate = 08/01/17 
 REPORTING LEVEL = 0.3  newdate = 07/14/17 
 REPORTING LEVEL = 0.3  newdate = 07/14/17 
 REPORTING LEVEL = 0.3  newdate = 06/24/17 
 REPORTING LEVEL = 0.3  newdate = 06/24/17 
 REPORTING LEVEL = 0.3  newdate = 06/13/17 
 REPORTING LEVEL = 0.3  newdate = 06/13/17 
 REPORTING LEVEL = 0.3  newdate = 04/27/17 
 REPORTING LEVEL = 0.3  newdate = 04/27/17 
 REPORTING LEVEL = 0.3  newdate = 03/24/17 
 REPORTING LEVEL = 0.3  newdate = 03/24/17 
 REPORTING LEVEL = 0.3  newdate = 03/10/17 
 REPORTING LEVEL = 0.3  newdate = 03/10/17 
 REPORTING LEVEL = 0.3  newdate = 03/09/17 
 REPORTING LEVEL = 0.3  newdate = 03/09/17 
 REPORTING LEVEL = 0.3  newdate = 02/24/17 
 REPORTING LEVEL = 0.3  newdate = 02/24/17 
 REPORTING LEVEL = 0.3  newdate = 02/02/17 
 REPORTING LEVEL = 0.3  newdate = 02/02/17 
 REPORTING LEVEL = 0.3  newdate = 01/24/17 
 REPORTING LEVEL = 0.3  newdate = 01/24/17 
 REPORTING LEVEL = 0.3  newdate = 01/14/17 
 REPORTING LEVEL = 0.3  newdate = 01/14/17 
 REPORTING LEVEL = 0.3  newdate = 12/23/16 
 REPORTING LEVEL = 0.3  newdate = 12/23/16 
 REPORTING LEVEL = 0.3  newdate = 12/05/16 
 REPORTING LEVEL = 0.3  newdate = 12/05/16 
 REPORTING LEVEL = 0.3  newdate = 11/18/16 
 REPORTING LEVEL = 0.3  newdate = 11/18/16 
 REPORTING LEVEL = 0.3  newdate = 11/18/16 
 REPORTING LEVEL = 0.3  newdate = 11/18/16 
 REPORTING LEVEL = 0.3  newdate = 10/21/16 
 REPORTING LEVEL = 0.3  newdate = 10/21/16 
 REPORTING LEVEL = 0.3  newdate = 10/07/16 
 REPORTING LEVEL = 0.3  newdate = 10/07/16 
 REPORTING LEVEL = 0.3  newdate = 09/23/16 
 REPORTING LEVEL = 0.3  newdate = 09/23/16 
 REPORTING LEVEL = 0.3  newdate = 09/08/16 
 REPORTING LEVEL = 0.3  newdate = 09/08/16 
 REPORTING LEVEL = 0.3  newdate = 08/31/16 
 REPORTING LEVEL = 0.3  newdate = 08/31/16 
 REPORTING LEVEL = 0.3  newdate = 08/18/16 
 REPORTING LEVEL = 0.3  newdate = 08/18/16 
 REPORTING LEVEL = 0.3  newdate = 08/11/16 
 REPORTING LEVEL = 0.3  newdate = 08/11/16 
 REPORTING LEVEL = 0.3  newdate = 07/27/16 
 REPORTING LEVEL = 0.3  newdate = 07/27/16 
 REPORTING LEVEL = 0.3  newdate = 07/14/16 
 REPORTING LEVEL = 0.3  newdate = 07/14/16 
 REPORTING LEVEL = 0.3  newdate = 07/06/16 
 REPORTING LEVEL = 0.3  newdate = 07/06/16 
 REPORTING LEVEL = 0.3  newdate = 06/29/16 
 REPORTING LEVEL = 0.3  newdate = 06/29/16 
 REPORTING LEVEL = 0.3  newdate = 06/23/16 
 REPORTING LEVEL = 0.3  newdate = 06/23/16 
 REPORTING LEVEL = 0.3  newdate = 06/03/16 
 REPORTING LEVEL = 0.3  newdate = 06/03/16 
 REPORTING LEVEL = 0.3  newdate = 04/28/16 
 REPORTING LEVEL = 0.3  newdate = 04/28/16 
 REPORTING LEVEL = 0.3  newdate = 03/22/16 
 REPORTING LEVEL = 0.3  newdate = 03/22/16 
 REPORTING LEVEL = 0.3  newdate = 02/12/16 
 REPORTING LEVEL = 0.3
The SGPlot Procedure

False Positive & Negative Listing for 1METHOXY-4(2-PROPENYL)BENZENE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Positive 20171720144 Supelco LC20145V: 25 µl & Abs 060916HVOC: 25 µl & Accu 216041225: 25 µl 0.3 06/24/17 1.2 0

Updated 04/25/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
2-ETHOXYETHYL_ACETATE
Method: 4437 Testid: 68728GM016
Link to Individual Chart

 newdate = 03/10/17 
 falseneg = -0.01  newdate = 06/23/16 
 falsepos = 8.19  newdate = 08/30/17 
 CENC_VAL = 7.490  newdate = 08/16/17 
 CENC_VAL = 14.700  newdate = 08/10/17 
 CENC_VAL = 9.640  newdate = 07/14/17 
 CENC_VAL = 13.600  newdate = 06/24/17 
 CENC_VAL = 20.500  newdate = 06/01/17 
 CENC_VAL = 11.800  newdate = 03/24/17 
 CENC_VAL = 17.800  newdate = 02/24/17 
 CENC_VAL = 13.300  newdate = 02/02/17 
 CENC_VAL = 34.800  newdate = 02/02/17 
 CENC_VAL = 13.100  newdate = 11/18/16 
 CENC_VAL = 12.900  newdate = 11/10/16 
 CENC_VAL = 26.200  newdate = 11/02/16 
 CENC_VAL = 13.900  newdate = 09/28/16 
 CENC_VAL = 27.600  newdate = 07/27/16 
 CENC_VAL = 11.400  newdate = 05/20/16 
 CENC_VAL = 12.800  newdate = 04/28/16 
 CENC_VAL = 11.000  newdate = 03/22/16 
 CENC_VAL = 8.600  newdate = 02/12/16 
 CENC_VAL = 7.180  newdate = 08/30/17 
 REPORTING LEVEL = 5.4  newdate = 08/16/17 
 REPORTING LEVEL = 5.4  newdate = 08/16/17 
 REPORTING LEVEL = 5.4  newdate = 08/10/17 
 REPORTING LEVEL = 5.4  newdate = 08/10/17 
 REPORTING LEVEL = 5.4  newdate = 07/14/17 
 REPORTING LEVEL = 5.4  newdate = 07/14/17 
 REPORTING LEVEL = 5.4  newdate = 06/24/17 
 REPORTING LEVEL = 5.4  newdate = 06/24/17 
 REPORTING LEVEL = 5.4  newdate = 06/01/17 
 REPORTING LEVEL = 5.4  newdate = 06/01/17 
 REPORTING LEVEL = 5.4  newdate = 03/24/17 
 REPORTING LEVEL = 5.4  newdate = 03/24/17 
 REPORTING LEVEL = 5.4  newdate = 03/10/17 
 REPORTING LEVEL = 5.4  newdate = 03/10/17 
 REPORTING LEVEL = 5.4  newdate = 02/24/17 
 REPORTING LEVEL = 5.4  newdate = 02/24/17 
 REPORTING LEVEL = 5.4  newdate = 02/02/17 
 REPORTING LEVEL = 5.4  newdate = 02/02/17 
 REPORTING LEVEL = 5.4  newdate = 02/02/17 
 REPORTING LEVEL = 5.4  newdate = 02/02/17 
 REPORTING LEVEL = 5.4  newdate = 11/18/16 
 REPORTING LEVEL = 5.4  newdate = 11/18/16 
 REPORTING LEVEL = 5.4  newdate = 11/10/16 
 REPORTING LEVEL = 5.4  newdate = 11/10/16 
 REPORTING LEVEL = 5.4  newdate = 11/02/16 
 REPORTING LEVEL = 5.4  newdate = 11/02/16 
 REPORTING LEVEL = 5.4  newdate = 09/28/16 
 REPORTING LEVEL = 5.4  newdate = 09/28/16 
 REPORTING LEVEL = 5.4  newdate = 07/27/16 
 REPORTING LEVEL = 5.4  newdate = 07/27/16 
 REPORTING LEVEL = 5.4  newdate = 06/23/16 
 REPORTING LEVEL = 5.4  newdate = 06/23/16 
 REPORTING LEVEL = 5.4  newdate = 05/20/16 
 REPORTING LEVEL = 5.4  newdate = 05/20/16 
 REPORTING LEVEL = 5.4  newdate = 04/28/16 
 REPORTING LEVEL = 5.4  newdate = 04/28/16 
 REPORTING LEVEL = 5.4  newdate = 03/22/16 
 REPORTING LEVEL = 5.4  newdate = 03/22/16 
 REPORTING LEVEL = 5.4  newdate = 02/12/16 
 REPORTING LEVEL = 5.4  Y = 0
The SGPlot Procedure

False Positive & Negative Listing for 2-ETHOXYETHYL_ACETATE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20170680005 Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & Accu 216041225: 25 µl 5.4 03/10/17 < 5.4 22.57
False Positive 20161680364   5.4 06/23/16 8.19 0

Updated 04/25/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
2-HEXANONE,_5-METHYL-
Method: 4437 Testid: 77179GM016
Link to Individual Chart

 newdate = 08/16/17 
 CENC_VAL = 0.067  newdate = 06/24/17 
 CENC_VAL = 0.087  newdate = 06/13/17 
 CENC_VAL = 0.079  newdate = 04/27/17 
 CENC_VAL = 0.049  newdate = 03/24/17 
 CENC_VAL = 0.056  newdate = 03/09/17 
 CENC_VAL = 0.126  newdate = 02/24/17 
 CENC_VAL = 0.069  newdate = 02/02/17 
 CENC_VAL = 0.143  newdate = 02/02/17 
 CENC_VAL = 0.043  newdate = 01/03/17 
 CENC_VAL = 0.055  newdate = 12/05/16 
 CENC_VAL = 0.147  newdate = 11/29/16 
 CENC_VAL = 0.150  newdate = 11/18/16 
 CENC_VAL = 0.043  newdate = 11/02/16 
 CENC_VAL = 0.050  newdate = 10/07/16 
 CENC_VAL = 0.053  newdate = 09/28/16 
 CENC_VAL = 0.091  newdate = 09/08/16 
 CENC_VAL = 0.085  newdate = 09/08/16 
 CENC_VAL = 0.085  newdate = 08/18/16 
 CENC_VAL = 0.048  newdate = 08/12/16 
 CENC_VAL = 0.043  newdate = 04/28/16 
 CENC_VAL = 0.046  newdate = 03/22/16 
 CENC_VAL = 0.039  newdate = 02/12/16 
 CENC_VAL = 0.035  newdate = 08/16/17 
 REPORTING LEVEL = 0.022  newdate = 06/24/17 
 REPORTING LEVEL = 0.022  newdate = 06/24/17 
 REPORTING LEVEL = 0.022  newdate = 06/13/17 
 REPORTING LEVEL = 0.022  newdate = 06/13/17 
 REPORTING LEVEL = 0.022  newdate = 04/27/17 
 REPORTING LEVEL = 0.022  newdate = 04/27/17 
 REPORTING LEVEL = 0.022  newdate = 03/24/17 
 REPORTING LEVEL = 0.022  newdate = 03/24/17 
 REPORTING LEVEL = 0.022  newdate = 03/09/17 
 REPORTING LEVEL = 0.022  newdate = 03/09/17 
 REPORTING LEVEL = 0.022  newdate = 02/24/17 
 REPORTING LEVEL = 0.022  newdate = 02/24/17 
 REPORTING LEVEL = 0.022  newdate = 02/02/17 
 REPORTING LEVEL = 0.022  newdate = 02/02/17 
 REPORTING LEVEL = 0.022  newdate = 02/02/17 
 REPORTING LEVEL = 0.022  newdate = 02/02/17 
 REPORTING LEVEL = 0.022  newdate = 01/03/17 
 REPORTING LEVEL = 0.022  newdate = 01/03/17 
 REPORTING LEVEL = 0.022  newdate = 12/05/16 
 REPORTING LEVEL = 0.022  newdate = 12/05/16 
 REPORTING LEVEL = 0.022  newdate = 11/29/16 
 REPORTING LEVEL = 0.022  newdate = 11/29/16 
 REPORTING LEVEL = 0.022  newdate = 11/18/16 
 REPORTING LEVEL = 0.022  newdate = 11/18/16 
 REPORTING LEVEL = 0.022  newdate = 11/02/16 
 REPORTING LEVEL = 0.022  newdate = 11/02/16 
 REPORTING LEVEL = 0.022  newdate = 10/07/16 
 REPORTING LEVEL = 0.022  newdate = 10/07/16 
 REPORTING LEVEL = 0.022  newdate = 09/28/16 
 REPORTING LEVEL = 0.022  newdate = 09/28/16 
 REPORTING LEVEL = 0.022  newdate = 09/08/16 
 REPORTING LEVEL = 0.022  newdate = 09/08/16 
 REPORTING LEVEL = 0.022  newdate = 09/08/16 
 REPORTING LEVEL = 0.022  newdate = 09/08/16 
 REPORTING LEVEL = 0.022  newdate = 08/18/16 
 REPORTING LEVEL = 0.022  newdate = 08/18/16 
 REPORTING LEVEL = 0.022  newdate = 08/12/16 
 REPORTING LEVEL = 0.022  newdate = 08/12/16 
 REPORTING LEVEL = 0.022  newdate = 04/28/16 
 REPORTING LEVEL = 0.022  newdate = 04/28/16 
 REPORTING LEVEL = 0.022  newdate = 03/22/16 
 REPORTING LEVEL = 0.022  newdate = 03/22/16 
 REPORTING LEVEL = 0.022  newdate = 02/12/16 
 REPORTING LEVEL = 0.022
The SGPlot Procedure

back to table
Organic Blind Sample Program
False Positives & False Negatives
2-NITROPROPANE
Method: 4437 Testid: 77076GM016
Link to Individual Chart

 newdate = 08/16/17 
 CENC_VAL = 0.339  newdate = 07/14/17 
 CENC_VAL = 0.234  newdate = 02/24/17 
 CENC_VAL = 0.282  newdate = 02/02/17 
 CENC_VAL = 0.249  newdate = 12/23/16 
 CENC_VAL = 0.432  newdate = 11/29/16 
 CENC_VAL = 0.635  newdate = 09/28/16 
 CENC_VAL = 0.440  newdate = 09/23/16 
 CENC_VAL = 0.743  newdate = 08/31/16 
 CENC_VAL = 0.436  newdate = 08/12/16 
 CENC_VAL = 0.231  newdate = 07/06/16 
 CENC_VAL = 0.638  newdate = 07/06/16 
 CENC_VAL = 0.228  newdate = 06/23/16 
 CENC_VAL = 0.237  newdate = 05/20/16 
 CENC_VAL = 0.259  newdate = 04/09/16 
 CENC_VAL = 0.187  newdate = 03/22/16 
 CENC_VAL = 0.161  newdate = 01/22/16 
 CENC_VAL = 0.388  newdate = 08/16/17 
 REPORTING LEVEL = 0.12  newdate = 07/14/17 
 REPORTING LEVEL = 0.12  newdate = 07/14/17 
 REPORTING LEVEL = 0.12  newdate = 02/24/17 
 REPORTING LEVEL = 0.12  newdate = 02/24/17 
 REPORTING LEVEL = 0.12  newdate = 02/02/17 
 REPORTING LEVEL = 0.12  newdate = 02/02/17 
 REPORTING LEVEL = 0.12  newdate = 12/23/16 
 REPORTING LEVEL = 0.12  newdate = 12/23/16 
 REPORTING LEVEL = 0.12  newdate = 11/29/16 
 REPORTING LEVEL = 0.12  newdate = 11/29/16 
 REPORTING LEVEL = 0.12  newdate = 09/28/16 
 REPORTING LEVEL = 0.12  newdate = 09/28/16 
 REPORTING LEVEL = 0.12  newdate = 09/23/16 
 REPORTING LEVEL = 0.12  newdate = 09/23/16 
 REPORTING LEVEL = 0.12  newdate = 08/31/16 
 REPORTING LEVEL = 0.12  newdate = 08/31/16 
 REPORTING LEVEL = 0.12  newdate = 08/12/16 
 REPORTING LEVEL = 0.12  newdate = 08/12/16 
 REPORTING LEVEL = 0.12  newdate = 07/06/16 
 REPORTING LEVEL = 0.12  newdate = 07/06/16 
 REPORTING LEVEL = 0.12  newdate = 07/06/16 
 REPORTING LEVEL = 0.12  newdate = 07/06/16 
 REPORTING LEVEL = 0.12  newdate = 06/23/16 
 REPORTING LEVEL = 0.12  newdate = 06/23/16 
 REPORTING LEVEL = 0.12  newdate = 05/20/16 
 REPORTING LEVEL = 0.12  newdate = 05/20/16 
 REPORTING LEVEL = 0.12  newdate = 04/09/16 
 REPORTING LEVEL = 0.12  newdate = 04/09/16 
 REPORTING LEVEL = 0.12  newdate = 03/22/16 
 REPORTING LEVEL = 0.12  newdate = 03/22/16 
 REPORTING LEVEL = 0.12  newdate = 01/22/16 
 REPORTING LEVEL = 0.12
The SGPlot Procedure

back to table
Organic Blind Sample Program
False Positives & False Negatives
2-PENTANOL,_4-METHYL-
Method: 4437 Testid: 77113GM016
Link to Individual Chart

 newdate = 08/30/17 
 falsepos = 0.357  newdate = 08/16/17 
 falsepos = 0.541  newdate = 08/10/17 
 falsepos = 0.357  newdate = 08/01/17 
 CENC_VAL = 0.581  newdate = 06/24/17 
 CENC_VAL = 0.828  newdate = 06/13/17 
 CENC_VAL = 0.698  newdate = 04/27/17 
 CENC_VAL = 0.433  newdate = 03/24/17 
 CENC_VAL = 0.537  newdate = 03/09/17 
 CENC_VAL = 1.210  newdate = 02/24/17 
 CENC_VAL = 0.719  newdate = 02/02/17 
 CENC_VAL = 1.240  newdate = 02/02/17 
 CENC_VAL = 0.461  newdate = 01/03/17 
 CENC_VAL = 0.456  newdate = 12/05/16 
 CENC_VAL = 1.210  newdate = 11/29/16 
 CENC_VAL = 1.180  newdate = 11/18/16 
 CENC_VAL = 0.448  newdate = 11/02/16 
 CENC_VAL = 0.492  newdate = 10/07/16 
 CENC_VAL = 0.544  newdate = 09/28/16 
 CENC_VAL = 0.807  newdate = 09/08/16 
 CENC_VAL = 0.770  newdate = 09/08/16 
 CENC_VAL = 0.820  newdate = 08/18/16 
 CENC_VAL = 0.486  newdate = 08/12/16 
 CENC_VAL = 0.490  newdate = 04/28/16 
 CENC_VAL = 0.441  newdate = 03/22/16 
 CENC_VAL = 0.297  newdate = 02/12/16 
 CENC_VAL = 0.237  newdate = 08/30/17 
 REPORTING LEVEL = 0.2  newdate = 08/16/17 
 REPORTING LEVEL = 0.2  newdate = 08/16/17 
 REPORTING LEVEL = 0.2  newdate = 08/10/17 
 REPORTING LEVEL = 0.2  newdate = 08/10/17 
 REPORTING LEVEL = 0.2  newdate = 08/01/17 
 REPORTING LEVEL = 0.2  newdate = 08/01/17 
 REPORTING LEVEL = 0.2  newdate = 06/24/17 
 REPORTING LEVEL = 0.2  newdate = 06/24/17 
 REPORTING LEVEL = 0.2  newdate = 06/13/17 
 REPORTING LEVEL = 0.2  newdate = 06/13/17 
 REPORTING LEVEL = 0.2  newdate = 04/27/17 
 REPORTING LEVEL = 0.2  newdate = 04/27/17 
 REPORTING LEVEL = 0.2  newdate = 03/24/17 
 REPORTING LEVEL = 0.2  newdate = 03/24/17 
 REPORTING LEVEL = 0.2  newdate = 03/09/17 
 REPORTING LEVEL = 0.2  newdate = 03/09/17 
 REPORTING LEVEL = 0.2  newdate = 02/24/17 
 REPORTING LEVEL = 0.2  newdate = 02/24/17 
 REPORTING LEVEL = 0.2  newdate = 02/02/17 
 REPORTING LEVEL = 0.2  newdate = 02/02/17 
 REPORTING LEVEL = 0.2  newdate = 02/02/17 
 REPORTING LEVEL = 0.2  newdate = 02/02/17 
 REPORTING LEVEL = 0.2  newdate = 01/03/17 
 REPORTING LEVEL = 0.2  newdate = 01/03/17 
 REPORTING LEVEL = 0.2  newdate = 12/05/16 
 REPORTING LEVEL = 0.2  newdate = 12/05/16 
 REPORTING LEVEL = 0.2  newdate = 11/29/16 
 REPORTING LEVEL = 0.2  newdate = 11/29/16 
 REPORTING LEVEL = 0.2  newdate = 11/18/16 
 REPORTING LEVEL = 0.2  newdate = 11/18/16 
 REPORTING LEVEL = 0.2  newdate = 11/02/16 
 REPORTING LEVEL = 0.2  newdate = 11/02/16 
 REPORTING LEVEL = 0.2  newdate = 10/07/16 
 REPORTING LEVEL = 0.2  newdate = 10/07/16 
 REPORTING LEVEL = 0.2  newdate = 09/28/16 
 REPORTING LEVEL = 0.2  newdate = 09/28/16 
 REPORTING LEVEL = 0.2  newdate = 09/08/16 
 REPORTING LEVEL = 0.2  newdate = 09/08/16 
 REPORTING LEVEL = 0.2  newdate = 09/08/16 
 REPORTING LEVEL = 0.2  newdate = 09/08/16 
 REPORTING LEVEL = 0.2  newdate = 08/18/16 
 REPORTING LEVEL = 0.2  newdate = 08/18/16 
 REPORTING LEVEL = 0.2  newdate = 08/12/16 
 REPORTING LEVEL = 0.2  newdate = 08/12/16 
 REPORTING LEVEL = 0.2  newdate = 04/28/16 
 REPORTING LEVEL = 0.2  newdate = 04/28/16 
 REPORTING LEVEL = 0.2  newdate = 03/22/16 
 REPORTING LEVEL = 0.2  newdate = 03/22/16 
 REPORTING LEVEL = 0.2  newdate = 02/12/16 
 REPORTING LEVEL = 0.2
The SGPlot Procedure

False Positive & Negative Listing for 2-PENTANOL,_4-METHYL-

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Positive 20172150193 ChemService 6441300: 10 µl & ChemService 6441600: 10 µl & ChemService 6424500: 1 0.2 08/10/17 0.357 0
  20172230006 ChemService 6441300: 15 µl & Spex Organics BW170726021: 15 µl & ChemService 6424 0.2 08/16/17 0.541 0
  20172370006 ChemService 6441300: 10 µl & ChemService 6424500: 10 µl & Spex Organics BW170725 0.2 08/30/17 0.357 0

Updated 04/25/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
2-PROPEN-1-OL
Method: 4437 Testid: 68729GM016
Link to Individual Chart

 newdate = 08/30/17 
 CENC_VAL = 14.700  newdate = 08/16/17 
 CENC_VAL = 20.300  newdate = 08/10/17 
 CENC_VAL = 18.400  newdate = 08/01/17 
 CENC_VAL = 20.700  newdate = 06/24/17 
 CENC_VAL = 35.300  newdate = 06/13/17 
 CENC_VAL = 34.400  newdate = 04/27/17 
 CENC_VAL = 17.300  newdate = 03/24/17 
 CENC_VAL = 18.100  newdate = 03/09/17 
 CENC_VAL = 51.000  newdate = 02/24/17 
 CENC_VAL = 28.800  newdate = 02/02/17 
 CENC_VAL = 48.000  newdate = 02/02/17 
 CENC_VAL = 17.200  newdate = 01/03/17 
 CENC_VAL = 19.000  newdate = 12/05/16 
 CENC_VAL = 48.800  newdate = 11/29/16 
 CENC_VAL = 47.700  newdate = 11/18/16 
 CENC_VAL = 18.600  newdate = 11/10/16 
 CENC_VAL = 28.100  newdate = 11/02/16 
 CENC_VAL = 19.100  newdate = 10/07/16 
 CENC_VAL = 19.200  newdate = 09/28/16 
 CENC_VAL = 29.600  newdate = 09/08/16 
 CENC_VAL = 30.000  newdate = 09/08/16 
 CENC_VAL = 30.600  newdate = 08/18/16 
 CENC_VAL = 18.500  newdate = 08/12/16 
 CENC_VAL = 18.100  newdate = 07/29/16 
 CENC_VAL = 45.600  newdate = 07/14/16 
 CENC_VAL = 26.600  newdate = 07/06/16 
 CENC_VAL = 50.800  newdate = 06/29/16 
 CENC_VAL = 51.400  newdate = 06/03/16 
 CENC_VAL = 18.300  newdate = 05/21/16 
 CENC_VAL = 28.400  newdate = 05/20/16 
 CENC_VAL = 15.400  newdate = 04/28/16 
 CENC_VAL = 16.600  newdate = 03/22/16 
 CENC_VAL = 10.000  newdate = 02/12/16 
 CENC_VAL = 10.800  newdate = 08/30/17 
 REPORTING LEVEL = 7.8  newdate = 08/16/17 
 REPORTING LEVEL = 7.8  newdate = 08/16/17 
 REPORTING LEVEL = 7.8  newdate = 08/10/17 
 REPORTING LEVEL = 7.8  newdate = 08/10/17 
 REPORTING LEVEL = 7.8  newdate = 08/01/17 
 REPORTING LEVEL = 7.8  newdate = 08/01/17 
 REPORTING LEVEL = 7.8  newdate = 06/24/17 
 REPORTING LEVEL = 7.8  newdate = 06/24/17 
 REPORTING LEVEL = 7.8  newdate = 06/13/17 
 REPORTING LEVEL = 7.8  newdate = 06/13/17 
 REPORTING LEVEL = 7.8  newdate = 04/27/17 
 REPORTING LEVEL = 7.8  newdate = 04/27/17 
 REPORTING LEVEL = 7.8  newdate = 03/24/17 
 REPORTING LEVEL = 7.8  newdate = 03/24/17 
 REPORTING LEVEL = 7.8  newdate = 03/09/17 
 REPORTING LEVEL = 7.8  newdate = 03/09/17 
 REPORTING LEVEL = 7.8  newdate = 02/24/17 
 REPORTING LEVEL = 7.8  newdate = 02/24/17 
 REPORTING LEVEL = 7.8  newdate = 02/02/17 
 REPORTING LEVEL = 7.8  newdate = 02/02/17 
 REPORTING LEVEL = 7.8  newdate = 02/02/17 
 REPORTING LEVEL = 7.8  newdate = 02/02/17 
 REPORTING LEVEL = 7.8  newdate = 01/03/17 
 REPORTING LEVEL = 7.8  newdate = 01/03/17 
 REPORTING LEVEL = 7.8  newdate = 12/05/16 
 REPORTING LEVEL = 7.8  newdate = 12/05/16 
 REPORTING LEVEL = 7.8  newdate = 11/29/16 
 REPORTING LEVEL = 7.8  newdate = 11/29/16 
 REPORTING LEVEL = 7.8  newdate = 11/18/16 
 REPORTING LEVEL = 7.8  newdate = 11/18/16 
 REPORTING LEVEL = 7.8  newdate = 11/10/16 
 REPORTING LEVEL = 7.8  newdate = 11/10/16 
 REPORTING LEVEL = 7.8  newdate = 11/02/16 
 REPORTING LEVEL = 7.8  newdate = 11/02/16 
 REPORTING LEVEL = 7.8  newdate = 10/07/16 
 REPORTING LEVEL = 7.8  newdate = 10/07/16 
 REPORTING LEVEL = 7.8  newdate = 09/28/16 
 REPORTING LEVEL = 7.8  newdate = 09/28/16 
 REPORTING LEVEL = 7.8  newdate = 09/08/16 
 REPORTING LEVEL = 7.8  newdate = 09/08/16 
 REPORTING LEVEL = 7.8  newdate = 09/08/16 
 REPORTING LEVEL = 7.8  newdate = 09/08/16 
 REPORTING LEVEL = 7.8  newdate = 08/18/16 
 REPORTING LEVEL = 7.8  newdate = 08/18/16 
 REPORTING LEVEL = 7.8  newdate = 08/12/16 
 REPORTING LEVEL = 7.8  newdate = 08/12/16 
 REPORTING LEVEL = 7.8  newdate = 07/29/16 
 REPORTING LEVEL = 7.8  newdate = 07/29/16 
 REPORTING LEVEL = 7.8  newdate = 07/14/16 
 REPORTING LEVEL = 7.8  newdate = 07/14/16 
 REPORTING LEVEL = 7.8  newdate = 07/06/16 
 REPORTING LEVEL = 7.8  newdate = 07/06/16 
 REPORTING LEVEL = 7.8  newdate = 06/29/16 
 REPORTING LEVEL = 7.8  newdate = 06/29/16 
 REPORTING LEVEL = 7.8  newdate = 06/03/16 
 REPORTING LEVEL = 7.8  newdate = 06/03/16 
 REPORTING LEVEL = 7.8  newdate = 05/21/16 
 REPORTING LEVEL = 7.8  newdate = 05/21/16 
 REPORTING LEVEL = 7.8  newdate = 05/20/16 
 REPORTING LEVEL = 7.8  newdate = 05/20/16 
 REPORTING LEVEL = 7.8  newdate = 04/28/16 
 REPORTING LEVEL = 7.8  newdate = 04/28/16 
 REPORTING LEVEL = 7.8  newdate = 03/22/16 
 REPORTING LEVEL = 7.8  newdate = 03/22/16 
 REPORTING LEVEL = 7.8  newdate = 02/12/16 
 REPORTING LEVEL = 7.8
The SGPlot Procedure

back to table
Organic Blind Sample Program
False Positives & False Negatives
4-HEPTANONE,_2,6-DIMETHYL-
Method: 4437 Testid: 77419GM016
Link to Individual Chart

 newdate = 06/24/17 
 falsepos = 0.124  newdate = 07/29/16 
 falsepos = 0.0127  newdate = 07/06/16 
 falsepos = 0.0108  newdate = 08/16/17 
 CENC_VAL = 0.102  newdate = 08/01/17 
 CENC_VAL = 0.078  newdate = 07/14/17 
 CENC_VAL = 0.089  newdate = 06/13/17 
 CENC_VAL = 0.118  newdate = 04/27/17 
 CENC_VAL = 0.075  newdate = 03/24/17 
 CENC_VAL = 0.081  newdate = 03/10/17 
 CENC_VAL = 0.121  newdate = 03/09/17 
 CENC_VAL = 0.188  newdate = 02/24/17 
 CENC_VAL = 0.066  newdate = 02/02/17 
 CENC_VAL = 0.187  newdate = 01/24/17 
 CENC_VAL = 0.183  newdate = 01/14/17 
 CENC_VAL = 0.067  newdate = 12/23/16 
 CENC_VAL = 0.133  newdate = 12/05/16 
 CENC_VAL = 0.185  newdate = 11/18/16 
 CENC_VAL = 0.076  newdate = 11/10/16 
 CENC_VAL = 0.114  newdate = 10/21/16 
 CENC_VAL = 0.191  newdate = 10/07/16 
 CENC_VAL = 0.079  newdate = 09/23/16 
 CENC_VAL = 0.189  newdate = 09/08/16 
 CENC_VAL = 0.111  newdate = 08/31/16 
 CENC_VAL = 0.124  newdate = 08/18/16 
 CENC_VAL = 0.078  newdate = 08/11/16 
 CENC_VAL = 0.117  newdate = 07/27/16 
 CENC_VAL = 0.074  newdate = 07/14/16 
 CENC_VAL = 0.119  newdate = 07/06/16 
 CENC_VAL = 0.071  newdate = 06/29/16 
 CENC_VAL = 0.219  newdate = 06/23/16 
 CENC_VAL = 0.078  newdate = 06/03/16 
 CENC_VAL = 0.073  newdate = 04/28/16 
 CENC_VAL = 0.071  newdate = 03/22/16 
 CENC_VAL = 0.052  newdate = 02/12/16 
 CENC_VAL = 0.041  newdate = 08/16/17 
 REPORTING LEVEL = 0.032  newdate = 08/01/17 
 REPORTING LEVEL = 0.032  newdate = 08/01/17 
 REPORTING LEVEL = 0.032  newdate = 07/14/17 
 REPORTING LEVEL = 0.032  newdate = 07/14/17 
 REPORTING LEVEL = 0.032  newdate = 06/24/17 
 REPORTING LEVEL = 0.032  newdate = 06/24/17 
 REPORTING LEVEL = 0.032  newdate = 06/13/17 
 REPORTING LEVEL = 0.032  newdate = 06/13/17 
 REPORTING LEVEL = 0.032  newdate = 04/27/17 
 REPORTING LEVEL = 0.032  newdate = 04/27/17 
 REPORTING LEVEL = 0.032  newdate = 03/24/17 
 REPORTING LEVEL = 0.032  newdate = 03/24/17 
 REPORTING LEVEL = 0.032  newdate = 03/10/17 
 REPORTING LEVEL = 0.032  newdate = 03/10/17 
 REPORTING LEVEL = 0.032  newdate = 03/09/17 
 REPORTING LEVEL = 0.032  newdate = 03/09/17 
 REPORTING LEVEL = 0.032  newdate = 02/24/17 
 REPORTING LEVEL = 0.032  newdate = 02/24/17 
 REPORTING LEVEL = 0.032  newdate = 02/02/17 
 REPORTING LEVEL = 0.032  newdate = 02/02/17 
 REPORTING LEVEL = 0.032  newdate = 01/24/17 
 REPORTING LEVEL = 0.032  newdate = 01/24/17 
 REPORTING LEVEL = 0.032  newdate = 01/14/17 
 REPORTING LEVEL = 0.032  newdate = 01/14/17 
 REPORTING LEVEL = 0.032  newdate = 12/23/16 
 REPORTING LEVEL = 0.032  newdate = 12/23/16 
 REPORTING LEVEL = 0.032  newdate = 12/05/16 
 REPORTING LEVEL = 0.032  newdate = 12/05/16 
 REPORTING LEVEL = 0.032  newdate = 11/18/16 
 REPORTING LEVEL = 0.032  newdate = 11/18/16 
 REPORTING LEVEL = 0.032  newdate = 11/10/16 
 REPORTING LEVEL = 0.032  newdate = 11/10/16 
 REPORTING LEVEL = 0.032  newdate = 10/21/16 
 REPORTING LEVEL = 0.032  newdate = 10/21/16 
 REPORTING LEVEL = 0.032  newdate = 10/07/16 
 REPORTING LEVEL = 0.032  newdate = 10/07/16 
 REPORTING LEVEL = 0.032  newdate = 09/23/16 
 REPORTING LEVEL = 0.032  newdate = 09/23/16 
 REPORTING LEVEL = 0.032  newdate = 09/08/16 
 REPORTING LEVEL = 0.032  newdate = 09/08/16 
 REPORTING LEVEL = 0.032  newdate = 08/31/16 
 REPORTING LEVEL = 0.032  newdate = 08/31/16 
 REPORTING LEVEL = 0.032  newdate = 08/18/16 
 REPORTING LEVEL = 0.032  newdate = 08/18/16 
 REPORTING LEVEL = 0.032  newdate = 08/11/16 
 REPORTING LEVEL = 0.032  newdate = 08/11/16 
 REPORTING LEVEL = 0.032  newdate = 07/29/16 
 REPORTING LEVEL = 0.032  newdate = 07/29/16 
 REPORTING LEVEL = 0.032  newdate = 07/27/16 
 REPORTING LEVEL = 0.032  newdate = 07/27/16 
 REPORTING LEVEL = 0.032  newdate = 07/14/16 
 REPORTING LEVEL = 0.032  newdate = 07/14/16 
 REPORTING LEVEL = 0.032  newdate = 07/06/16 
 REPORTING LEVEL = 0.032  newdate = 07/06/16 
 REPORTING LEVEL = 0.032  newdate = 07/06/16 
 REPORTING LEVEL = 0.032  newdate = 07/06/16 
 REPORTING LEVEL = 0.032  newdate = 06/29/16 
 REPORTING LEVEL = 0.032  newdate = 06/29/16 
 REPORTING LEVEL = 0.032  newdate = 06/23/16 
 REPORTING LEVEL = 0.032  newdate = 06/23/16 
 REPORTING LEVEL = 0.032  newdate = 06/03/16 
 REPORTING LEVEL = 0.032  newdate = 06/03/16 
 REPORTING LEVEL = 0.032  newdate = 04/28/16 
 REPORTING LEVEL = 0.032  newdate = 04/28/16 
 REPORTING LEVEL = 0.032  newdate = 03/22/16 
 REPORTING LEVEL = 0.032  newdate = 03/22/16 
 REPORTING LEVEL = 0.032  newdate = 02/12/16 
 REPORTING LEVEL = 0.032  Y = 0
The SGPlot Procedure

False Positive & Negative Listing for 4-HEPTANONE,_2,6-DIMETHYL-

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Positive 20161880112 Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 0.032 07/06/16 0.0108 0
  20162100018 Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 0.032 07/29/16 0.0127 0
  20171720144 Supelco LC20145V: 25 µl & Abs 060916HVOC: 25 µl & Accu 216041225: 25 µl 0.032 06/24/17 0.124 0

Updated 04/25/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
ACETATE,_ETHYL
Method: 4437 Testid: 81585GM016
Link to Individual Chart

 newdate = 03/10/17 
 falseneg = -0.01  newdate = 12/05/16 
 falsepos = 0.402  newdate = 08/30/17 
 CENC_VAL = 0.100  newdate = 08/16/17 
 CENC_VAL = 0.195  newdate = 08/10/17 
 CENC_VAL = 0.117  newdate = 06/29/17 
 CENC_VAL = 0.194  newdate = 06/17/17 
 CENC_VAL = 0.220  newdate = 06/01/17 
 CENC_VAL = 0.127  newdate = 04/13/17 
 CENC_VAL = 0.201  newdate = 03/24/17 
 CENC_VAL = 0.162  newdate = 02/24/17 
 CENC_VAL = 0.137  newdate = 02/02/17 
 CENC_VAL = 0.123  newdate = 01/03/17 
 CENC_VAL = 0.124  newdate = 11/10/16 
 CENC_VAL = 0.270  newdate = 11/02/16 
 CENC_VAL = 0.130  newdate = 09/28/16 
 CENC_VAL = 0.230  newdate = 09/08/16 
 CENC_VAL = 0.251  newdate = 08/11/16 
 CENC_VAL = 0.190  newdate = 07/29/16 
 CENC_VAL = 0.363  newdate = 07/06/16 
 CENC_VAL = 0.425  newdate = 07/06/16 
 CENC_VAL = 0.155  newdate = 06/03/16 
 CENC_VAL = 0.166  newdate = 05/21/16 
 CENC_VAL = 0.317  newdate = 05/20/16 
 CENC_VAL = 0.217  newdate = 04/28/16 
 CENC_VAL = 0.143  newdate = 03/22/16 
 CENC_VAL = 0.105  newdate = 02/12/16 
 CENC_VAL = 0.077  newdate = 08/30/17 
 REPORTING LEVEL = 0.06  newdate = 08/16/17 
 REPORTING LEVEL = 0.06  newdate = 08/16/17 
 REPORTING LEVEL = 0.06  newdate = 08/10/17 
 REPORTING LEVEL = 0.06  newdate = 08/10/17 
 REPORTING LEVEL = 0.06  newdate = 06/29/17 
 REPORTING LEVEL = 0.06  newdate = 06/29/17 
 REPORTING LEVEL = 0.06  newdate = 06/17/17 
 REPORTING LEVEL = 0.06  newdate = 06/17/17 
 REPORTING LEVEL = 0.06  newdate = 06/01/17 
 REPORTING LEVEL = 0.06  newdate = 06/01/17 
 REPORTING LEVEL = 0.06  newdate = 04/13/17 
 REPORTING LEVEL = 0.06  newdate = 04/13/17 
 REPORTING LEVEL = 0.06  newdate = 03/24/17 
 REPORTING LEVEL = 0.06  newdate = 03/24/17 
 REPORTING LEVEL = 0.06  newdate = 03/10/17 
 REPORTING LEVEL = 0.06  newdate = 03/10/17 
 REPORTING LEVEL = 0.06  newdate = 02/24/17 
 REPORTING LEVEL = 0.06  newdate = 02/24/17 
 REPORTING LEVEL = 0.06  newdate = 02/02/17 
 REPORTING LEVEL = 0.06  newdate = 02/02/17 
 REPORTING LEVEL = 0.06  newdate = 01/03/17 
 REPORTING LEVEL = 0.06  newdate = 01/03/17 
 REPORTING LEVEL = 0.06  newdate = 12/05/16 
 REPORTING LEVEL = 0.06  newdate = 12/05/16 
 REPORTING LEVEL = 0.06  newdate = 11/10/16 
 REPORTING LEVEL = 0.06  newdate = 11/10/16 
 REPORTING LEVEL = 0.06  newdate = 11/02/16 
 REPORTING LEVEL = 0.06  newdate = 11/02/16 
 REPORTING LEVEL = 0.06  newdate = 09/28/16 
 REPORTING LEVEL = 0.06  newdate = 09/28/16 
 REPORTING LEVEL = 0.06  newdate = 09/08/16 
 REPORTING LEVEL = 0.06  newdate = 09/08/16 
 REPORTING LEVEL = 0.06  newdate = 08/11/16 
 REPORTING LEVEL = 0.06  newdate = 08/11/16 
 REPORTING LEVEL = 0.06  newdate = 07/29/16 
 REPORTING LEVEL = 0.06  newdate = 07/29/16 
 REPORTING LEVEL = 0.06  newdate = 07/06/16 
 REPORTING LEVEL = 0.06  newdate = 07/06/16 
 REPORTING LEVEL = 0.06  newdate = 07/06/16 
 REPORTING LEVEL = 0.06  newdate = 07/06/16 
 REPORTING LEVEL = 0.06  newdate = 06/03/16 
 REPORTING LEVEL = 0.06  newdate = 06/03/16 
 REPORTING LEVEL = 0.06  newdate = 05/21/16 
 REPORTING LEVEL = 0.06  newdate = 05/21/16 
 REPORTING LEVEL = 0.06  newdate = 05/20/16 
 REPORTING LEVEL = 0.06  newdate = 05/20/16 
 REPORTING LEVEL = 0.06  newdate = 04/28/16 
 REPORTING LEVEL = 0.06  newdate = 04/28/16 
 REPORTING LEVEL = 0.06  newdate = 03/22/16 
 REPORTING LEVEL = 0.06  newdate = 03/22/16 
 REPORTING LEVEL = 0.06  newdate = 02/12/16 
 REPORTING LEVEL = 0.06  Y = 0
The SGPlot Procedure

False Positive & Negative Listing for ACETATE,_ETHYL

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20170680005 Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & Accu 216041225: 25 µl 0.06 03/10/17 < 0.06 0.2505
False Positive 20163370003 Abs 060916HVOC: 40 µl & Phenova B20160303: 40 µl 0.06 12/05/16 0.402 0

Updated 04/25/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
ACETATE,_ISOBUTYL
Method: 4437 Testid: 77201GM016
Link to Individual Chart

 newdate = 03/10/17 
 falseneg = -0.01  newdate = 06/23/16 
 falsepos = 0.0572  newdate = 08/30/17 
 CENC_VAL = 0.050  newdate = 08/16/17 
 CENC_VAL = 0.078  newdate = 08/10/17 
 CENC_VAL = 0.055  newdate = 07/14/17 
 CENC_VAL = 0.071  newdate = 06/24/17 
 CENC_VAL = 0.109  newdate = 06/17/17 
 CENC_VAL = 0.098  newdate = 06/01/17 
 CENC_VAL = 0.060  newdate = 04/27/17 
 CENC_VAL = 0.057  newdate = 04/13/17 
 CENC_VAL = 0.084  newdate = 03/24/17 
 CENC_VAL = 0.085  newdate = 02/24/17 
 CENC_VAL = 0.074  newdate = 02/02/17 
 CENC_VAL = 0.179  newdate = 02/02/17 
 CENC_VAL = 0.071  newdate = 01/03/17 
 CENC_VAL = 0.058  newdate = 12/23/16 
 CENC_VAL = 0.090  newdate = 11/18/16 
 CENC_VAL = 0.071  newdate = 11/10/16 
 CENC_VAL = 0.142  newdate = 11/02/16 
 CENC_VAL = 0.070  newdate = 10/21/16 
 CENC_VAL = 0.123  newdate = 09/28/16 
 CENC_VAL = 0.113  newdate = 09/08/16 
 CENC_VAL = 0.097  newdate = 08/11/16 
 CENC_VAL = 0.090  newdate = 07/29/16 
 CENC_VAL = 0.191  newdate = 07/27/16 
 CENC_VAL = 0.060  newdate = 07/14/16 
 CENC_VAL = 0.129  newdate = 07/06/16 
 CENC_VAL = 0.223  newdate = 07/06/16 
 CENC_VAL = 0.047  newdate = 06/03/16 
 CENC_VAL = 0.075  newdate = 05/21/16 
 CENC_VAL = 0.141  newdate = 05/20/16 
 CENC_VAL = 0.081  newdate = 04/09/16 
 CENC_VAL = 0.043  newdate = 03/22/16 
 CENC_VAL = 0.039  newdate = 01/22/16 
 CENC_VAL = 0.092  newdate = 08/30/17 
 REPORTING LEVEL = 0.028  newdate = 08/16/17 
 REPORTING LEVEL = 0.028  newdate = 08/16/17 
 REPORTING LEVEL = 0.028  newdate = 08/10/17 
 REPORTING LEVEL = 0.028  newdate = 08/10/17 
 REPORTING LEVEL = 0.028  newdate = 07/14/17 
 REPORTING LEVEL = 0.028  newdate = 07/14/17 
 REPORTING LEVEL = 0.028  newdate = 06/24/17 
 REPORTING LEVEL = 0.028  newdate = 06/24/17 
 REPORTING LEVEL = 0.028  newdate = 06/17/17 
 REPORTING LEVEL = 0.028  newdate = 06/17/17 
 REPORTING LEVEL = 0.028  newdate = 06/01/17 
 REPORTING LEVEL = 0.028  newdate = 06/01/17 
 REPORTING LEVEL = 0.028  newdate = 04/27/17 
 REPORTING LEVEL = 0.028  newdate = 04/27/17 
 REPORTING LEVEL = 0.028  newdate = 04/13/17 
 REPORTING LEVEL = 0.028  newdate = 04/13/17 
 REPORTING LEVEL = 0.028  newdate = 03/24/17 
 REPORTING LEVEL = 0.028  newdate = 03/24/17 
 REPORTING LEVEL = 0.028  newdate = 03/10/17 
 REPORTING LEVEL = 0.028  newdate = 03/10/17 
 REPORTING LEVEL = 0.028  newdate = 02/24/17 
 REPORTING LEVEL = 0.028  newdate = 02/24/17 
 REPORTING LEVEL = 0.028  newdate = 02/02/17 
 REPORTING LEVEL = 0.028  newdate = 02/02/17 
 REPORTING LEVEL = 0.028  newdate = 02/02/17 
 REPORTING LEVEL = 0.028  newdate = 02/02/17 
 REPORTING LEVEL = 0.028  newdate = 01/03/17 
 REPORTING LEVEL = 0.028  newdate = 01/03/17 
 REPORTING LEVEL = 0.028  newdate = 12/23/16 
 REPORTING LEVEL = 0.028  newdate = 12/23/16 
 REPORTING LEVEL = 0.028  newdate = 11/18/16 
 REPORTING LEVEL = 0.028  newdate = 11/18/16 
 REPORTING LEVEL = 0.028  newdate = 11/10/16 
 REPORTING LEVEL = 0.028  newdate = 11/10/16 
 REPORTING LEVEL = 0.028  newdate = 11/02/16 
 REPORTING LEVEL = 0.028  newdate = 11/02/16 
 REPORTING LEVEL = 0.028  newdate = 10/21/16 
 REPORTING LEVEL = 0.028  newdate = 10/21/16 
 REPORTING LEVEL = 0.028  newdate = 09/28/16 
 REPORTING LEVEL = 0.028  newdate = 09/28/16 
 REPORTING LEVEL = 0.028  newdate = 09/08/16 
 REPORTING LEVEL = 0.028  newdate = 09/08/16 
 REPORTING LEVEL = 0.028  newdate = 08/11/16 
 REPORTING LEVEL = 0.028  newdate = 08/11/16 
 REPORTING LEVEL = 0.028  newdate = 07/29/16 
 REPORTING LEVEL = 0.028  newdate = 07/29/16 
 REPORTING LEVEL = 0.028  newdate = 07/27/16 
 REPORTING LEVEL = 0.028  newdate = 07/27/16 
 REPORTING LEVEL = 0.028  newdate = 07/14/16 
 REPORTING LEVEL = 0.028  newdate = 07/14/16 
 REPORTING LEVEL = 0.028  newdate = 07/06/16 
 REPORTING LEVEL = 0.028  newdate = 07/06/16 
 REPORTING LEVEL = 0.028  newdate = 07/06/16 
 REPORTING LEVEL = 0.028  newdate = 07/06/16 
 REPORTING LEVEL = 0.028  newdate = 06/23/16 
 REPORTING LEVEL = 0.028  newdate = 06/23/16 
 REPORTING LEVEL = 0.028  newdate = 06/03/16 
 REPORTING LEVEL = 0.028  newdate = 06/03/16 
 REPORTING LEVEL = 0.028  newdate = 05/21/16 
 REPORTING LEVEL = 0.028  newdate = 05/21/16 
 REPORTING LEVEL = 0.028  newdate = 05/20/16 
 REPORTING LEVEL = 0.028  newdate = 05/20/16 
 REPORTING LEVEL = 0.028  newdate = 04/09/16 
 REPORTING LEVEL = 0.028  newdate = 04/09/16 
 REPORTING LEVEL = 0.028  newdate = 03/22/16 
 REPORTING LEVEL = 0.028  newdate = 03/22/16 
 REPORTING LEVEL = 0.028  newdate = 01/22/16 
 REPORTING LEVEL = 0.028  Y = 0
The SGPlot Procedure

False Positive & Negative Listing for ACETATE,_ISOBUTYL

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20170680005 Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & Accu 216041225: 25 µl 0.028 03/10/17 < 0.028 0.11485
False Positive 20161680364   0.028 06/23/16 0.0572 0

Updated 04/25/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
ACETATE,_ISOPROPYL
Method: 4437 Testid: 45013GM016
Link to Individual Chart

 newdate = 03/10/17 
 falseneg = -0.01  newdate = 06/23/16 
 falsepos = 0.0177  newdate = 08/30/17 
 CENC_VAL = 0.021  newdate = 08/16/17 
 CENC_VAL = 0.033  newdate = 08/10/17 
 CENC_VAL = 0.021  newdate = 07/14/17 
 CENC_VAL = 0.024  newdate = 06/24/17 
 CENC_VAL = 0.040  newdate = 06/17/17 
 CENC_VAL = 0.035  newdate = 06/01/17 
 CENC_VAL = 0.023  newdate = 04/27/17 
 CENC_VAL = 0.018  newdate = 04/13/17 
 CENC_VAL = 0.031  newdate = 03/24/17 
 CENC_VAL = 0.031  newdate = 02/24/17 
 CENC_VAL = 0.024  newdate = 02/02/17 
 CENC_VAL = 0.058  newdate = 02/02/17 
 CENC_VAL = 0.021  newdate = 01/03/17 
 CENC_VAL = 0.020  newdate = 12/23/16 
 CENC_VAL = 0.030  newdate = 11/18/16 
 CENC_VAL = 0.024  newdate = 11/10/16 
 CENC_VAL = 0.049  newdate = 11/02/16 
 CENC_VAL = 0.023  newdate = 10/21/16 
 CENC_VAL = 0.059  newdate = 09/28/16 
 CENC_VAL = 0.045  newdate = 09/08/16 
 CENC_VAL = 0.034  newdate = 08/11/16 
 CENC_VAL = 0.031  newdate = 07/29/16 
 CENC_VAL = 0.050  newdate = 07/27/16 
 CENC_VAL = 0.020  newdate = 07/14/16 
 CENC_VAL = 0.034  newdate = 07/06/16 
 CENC_VAL = 0.046  newdate = 07/06/16 
 CENC_VAL = 0.016  newdate = 06/03/16 
 CENC_VAL = 0.023  newdate = 05/26/16 
 CENC_VAL = 0.031  newdate = 05/26/16 
 CENC_VAL = 0.020  newdate = 04/28/16 
 CENC_VAL = 0.024  newdate = 04/09/16 
 CENC_VAL = 0.017  newdate = 02/12/16 
 CENC_VAL = 0.017  newdate = 01/22/16 
 CENC_VAL = 0.042  newdate = 08/30/17 
 REPORTING LEVEL = 0.01  newdate = 08/16/17 
 REPORTING LEVEL = 0.01  newdate = 08/16/17 
 REPORTING LEVEL = 0.01  newdate = 08/10/17 
 REPORTING LEVEL = 0.01  newdate = 08/10/17 
 REPORTING LEVEL = 0.01  newdate = 07/14/17 
 REPORTING LEVEL = 0.01  newdate = 07/14/17 
 REPORTING LEVEL = 0.01  newdate = 06/24/17 
 REPORTING LEVEL = 0.01  newdate = 06/24/17 
 REPORTING LEVEL = 0.01  newdate = 06/17/17 
 REPORTING LEVEL = 0.01  newdate = 06/17/17 
 REPORTING LEVEL = 0.01  newdate = 06/01/17 
 REPORTING LEVEL = 0.01  newdate = 06/01/17 
 REPORTING LEVEL = 0.01  newdate = 04/27/17 
 REPORTING LEVEL = 0.01  newdate = 04/27/17 
 REPORTING LEVEL = 0.01  newdate = 04/13/17 
 REPORTING LEVEL = 0.01  newdate = 04/13/17 
 REPORTING LEVEL = 0.01  newdate = 03/24/17 
 REPORTING LEVEL = 0.01  newdate = 03/24/17 
 REPORTING LEVEL = 0.01  newdate = 03/10/17 
 REPORTING LEVEL = 0.01  newdate = 03/10/17 
 REPORTING LEVEL = 0.01  newdate = 02/24/17 
 REPORTING LEVEL = 0.01  newdate = 02/24/17 
 REPORTING LEVEL = 0.01  newdate = 02/02/17 
 REPORTING LEVEL = 0.01  newdate = 02/02/17 
 REPORTING LEVEL = 0.01  newdate = 02/02/17 
 REPORTING LEVEL = 0.01  newdate = 02/02/17 
 REPORTING LEVEL = 0.01  newdate = 01/03/17 
 REPORTING LEVEL = 0.01  newdate = 01/03/17 
 REPORTING LEVEL = 0.01  newdate = 12/23/16 
 REPORTING LEVEL = 0.01  newdate = 12/23/16 
 REPORTING LEVEL = 0.01  newdate = 11/18/16 
 REPORTING LEVEL = 0.01  newdate = 11/18/16 
 REPORTING LEVEL = 0.01  newdate = 11/10/16 
 REPORTING LEVEL = 0.01  newdate = 11/10/16 
 REPORTING LEVEL = 0.01  newdate = 11/02/16 
 REPORTING LEVEL = 0.01  newdate = 11/02/16 
 REPORTING LEVEL = 0.01  newdate = 10/21/16 
 REPORTING LEVEL = 0.01  newdate = 10/21/16 
 REPORTING LEVEL = 0.01  newdate = 09/28/16 
 REPORTING LEVEL = 0.01  newdate = 09/28/16 
 REPORTING LEVEL = 0.01  newdate = 09/08/16 
 REPORTING LEVEL = 0.01  newdate = 09/08/16 
 REPORTING LEVEL = 0.01  newdate = 08/11/16 
 REPORTING LEVEL = 0.01  newdate = 08/11/16 
 REPORTING LEVEL = 0.01  newdate = 07/29/16 
 REPORTING LEVEL = 0.01  newdate = 07/29/16 
 REPORTING LEVEL = 0.01  newdate = 07/27/16 
 REPORTING LEVEL = 0.01  newdate = 07/27/16 
 REPORTING LEVEL = 0.01  newdate = 07/14/16 
 REPORTING LEVEL = 0.01  newdate = 07/14/16 
 REPORTING LEVEL = 0.01  newdate = 07/06/16 
 REPORTING LEVEL = 0.01  newdate = 07/06/16 
 REPORTING LEVEL = 0.01  newdate = 07/06/16 
 REPORTING LEVEL = 0.01  newdate = 07/06/16 
 REPORTING LEVEL = 0.01  newdate = 06/23/16 
 REPORTING LEVEL = 0.01  newdate = 06/23/16 
 REPORTING LEVEL = 0.01  newdate = 06/03/16 
 REPORTING LEVEL = 0.01  newdate = 06/03/16 
 REPORTING LEVEL = 0.01  newdate = 05/26/16 
 REPORTING LEVEL = 0.01  newdate = 05/26/16 
 REPORTING LEVEL = 0.01  newdate = 05/26/16 
 REPORTING LEVEL = 0.01  newdate = 05/26/16 
 REPORTING LEVEL = 0.01  newdate = 04/28/16 
 REPORTING LEVEL = 0.01  newdate = 04/28/16 
 REPORTING LEVEL = 0.01  newdate = 04/09/16 
 REPORTING LEVEL = 0.01  newdate = 04/09/16 
 REPORTING LEVEL = 0.01  newdate = 02/12/16 
 REPORTING LEVEL = 0.01  newdate = 02/12/16 
 REPORTING LEVEL = 0.01  newdate = 01/22/16 
 REPORTING LEVEL = 0.01  Y = 0
The SGPlot Procedure

False Positive & Negative Listing for ACETATE,_ISOPROPYL

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20170680005 Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & Accu 216041225: 25 µl 0.01 03/10/17 < 0.01 0.03975
False Positive 20161680364   0.01 06/23/16 0.0177 0

Updated 04/25/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
ACETATE,_PROPYL
Method: 4437 Testid: 45022GM016
Link to Individual Chart

 newdate = 03/10/17 
 falseneg = -0.01  newdate = 06/23/16 
 falsepos = 0.0728  newdate = 08/30/17 
 CENC_VAL = 0.056  newdate = 08/16/17 
 CENC_VAL = 0.087  newdate = 08/10/17 
 CENC_VAL = 0.062  newdate = 07/14/17 
 CENC_VAL = 0.080  newdate = 06/29/17 
 CENC_VAL = 0.121  newdate = 06/17/17 
 CENC_VAL = 0.129  newdate = 06/01/17 
 CENC_VAL = 0.068  newdate = 04/27/17 
 CENC_VAL = 0.065  newdate = 04/13/17 
 CENC_VAL = 0.105  newdate = 03/24/17 
 CENC_VAL = 0.081  newdate = 02/24/17 
 CENC_VAL = 0.075  newdate = 02/02/17 
 CENC_VAL = 0.190  newdate = 02/02/17 
 CENC_VAL = 0.068  newdate = 01/03/17 
 CENC_VAL = 0.061  newdate = 12/23/16 
 CENC_VAL = 0.112  newdate = 11/18/16 
 CENC_VAL = 0.067  newdate = 11/10/16 
 CENC_VAL = 0.143  newdate = 11/02/16 
 CENC_VAL = 0.083  newdate = 10/21/16 
 CENC_VAL = 0.214  newdate = 09/28/16 
 CENC_VAL = 0.150  newdate = 09/08/16 
 CENC_VAL = 0.121  newdate = 08/11/16 
 CENC_VAL = 0.115  newdate = 07/29/16 
 CENC_VAL = 0.184  newdate = 07/27/16 
 CENC_VAL = 0.076  newdate = 07/14/16 
 CENC_VAL = 0.114  newdate = 07/06/16 
 CENC_VAL = 0.154  newdate = 07/06/16 
 CENC_VAL = 0.069  newdate = 06/03/16 
 CENC_VAL = 0.076  newdate = 05/21/16 
 CENC_VAL = 0.138  newdate = 05/20/16 
 CENC_VAL = 0.093  newdate = 04/28/16 
 CENC_VAL = 0.081  newdate = 04/09/16 
 CENC_VAL = 0.061  newdate = 02/12/16 
 CENC_VAL = 0.044  newdate = 01/22/16 
 CENC_VAL = 0.118  newdate = 08/30/17 
 REPORTING LEVEL = 0.032  newdate = 08/16/17 
 REPORTING LEVEL = 0.032  newdate = 08/16/17 
 REPORTING LEVEL = 0.032  newdate = 08/10/17 
 REPORTING LEVEL = 0.032  newdate = 08/10/17 
 REPORTING LEVEL = 0.032  newdate = 07/14/17 
 REPORTING LEVEL = 0.032  newdate = 07/14/17 
 REPORTING LEVEL = 0.032  newdate = 06/29/17 
 REPORTING LEVEL = 0.032  newdate = 06/29/17 
 REPORTING LEVEL = 0.032  newdate = 06/17/17 
 REPORTING LEVEL = 0.032  newdate = 06/17/17 
 REPORTING LEVEL = 0.032  newdate = 06/01/17 
 REPORTING LEVEL = 0.032  newdate = 06/01/17 
 REPORTING LEVEL = 0.032  newdate = 04/27/17 
 REPORTING LEVEL = 0.032  newdate = 04/27/17 
 REPORTING LEVEL = 0.032  newdate = 04/13/17 
 REPORTING LEVEL = 0.032  newdate = 04/13/17 
 REPORTING LEVEL = 0.032  newdate = 03/24/17 
 REPORTING LEVEL = 0.032  newdate = 03/24/17 
 REPORTING LEVEL = 0.032  newdate = 03/10/17 
 REPORTING LEVEL = 0.032  newdate = 03/10/17 
 REPORTING LEVEL = 0.032  newdate = 02/24/17 
 REPORTING LEVEL = 0.032  newdate = 02/24/17 
 REPORTING LEVEL = 0.032  newdate = 02/02/17 
 REPORTING LEVEL = 0.032  newdate = 02/02/17 
 REPORTING LEVEL = 0.032  newdate = 02/02/17 
 REPORTING LEVEL = 0.032  newdate = 02/02/17 
 REPORTING LEVEL = 0.032  newdate = 01/03/17 
 REPORTING LEVEL = 0.032  newdate = 01/03/17 
 REPORTING LEVEL = 0.032  newdate = 12/23/16 
 REPORTING LEVEL = 0.032  newdate = 12/23/16 
 REPORTING LEVEL = 0.032  newdate = 11/18/16 
 REPORTING LEVEL = 0.032  newdate = 11/18/16 
 REPORTING LEVEL = 0.032  newdate = 11/10/16 
 REPORTING LEVEL = 0.032  newdate = 11/10/16 
 REPORTING LEVEL = 0.032  newdate = 11/02/16 
 REPORTING LEVEL = 0.032  newdate = 11/02/16 
 REPORTING LEVEL = 0.032  newdate = 10/21/16 
 REPORTING LEVEL = 0.032  newdate = 10/21/16 
 REPORTING LEVEL = 0.032  newdate = 09/28/16 
 REPORTING LEVEL = 0.032  newdate = 09/28/16 
 REPORTING LEVEL = 0.032  newdate = 09/08/16 
 REPORTING LEVEL = 0.032  newdate = 09/08/16 
 REPORTING LEVEL = 0.032  newdate = 08/11/16 
 REPORTING LEVEL = 0.032  newdate = 08/11/16 
 REPORTING LEVEL = 0.032  newdate = 07/29/16 
 REPORTING LEVEL = 0.032  newdate = 07/29/16 
 REPORTING LEVEL = 0.032  newdate = 07/27/16 
 REPORTING LEVEL = 0.032  newdate = 07/27/16 
 REPORTING LEVEL = 0.032  newdate = 07/14/16 
 REPORTING LEVEL = 0.032  newdate = 07/14/16 
 REPORTING LEVEL = 0.032  newdate = 07/06/16 
 REPORTING LEVEL = 0.032  newdate = 07/06/16 
 REPORTING LEVEL = 0.032  newdate = 07/06/16 
 REPORTING LEVEL = 0.032  newdate = 07/06/16 
 REPORTING LEVEL = 0.032  newdate = 06/23/16 
 REPORTING LEVEL = 0.032  newdate = 06/23/16 
 REPORTING LEVEL = 0.032  newdate = 06/03/16 
 REPORTING LEVEL = 0.032  newdate = 06/03/16 
 REPORTING LEVEL = 0.032  newdate = 05/21/16 
 REPORTING LEVEL = 0.032  newdate = 05/21/16 
 REPORTING LEVEL = 0.032  newdate = 05/20/16 
 REPORTING LEVEL = 0.032  newdate = 05/20/16 
 REPORTING LEVEL = 0.032  newdate = 04/28/16 
 REPORTING LEVEL = 0.032  newdate = 04/28/16 
 REPORTING LEVEL = 0.032  newdate = 04/09/16 
 REPORTING LEVEL = 0.032  newdate = 04/09/16 
 REPORTING LEVEL = 0.032  newdate = 02/12/16 
 REPORTING LEVEL = 0.032  newdate = 02/12/16 
 REPORTING LEVEL = 0.032  newdate = 01/22/16 
 REPORTING LEVEL = 0.032  Y = 0
The SGPlot Procedure

False Positive & Negative Listing for ACETATE,_PROPYL

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20170680005 Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & Accu 216041225: 25 µl 0.032 03/10/17 < 0.032 0.1339
False Positive 20161680364   0.032 06/23/16 0.0728 0

Updated 04/25/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
ACETONITRILE
Method: 4437 Testid: 76997GM016
Link to Individual Chart

 newdate = 09/08/16 
 falsepos = 0.45  newdate = 04/28/16 
 falsepos = 0.18  newdate = 02/12/16 
 falsepos = 0.16  newdate = 08/16/17 
 CENC_VAL = 2.540  newdate = 07/14/17 
 CENC_VAL = 2.420  newdate = 02/24/17 
 CENC_VAL = 3.570  newdate = 12/23/16 
 CENC_VAL = 5.590  newdate = 11/29/16 
 CENC_VAL = 8.510  newdate = 09/28/16 
 CENC_VAL = 9.960  newdate = 09/23/16 
 CENC_VAL = 8.040  newdate = 08/12/16 
 CENC_VAL = 3.120  newdate = 07/15/16 
 CENC_VAL = 7.620  newdate = 07/06/16 
 CENC_VAL = 3.490  newdate = 04/09/16 
 CENC_VAL = 1.310  newdate = 03/22/16 
 CENC_VAL = 1.400  newdate = 01/22/16 
 CENC_VAL = 3.200  newdate = 08/16/17 
 REPORTING LEVEL = 0.8  newdate = 07/14/17 
 REPORTING LEVEL = 0.8  newdate = 07/14/17 
 REPORTING LEVEL = 0.8  newdate = 02/24/17 
 REPORTING LEVEL = 0.8  newdate = 02/24/17 
 REPORTING LEVEL = 0.8  newdate = 12/23/16 
 REPORTING LEVEL = 0.8  newdate = 12/23/16 
 REPORTING LEVEL = 0.8  newdate = 11/29/16 
 REPORTING LEVEL = 0.8  newdate = 11/29/16 
 REPORTING LEVEL = 0.8  newdate = 09/28/16 
 REPORTING LEVEL = 0.8  newdate = 09/28/16 
 REPORTING LEVEL = 0.8  newdate = 09/23/16 
 REPORTING LEVEL = 0.8  newdate = 09/23/16 
 REPORTING LEVEL = 0.8  newdate = 09/08/16 
 REPORTING LEVEL = 0.8  newdate = 09/08/16 
 REPORTING LEVEL = 0.8  newdate = 08/12/16 
 REPORTING LEVEL = 0.8  newdate = 08/12/16 
 REPORTING LEVEL = 0.8  newdate = 07/15/16 
 REPORTING LEVEL = 0.8  newdate = 07/15/16 
 REPORTING LEVEL = 0.8  newdate = 07/06/16 
 REPORTING LEVEL = 0.8  newdate = 07/06/16 
 REPORTING LEVEL = 0.8  newdate = 04/28/16 
 REPORTING LEVEL = 0.8  newdate = 04/28/16 
 REPORTING LEVEL = 0.8  newdate = 04/09/16 
 REPORTING LEVEL = 0.8  newdate = 04/09/16 
 REPORTING LEVEL = 0.8  newdate = 03/22/16 
 REPORTING LEVEL = 0.8  newdate = 03/22/16 
 REPORTING LEVEL = 0.8  newdate = 02/12/16 
 REPORTING LEVEL = 0.8  newdate = 02/12/16 
 REPORTING LEVEL = 0.8  newdate = 01/22/16 
 REPORTING LEVEL = 0.8  Y = 0
The SGPlot Procedure

False Positive & Negative Listing for ACETONITRILE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Positive 20160350048 ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl 0.8 02/12/16 0.16 0
  20161190073 ChemService 3818700: 15 µl & Supelco LC13544: 15 µl 0.8 04/28/16 0.18 0
  20162520005 Abs 060916HVOC: 25 µl & Phenova B20160303: 25 µl & NSI 041416HVOC: 25 µl 0.8 09/08/16 0.45 0

Updated 04/25/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
ACROLEIN
Method: 4437 Testid: 34210GM016
Link to Individual Chart

 newdate = 03/22/16 
 CENC_VAL = 1.500  newdate = 01/22/16 
 CENC_VAL = 9.500  newdate = 03/22/16 
 REPORTING LEVEL = 2  newdate = 01/22/16 
 REPORTING LEVEL = 2
The SGPlot Procedure

back to table
Organic Blind Sample Program
False Positives & False Negatives
ALPHA-TERPINEOL
Method: 4437 Testid: 68730GM016
Link to Individual Chart

 newdate = 08/30/17 
 CENC_VAL = 10.800  newdate = 08/10/17 
 CENC_VAL = 9.510  newdate = 07/14/17 
 CENC_VAL = 9.310  newdate = 02/24/17 
 CENC_VAL = 11.000  newdate = 02/02/17 
 CENC_VAL = 10.700  newdate = 12/23/16 
 CENC_VAL = 21.900  newdate = 11/29/16 
 CENC_VAL = 24.300  newdate = 09/28/16 
 CENC_VAL = 19.900  newdate = 09/23/16 
 CENC_VAL = 32.500  newdate = 08/31/16 
 CENC_VAL = 20.300  newdate = 08/12/16 
 CENC_VAL = 11.600  newdate = 07/06/16 
 CENC_VAL = 36.500  newdate = 07/06/16 
 CENC_VAL = 11.000  newdate = 06/23/16 
 CENC_VAL = 7.270  newdate = 05/20/16 
 CENC_VAL = 14.400  newdate = 04/28/16 
 CENC_VAL = 15.600  newdate = 04/09/16 
 CENC_VAL = 7.300  newdate = 02/12/16 
 CENC_VAL = 7.500  newdate = 01/22/16 
 CENC_VAL = 20.800  newdate = 08/30/17 
 REPORTING LEVEL = 6.8  newdate = 08/10/17 
 REPORTING LEVEL = 6.8  newdate = 08/10/17 
 REPORTING LEVEL = 6.8  newdate = 07/14/17 
 REPORTING LEVEL = 6.8  newdate = 07/14/17 
 REPORTING LEVEL = 6.8  newdate = 02/24/17 
 REPORTING LEVEL = 6.8  newdate = 02/24/17 
 REPORTING LEVEL = 6.8  newdate = 02/02/17 
 REPORTING LEVEL = 6.8  newdate = 02/02/17 
 REPORTING LEVEL = 6.8  newdate = 12/23/16 
 REPORTING LEVEL = 6.8  newdate = 12/23/16 
 REPORTING LEVEL = 6.8  newdate = 11/29/16 
 REPORTING LEVEL = 6.8  newdate = 11/29/16 
 REPORTING LEVEL = 6.8  newdate = 09/28/16 
 REPORTING LEVEL = 6.8  newdate = 09/28/16 
 REPORTING LEVEL = 6.8  newdate = 09/23/16 
 REPORTING LEVEL = 6.8  newdate = 09/23/16 
 REPORTING LEVEL = 6.8  newdate = 08/31/16 
 REPORTING LEVEL = 6.8  newdate = 08/31/16 
 REPORTING LEVEL = 6.8  newdate = 08/12/16 
 REPORTING LEVEL = 6.8  newdate = 08/12/16 
 REPORTING LEVEL = 6.8  newdate = 07/06/16 
 REPORTING LEVEL = 6.8  newdate = 07/06/16 
 REPORTING LEVEL = 6.8  newdate = 07/06/16 
 REPORTING LEVEL = 6.8  newdate = 07/06/16 
 REPORTING LEVEL = 6.8  newdate = 06/23/16 
 REPORTING LEVEL = 6.8  newdate = 06/23/16 
 REPORTING LEVEL = 6.8  newdate = 05/20/16 
 REPORTING LEVEL = 6.8  newdate = 05/20/16 
 REPORTING LEVEL = 6.8  newdate = 04/28/16 
 REPORTING LEVEL = 6.8  newdate = 04/28/16 
 REPORTING LEVEL = 6.8  newdate = 04/09/16 
 REPORTING LEVEL = 6.8  newdate = 04/09/16 
 REPORTING LEVEL = 6.8  newdate = 02/12/16 
 REPORTING LEVEL = 6.8  newdate = 02/12/16 
 REPORTING LEVEL = 6.8  newdate = 01/22/16 
 REPORTING LEVEL = 6.8
The SGPlot Procedure

back to table
Organic Blind Sample Program
False Positives & False Negatives
BUTANAL
Method: 4437 Testid: 68732GM016
Link to Individual Chart

 newdate = 08/10/17 
 falseneg = -0.01  newdate = 06/29/16 
 falsepos = 27.6  newdate = 08/30/17 
 CENC_VAL = 0.767  newdate = 06/24/17 
 CENC_VAL = 1.630  newdate = 06/13/17 
 CENC_VAL = 1.440  newdate = 04/27/17 
 CENC_VAL = 0.847  newdate = 03/24/17 
 CENC_VAL = 0.870  newdate = 03/09/17 
 CENC_VAL = 2.200  newdate = 02/24/17 
 CENC_VAL = 1.190  newdate = 02/02/17 
 CENC_VAL = 2.390  newdate = 02/02/17 
 CENC_VAL = 0.784  newdate = 01/03/17 
 CENC_VAL = 0.875  newdate = 12/05/16 
 CENC_VAL = 2.450  newdate = 11/29/16 
 CENC_VAL = 2.430  newdate = 11/18/16 
 CENC_VAL = 0.767  newdate = 11/02/16 
 CENC_VAL = 0.819  newdate = 10/07/16 
 CENC_VAL = 0.844  newdate = 09/28/16 
 CENC_VAL = 1.310  newdate = 09/08/16 
 CENC_VAL = 1.420  newdate = 09/08/16 
 CENC_VAL = 1.430  newdate = 08/18/16 
 CENC_VAL = 0.914  newdate = 08/12/16 
 CENC_VAL = 0.890  newdate = 04/09/16 
 CENC_VAL = 0.499  newdate = 03/22/16 
 CENC_VAL = 0.487  newdate = 01/22/16 
 CENC_VAL = 1.130  newdate = 08/30/17 
 REPORTING LEVEL = 0.38  newdate = 08/10/17 
 REPORTING LEVEL = 0.38  newdate = 08/10/17 
 REPORTING LEVEL = 0.38  newdate = 06/24/17 
 REPORTING LEVEL = 0.38  newdate = 06/24/17 
 REPORTING LEVEL = 0.38  newdate = 06/13/17 
 REPORTING LEVEL = 0.38  newdate = 06/13/17 
 REPORTING LEVEL = 0.38  newdate = 04/27/17 
 REPORTING LEVEL = 0.38  newdate = 04/27/17 
 REPORTING LEVEL = 0.38  newdate = 03/24/17 
 REPORTING LEVEL = 0.38  newdate = 03/24/17 
 REPORTING LEVEL = 0.38  newdate = 03/09/17 
 REPORTING LEVEL = 0.38  newdate = 03/09/17 
 REPORTING LEVEL = 0.38  newdate = 02/24/17 
 REPORTING LEVEL = 0.38  newdate = 02/24/17 
 REPORTING LEVEL = 0.38  newdate = 02/02/17 
 REPORTING LEVEL = 0.38  newdate = 02/02/17 
 REPORTING LEVEL = 0.38  newdate = 02/02/17 
 REPORTING LEVEL = 0.38  newdate = 02/02/17 
 REPORTING LEVEL = 0.38  newdate = 01/03/17 
 REPORTING LEVEL = 0.38  newdate = 01/03/17 
 REPORTING LEVEL = 0.38  newdate = 12/05/16 
 REPORTING LEVEL = 0.38  newdate = 12/05/16 
 REPORTING LEVEL = 0.38  newdate = 11/29/16 
 REPORTING LEVEL = 0.38  newdate = 11/29/16 
 REPORTING LEVEL = 0.38  newdate = 11/18/16 
 REPORTING LEVEL = 0.38  newdate = 11/18/16 
 REPORTING LEVEL = 0.38  newdate = 11/02/16 
 REPORTING LEVEL = 0.38  newdate = 11/02/16 
 REPORTING LEVEL = 0.38  newdate = 10/07/16 
 REPORTING LEVEL = 0.38  newdate = 10/07/16 
 REPORTING LEVEL = 0.38  newdate = 09/28/16 
 REPORTING LEVEL = 0.38  newdate = 09/28/16 
 REPORTING LEVEL = 0.38  newdate = 09/08/16 
 REPORTING LEVEL = 0.38  newdate = 09/08/16 
 REPORTING LEVEL = 0.38  newdate = 09/08/16 
 REPORTING LEVEL = 0.38  newdate = 09/08/16 
 REPORTING LEVEL = 0.38  newdate = 08/18/16 
 REPORTING LEVEL = 0.38  newdate = 08/18/16 
 REPORTING LEVEL = 0.38  newdate = 08/12/16 
 REPORTING LEVEL = 0.38  newdate = 08/12/16 
 REPORTING LEVEL = 0.38  newdate = 06/29/16 
 REPORTING LEVEL = 0.38  newdate = 06/29/16 
 REPORTING LEVEL = 0.38  newdate = 04/09/16 
 REPORTING LEVEL = 0.38  newdate = 04/09/16 
 REPORTING LEVEL = 0.38  newdate = 03/22/16 
 REPORTING LEVEL = 0.38  newdate = 03/22/16 
 REPORTING LEVEL = 0.38  newdate = 01/22/16 
 REPORTING LEVEL = 0.38  Y = 0
The SGPlot Procedure

False Positive & Negative Listing for BUTANAL

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20172150193 ChemService 6441300: 10 µl & ChemService 6441600: 10 µl & ChemService 6424500: 1 0.38 08/10/17 < 0.38 0.768
False Positive 20161740256 NSI 041516: 40 µl & ChemService 5082800: 40 µl 0.38 06/29/16 E 27.6 0

Updated 04/25/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
BUTANOL
Method: 4437 Testid: 77034GM016
Link to Individual Chart

 newdate = 08/16/17 
 falsepos = 0.96  newdate = 06/13/17 
 falsepos = 0.72  newdate = 04/27/17 
 falsepos = 1  newdate = 02/02/17 
 falsepos = 1.13  newdate = 11/10/16 
 falsepos = 0.89  newdate = 08/30/17 
 CENC_VAL = 1.210  newdate = 08/10/17 
 CENC_VAL = 1.820  newdate = 07/14/17 
 CENC_VAL = 2.180  newdate = 02/24/17 
 CENC_VAL = 1.990  newdate = 02/02/17 
 CENC_VAL = 1.910  newdate = 12/23/16 
 CENC_VAL = 3.870  newdate = 11/29/16 
 CENC_VAL = 5.330  newdate = 09/28/16 
 CENC_VAL = 2.960  newdate = 09/23/16 
 CENC_VAL = 4.670  newdate = 08/31/16 
 CENC_VAL = 2.910  newdate = 08/12/16 
 CENC_VAL = 1.710  newdate = 07/06/16 
 CENC_VAL = 5.250  newdate = 07/06/16 
 CENC_VAL = 1.420  newdate = 06/23/16 
 CENC_VAL = 0.960  newdate = 05/20/16 
 CENC_VAL = 1.850  newdate = 04/28/16 
 CENC_VAL = 1.350  newdate = 04/09/16 
 CENC_VAL = 1.220  newdate = 02/12/16 
 CENC_VAL = 1.120  newdate = 01/22/16 
 CENC_VAL = 2.940  newdate = 08/30/17 
 REPORTING LEVEL = 0.8  newdate = 08/16/17 
 REPORTING LEVEL = 0.8  newdate = 08/16/17 
 REPORTING LEVEL = 0.8  newdate = 08/10/17 
 REPORTING LEVEL = 0.8  newdate = 08/10/17 
 REPORTING LEVEL = 0.8  newdate = 07/14/17 
 REPORTING LEVEL = 0.8  newdate = 07/14/17 
 REPORTING LEVEL = 0.8  newdate = 06/13/17 
 REPORTING LEVEL = 0.8  newdate = 06/13/17 
 REPORTING LEVEL = 0.8  newdate = 04/27/17 
 REPORTING LEVEL = 0.8  newdate = 04/27/17 
 REPORTING LEVEL = 0.8  newdate = 02/24/17 
 REPORTING LEVEL = 0.8  newdate = 02/24/17 
 REPORTING LEVEL = 0.8  newdate = 02/02/17 
 REPORTING LEVEL = 0.8  newdate = 02/02/17 
 REPORTING LEVEL = 0.8  newdate = 02/02/17 
 REPORTING LEVEL = 0.8  newdate = 02/02/17 
 REPORTING LEVEL = 0.8  newdate = 12/23/16 
 REPORTING LEVEL = 0.8  newdate = 12/23/16 
 REPORTING LEVEL = 0.8  newdate = 11/29/16 
 REPORTING LEVEL = 0.8  newdate = 11/29/16 
 REPORTING LEVEL = 0.8  newdate = 11/10/16 
 REPORTING LEVEL = 0.8  newdate = 11/10/16 
 REPORTING LEVEL = 0.8  newdate = 09/28/16 
 REPORTING LEVEL = 0.8  newdate = 09/28/16 
 REPORTING LEVEL = 0.8  newdate = 09/23/16 
 REPORTING LEVEL = 0.8  newdate = 09/23/16 
 REPORTING LEVEL = 0.8  newdate = 08/31/16 
 REPORTING LEVEL = 0.8  newdate = 08/31/16 
 REPORTING LEVEL = 0.8  newdate = 08/12/16 
 REPORTING LEVEL = 0.8  newdate = 08/12/16 
 REPORTING LEVEL = 0.8  newdate = 07/06/16 
 REPORTING LEVEL = 0.8  newdate = 07/06/16 
 REPORTING LEVEL = 0.8  newdate = 07/06/16 
 REPORTING LEVEL = 0.8  newdate = 07/06/16 
 REPORTING LEVEL = 0.8  newdate = 06/23/16 
 REPORTING LEVEL = 0.8  newdate = 06/23/16 
 REPORTING LEVEL = 0.8  newdate = 05/20/16 
 REPORTING LEVEL = 0.8  newdate = 05/20/16 
 REPORTING LEVEL = 0.8  newdate = 04/28/16 
 REPORTING LEVEL = 0.8  newdate = 04/28/16 
 REPORTING LEVEL = 0.8  newdate = 04/09/16 
 REPORTING LEVEL = 0.8  newdate = 04/09/16 
 REPORTING LEVEL = 0.8  newdate = 02/12/16 
 REPORTING LEVEL = 0.8  newdate = 02/12/16 
 REPORTING LEVEL = 0.8  newdate = 01/22/16 
 REPORTING LEVEL = 0.8
The SGPlot Procedure

False Positive & Negative Listing for BUTANOL

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Positive 20163150004 NSI 041516: 25 µl & Phenova B20160303: 25 µl & Accu 216041225: 25 µl 0.8 11/10/16 0.89 0
  20170320043 Abs 060916HVOC: 40 µl & ChemService 5082800: 40 µl & Accu 216041225: 40 µl 0.8 02/02/17 1.13 0
  20171160113 Abs 060916HVOC: 15 µl & ChemService 5082800: 15 µl & NSI 041416HVOC: 15 µl 0.8 04/27/17 1 0
  20171580166 Abs 060916HVOC: 25 µl & ChemService 5082800: 25 µl 0.8 06/13/17 0.72 0
  20172230006 ChemService 6441300: 15 µl & Spex Organics BW170726021: 15 µl & ChemService 6424 0.8 08/16/17 0.96 0

Updated 04/25/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
CHLOROPICRIN
Method: 4437 Testid: 77548GM016
Link to Individual Chart

 newdate = 08/30/17 
 CENC_VAL = 0.044  newdate = 08/16/17 
 CENC_VAL = 0.045  newdate = 08/16/17 
 CENC_VAL = 0.041  newdate = 08/01/17 
 CENC_VAL = 0.056  newdate = 06/24/17 
 CENC_VAL = 0.068  newdate = 06/13/17 
 CENC_VAL = 0.068  newdate = 05/04/17 
 CENC_VAL = 0.052  newdate = 03/24/17 
 CENC_VAL = 0.049  newdate = 03/09/17 
 CENC_VAL = 0.096  newdate = 02/24/17 
 CENC_VAL = 0.068  newdate = 02/02/17 
 CENC_VAL = 0.102  newdate = 02/02/17 
 CENC_VAL = 0.050  newdate = 01/03/17 
 CENC_VAL = 0.059  newdate = 12/05/16 
 CENC_VAL = 0.101  newdate = 11/29/16 
 CENC_VAL = 0.132  newdate = 11/18/16 
 CENC_VAL = 0.053  newdate = 11/18/16 
 CENC_VAL = 0.034  newdate = 11/02/16 
 CENC_VAL = 0.055  newdate = 10/07/16 
 CENC_VAL = 0.040  newdate = 09/28/16 
 CENC_VAL = 0.078  newdate = 09/08/16 
 CENC_VAL = 0.069  newdate = 09/08/16 
 CENC_VAL = 0.084  newdate = 08/18/16 
 CENC_VAL = 0.035  newdate = 08/12/16 
 CENC_VAL = 0.042  newdate = 07/29/16 
 CENC_VAL = 0.117  newdate = 07/14/16 
 CENC_VAL = 0.057  newdate = 07/06/16 
 CENC_VAL = 0.111  newdate = 06/29/16 
 CENC_VAL = 0.098  newdate = 06/03/16 
 CENC_VAL = 0.039  newdate = 05/21/16 
 CENC_VAL = 0.073  newdate = 05/20/16 
 CENC_VAL = 0.044  newdate = 04/09/16 
 CENC_VAL = 0.031  newdate = 03/22/16 
 CENC_VAL = 0.035  newdate = 01/22/16 
 CENC_VAL = 0.088  newdate = 08/30/17 
 REPORTING LEVEL = 0.018  newdate = 08/16/17 
 REPORTING LEVEL = 0.018  newdate = 08/16/17 
 REPORTING LEVEL = 0.018  newdate = 08/16/17 
 REPORTING LEVEL = 0.018  newdate = 08/16/17 
 REPORTING LEVEL = 0.018  newdate = 08/01/17 
 REPORTING LEVEL = 0.018  newdate = 08/01/17 
 REPORTING LEVEL = 0.018  newdate = 06/24/17 
 REPORTING LEVEL = 0.018  newdate = 06/24/17 
 REPORTING LEVEL = 0.018  newdate = 06/13/17 
 REPORTING LEVEL = 0.018  newdate = 06/13/17 
 REPORTING LEVEL = 0.018  newdate = 05/04/17 
 REPORTING LEVEL = 0.018  newdate = 05/04/17 
 REPORTING LEVEL = 0.018  newdate = 03/24/17 
 REPORTING LEVEL = 0.018  newdate = 03/24/17 
 REPORTING LEVEL = 0.018  newdate = 03/09/17 
 REPORTING LEVEL = 0.018  newdate = 03/09/17 
 REPORTING LEVEL = 0.018  newdate = 02/24/17 
 REPORTING LEVEL = 0.018  newdate = 02/24/17 
 REPORTING LEVEL = 0.018  newdate = 02/02/17 
 REPORTING LEVEL = 0.018  newdate = 02/02/17 
 REPORTING LEVEL = 0.018  newdate = 02/02/17 
 REPORTING LEVEL = 0.018  newdate = 02/02/17 
 REPORTING LEVEL = 0.018  newdate = 01/03/17 
 REPORTING LEVEL = 0.018  newdate = 01/03/17 
 REPORTING LEVEL = 0.018  newdate = 12/05/16 
 REPORTING LEVEL = 0.018  newdate = 12/05/16 
 REPORTING LEVEL = 0.018  newdate = 11/29/16 
 REPORTING LEVEL = 0.018  newdate = 11/29/16 
 REPORTING LEVEL = 0.018  newdate = 11/18/16 
 REPORTING LEVEL = 0.018  newdate = 11/18/16 
 REPORTING LEVEL = 0.018  newdate = 11/18/16 
 REPORTING LEVEL = 0.018  newdate = 11/18/16 
 REPORTING LEVEL = 0.018  newdate = 11/02/16 
 REPORTING LEVEL = 0.018  newdate = 11/02/16 
 REPORTING LEVEL = 0.018  newdate = 10/07/16 
 REPORTING LEVEL = 0.018  newdate = 10/07/16 
 REPORTING LEVEL = 0.018  newdate = 09/28/16 
 REPORTING LEVEL = 0.018  newdate = 09/28/16 
 REPORTING LEVEL = 0.018  newdate = 09/08/16 
 REPORTING LEVEL = 0.018  newdate = 09/08/16 
 REPORTING LEVEL = 0.018  newdate = 09/08/16 
 REPORTING LEVEL = 0.018  newdate = 09/08/16 
 REPORTING LEVEL = 0.018  newdate = 08/18/16 
 REPORTING LEVEL = 0.018  newdate = 08/18/16 
 REPORTING LEVEL = 0.018  newdate = 08/12/16 
 REPORTING LEVEL = 0.018  newdate = 08/12/16 
 REPORTING LEVEL = 0.018  newdate = 07/29/16 
 REPORTING LEVEL = 0.018  newdate = 07/29/16 
 REPORTING LEVEL = 0.018  newdate = 07/14/16 
 REPORTING LEVEL = 0.018  newdate = 07/14/16 
 REPORTING LEVEL = 0.018  newdate = 07/06/16 
 REPORTING LEVEL = 0.018  newdate = 07/06/16 
 REPORTING LEVEL = 0.018  newdate = 06/29/16 
 REPORTING LEVEL = 0.018  newdate = 06/29/16 
 REPORTING LEVEL = 0.018  newdate = 06/03/16 
 REPORTING LEVEL = 0.018  newdate = 06/03/16 
 REPORTING LEVEL = 0.018  newdate = 05/21/16 
 REPORTING LEVEL = 0.018  newdate = 05/21/16 
 REPORTING LEVEL = 0.018  newdate = 05/20/16 
 REPORTING LEVEL = 0.018  newdate = 05/20/16 
 REPORTING LEVEL = 0.018  newdate = 04/09/16 
 REPORTING LEVEL = 0.018  newdate = 04/09/16 
 REPORTING LEVEL = 0.018  newdate = 03/22/16 
 REPORTING LEVEL = 0.018  newdate = 03/22/16 
 REPORTING LEVEL = 0.018  newdate = 01/22/16 
 REPORTING LEVEL = 0.018
The SGPlot Procedure

back to table
Organic Blind Sample Program
False Positives & False Negatives
CYCLOHEXANONE
Method: 4437 Testid: 77097GM016
Link to Individual Chart

 newdate = 06/24/17 
 falsepos = 4.88  newdate = 08/16/17 
 CENC_VAL = 3.380  newdate = 08/01/17 
 CENC_VAL = 2.600  newdate = 07/14/17 
 CENC_VAL = 2.450  newdate = 06/13/17 
 CENC_VAL = 4.390  newdate = 04/27/17 
 CENC_VAL = 2.730  newdate = 03/24/17 
 CENC_VAL = 3.090  newdate = 03/10/17 
 CENC_VAL = 4.530  newdate = 03/09/17 
 CENC_VAL = 7.130  newdate = 02/24/17 
 CENC_VAL = 2.560  newdate = 02/02/17 
 CENC_VAL = 6.960  newdate = 01/24/17 
 CENC_VAL = 6.710  newdate = 01/14/17 
 CENC_VAL = 2.660  newdate = 12/23/16 
 CENC_VAL = 4.840  newdate = 12/05/16 
 CENC_VAL = 6.880  newdate = 11/18/16 
 CENC_VAL = 2.790  newdate = 11/10/16 
 CENC_VAL = 4.390  newdate = 10/21/16 
 CENC_VAL = 6.650  newdate = 10/07/16 
 CENC_VAL = 2.830  newdate = 09/23/16 
 CENC_VAL = 7.000  newdate = 09/08/16 
 CENC_VAL = 4.350  newdate = 08/31/16 
 CENC_VAL = 4.420  newdate = 08/18/16 
 CENC_VAL = 2.700  newdate = 08/11/16 
 CENC_VAL = 4.530  newdate = 07/27/16 
 CENC_VAL = 2.660  newdate = 07/14/16 
 CENC_VAL = 4.010  newdate = 07/06/16 
 CENC_VAL = 2.640  newdate = 06/29/16 
 CENC_VAL = 7.790  newdate = 06/23/16 
 CENC_VAL = 2.370  newdate = 06/03/16 
 CENC_VAL = 2.940  newdate = 04/28/16 
 CENC_VAL = 2.490  newdate = 03/22/16 
 CENC_VAL = 1.660  newdate = 02/12/16 
 CENC_VAL = 1.520  newdate = 08/16/17 
 REPORTING LEVEL = 1.2  newdate = 08/01/17 
 REPORTING LEVEL = 1.2  newdate = 08/01/17 
 REPORTING LEVEL = 1.2  newdate = 07/14/17 
 REPORTING LEVEL = 1.2  newdate = 07/14/17 
 REPORTING LEVEL = 1.2  newdate = 06/24/17 
 REPORTING LEVEL = 1.2  newdate = 06/24/17 
 REPORTING LEVEL = 1.2  newdate = 06/13/17 
 REPORTING LEVEL = 1.2  newdate = 06/13/17 
 REPORTING LEVEL = 1.2  newdate = 04/27/17 
 REPORTING LEVEL = 1.2  newdate = 04/27/17 
 REPORTING LEVEL = 1.2  newdate = 03/24/17 
 REPORTING LEVEL = 1.2  newdate = 03/24/17 
 REPORTING LEVEL = 1.2  newdate = 03/10/17 
 REPORTING LEVEL = 1.2  newdate = 03/10/17 
 REPORTING LEVEL = 1.2  newdate = 03/09/17 
 REPORTING LEVEL = 1.2  newdate = 03/09/17 
 REPORTING LEVEL = 1.2  newdate = 02/24/17 
 REPORTING LEVEL = 1.2  newdate = 02/24/17 
 REPORTING LEVEL = 1.2  newdate = 02/02/17 
 REPORTING LEVEL = 1.2  newdate = 02/02/17 
 REPORTING LEVEL = 1.2  newdate = 01/24/17 
 REPORTING LEVEL = 1.2  newdate = 01/24/17 
 REPORTING LEVEL = 1.2  newdate = 01/14/17 
 REPORTING LEVEL = 1.2  newdate = 01/14/17 
 REPORTING LEVEL = 1.2  newdate = 12/23/16 
 REPORTING LEVEL = 1.2  newdate = 12/23/16 
 REPORTING LEVEL = 1.2  newdate = 12/05/16 
 REPORTING LEVEL = 1.2  newdate = 12/05/16 
 REPORTING LEVEL = 1.2  newdate = 11/18/16 
 REPORTING LEVEL = 1.2  newdate = 11/18/16 
 REPORTING LEVEL = 1.2  newdate = 11/10/16 
 REPORTING LEVEL = 1.2  newdate = 11/10/16 
 REPORTING LEVEL = 1.2  newdate = 10/21/16 
 REPORTING LEVEL = 1.2  newdate = 10/21/16 
 REPORTING LEVEL = 1.2  newdate = 10/07/16 
 REPORTING LEVEL = 1.2  newdate = 10/07/16 
 REPORTING LEVEL = 1.2  newdate = 09/23/16 
 REPORTING LEVEL = 1.2  newdate = 09/23/16 
 REPORTING LEVEL = 1.2  newdate = 09/08/16 
 REPORTING LEVEL = 1.2  newdate = 09/08/16 
 REPORTING LEVEL = 1.2  newdate = 08/31/16 
 REPORTING LEVEL = 1.2  newdate = 08/31/16 
 REPORTING LEVEL = 1.2  newdate = 08/18/16 
 REPORTING LEVEL = 1.2  newdate = 08/18/16 
 REPORTING LEVEL = 1.2  newdate = 08/11/16 
 REPORTING LEVEL = 1.2  newdate = 08/11/16 
 REPORTING LEVEL = 1.2  newdate = 07/27/16 
 REPORTING LEVEL = 1.2  newdate = 07/27/16 
 REPORTING LEVEL = 1.2  newdate = 07/14/16 
 REPORTING LEVEL = 1.2  newdate = 07/14/16 
 REPORTING LEVEL = 1.2  newdate = 07/06/16 
 REPORTING LEVEL = 1.2  newdate = 07/06/16 
 REPORTING LEVEL = 1.2  newdate = 06/29/16 
 REPORTING LEVEL = 1.2  newdate = 06/29/16 
 REPORTING LEVEL = 1.2  newdate = 06/23/16 
 REPORTING LEVEL = 1.2  newdate = 06/23/16 
 REPORTING LEVEL = 1.2  newdate = 06/03/16 
 REPORTING LEVEL = 1.2  newdate = 06/03/16 
 REPORTING LEVEL = 1.2  newdate = 04/28/16 
 REPORTING LEVEL = 1.2  newdate = 04/28/16 
 REPORTING LEVEL = 1.2  newdate = 03/22/16 
 REPORTING LEVEL = 1.2  newdate = 03/22/16 
 REPORTING LEVEL = 1.2  newdate = 02/12/16 
 REPORTING LEVEL = 1.2
The SGPlot Procedure

False Positive & Negative Listing for CYCLOHEXANONE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Positive 20171720144 Supelco LC20145V: 25 µl & Abs 060916HVOC: 25 µl & Accu 216041225: 25 µl 1.2 06/24/17 4.88 0

Updated 04/25/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
DIETHYLAMINE,_N-NITROSO-
Method: 4437 Testid: 78200GM016
Link to Individual Chart

 newdate = 06/24/17 
 falsepos = 22  newdate = 08/16/17 
 CENC_VAL = 15.000  newdate = 08/01/17 
 CENC_VAL = 13.000  newdate = 07/14/17 
 CENC_VAL = 12.600  newdate = 06/13/17 
 CENC_VAL = 25.700  newdate = 05/04/17 
 CENC_VAL = 12.000  newdate = 03/24/17 
 CENC_VAL = 15.900  newdate = 03/10/17 
 CENC_VAL = 25.900  newdate = 03/09/17 
 CENC_VAL = 38.300  newdate = 02/24/17 
 CENC_VAL = 14.900  newdate = 02/02/17 
 CENC_VAL = 33.300  newdate = 01/24/17 
 CENC_VAL = 35.300  newdate = 01/14/17 
 CENC_VAL = 13.100  newdate = 12/23/16 
 CENC_VAL = 23.100  newdate = 12/05/16 
 CENC_VAL = 32.400  newdate = 11/18/16 
 CENC_VAL = 13.300  newdate = 11/10/16 
 CENC_VAL = 20.000  newdate = 10/21/16 
 CENC_VAL = 38.700  newdate = 10/07/16 
 CENC_VAL = 15.100  newdate = 09/23/16 
 CENC_VAL = 40.300  newdate = 09/08/16 
 CENC_VAL = 22.900  newdate = 08/31/16 
 CENC_VAL = 23.000  newdate = 08/18/16 
 CENC_VAL = 13.600  newdate = 08/11/16 
 CENC_VAL = 20.400  newdate = 07/27/16 
 CENC_VAL = 11.200  newdate = 07/14/16 
 CENC_VAL = 22.300  newdate = 07/06/16 
 CENC_VAL = 14.600  newdate = 06/29/16 
 CENC_VAL = 34.100  newdate = 06/23/16 
 CENC_VAL = 9.850  newdate = 06/03/16 
 CENC_VAL = 13.600  newdate = 04/09/16 
 CENC_VAL = 7.550  newdate = 03/22/16 
 CENC_VAL = 8.930  newdate = 01/22/16 
 CENC_VAL = 18.300  newdate = 08/16/17 
 REPORTING LEVEL = 6.2  newdate = 08/01/17 
 REPORTING LEVEL = 6.2  newdate = 08/01/17 
 REPORTING LEVEL = 6.2  newdate = 07/14/17 
 REPORTING LEVEL = 6.2  newdate = 07/14/17 
 REPORTING LEVEL = 6.2  newdate = 06/24/17 
 REPORTING LEVEL = 6.2  newdate = 06/24/17 
 REPORTING LEVEL = 6.2  newdate = 06/13/17 
 REPORTING LEVEL = 6.2  newdate = 06/13/17 
 REPORTING LEVEL = 6.2  newdate = 05/04/17 
 REPORTING LEVEL = 6.2  newdate = 05/04/17 
 REPORTING LEVEL = 6.2  newdate = 03/24/17 
 REPORTING LEVEL = 6.2  newdate = 03/24/17 
 REPORTING LEVEL = 6.2  newdate = 03/10/17 
 REPORTING LEVEL = 6.2  newdate = 03/10/17 
 REPORTING LEVEL = 6.2  newdate = 03/09/17 
 REPORTING LEVEL = 6.2  newdate = 03/09/17 
 REPORTING LEVEL = 6.2  newdate = 02/24/17 
 REPORTING LEVEL = 6.2  newdate = 02/24/17 
 REPORTING LEVEL = 6.2  newdate = 02/02/17 
 REPORTING LEVEL = 6.2  newdate = 02/02/17 
 REPORTING LEVEL = 6.2  newdate = 01/24/17 
 REPORTING LEVEL = 6.2  newdate = 01/24/17 
 REPORTING LEVEL = 6.2  newdate = 01/14/17 
 REPORTING LEVEL = 6.2  newdate = 01/14/17 
 REPORTING LEVEL = 6.2  newdate = 12/23/16 
 REPORTING LEVEL = 6.2  newdate = 12/23/16 
 REPORTING LEVEL = 6.2  newdate = 12/05/16 
 REPORTING LEVEL = 6.2  newdate = 12/05/16 
 REPORTING LEVEL = 6.2  newdate = 11/18/16 
 REPORTING LEVEL = 6.2  newdate = 11/18/16 
 REPORTING LEVEL = 6.2  newdate = 11/10/16 
 REPORTING LEVEL = 6.2  newdate = 11/10/16 
 REPORTING LEVEL = 6.2  newdate = 10/21/16 
 REPORTING LEVEL = 6.2  newdate = 10/21/16 
 REPORTING LEVEL = 6.2  newdate = 10/07/16 
 REPORTING LEVEL = 6.2  newdate = 10/07/16 
 REPORTING LEVEL = 6.2  newdate = 09/23/16 
 REPORTING LEVEL = 6.2  newdate = 09/23/16 
 REPORTING LEVEL = 6.2  newdate = 09/08/16 
 REPORTING LEVEL = 6.2  newdate = 09/08/16 
 REPORTING LEVEL = 6.2  newdate = 08/31/16 
 REPORTING LEVEL = 6.2  newdate = 08/31/16 
 REPORTING LEVEL = 6.2  newdate = 08/18/16 
 REPORTING LEVEL = 6.2  newdate = 08/18/16 
 REPORTING LEVEL = 6.2  newdate = 08/11/16 
 REPORTING LEVEL = 6.2  newdate = 08/11/16 
 REPORTING LEVEL = 6.2  newdate = 07/27/16 
 REPORTING LEVEL = 6.2  newdate = 07/27/16 
 REPORTING LEVEL = 6.2  newdate = 07/14/16 
 REPORTING LEVEL = 6.2  newdate = 07/14/16 
 REPORTING LEVEL = 6.2  newdate = 07/06/16 
 REPORTING LEVEL = 6.2  newdate = 07/06/16 
 REPORTING LEVEL = 6.2  newdate = 06/29/16 
 REPORTING LEVEL = 6.2  newdate = 06/29/16 
 REPORTING LEVEL = 6.2  newdate = 06/23/16 
 REPORTING LEVEL = 6.2  newdate = 06/23/16 
 REPORTING LEVEL = 6.2  newdate = 06/03/16 
 REPORTING LEVEL = 6.2  newdate = 06/03/16 
 REPORTING LEVEL = 6.2  newdate = 04/09/16 
 REPORTING LEVEL = 6.2  newdate = 04/09/16 
 REPORTING LEVEL = 6.2  newdate = 03/22/16 
 REPORTING LEVEL = 6.2  newdate = 03/22/16 
 REPORTING LEVEL = 6.2  newdate = 01/22/16 
 REPORTING LEVEL = 6.2
The SGPlot Procedure

False Positive & Negative Listing for DIETHYLAMINE,_N-NITROSO-

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Positive 20171720144 Supelco LC20145V: 25 µl & Abs 060916HVOC: 25 µl & Accu 216041225: 25 µl 6.2 06/24/17 22 0

Updated 04/25/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
DIMETHOXYMETHANE
Method: 4437 Testid: 81578GM016
Link to Individual Chart

 newdate = 08/30/17 
 CENC_VAL = 0.094  newdate = 08/16/17 
 CENC_VAL = 0.130  newdate = 08/10/17 
 CENC_VAL = 0.095  newdate = 08/01/17 
 CENC_VAL = 0.140  newdate = 07/14/17 
 CENC_VAL = 0.113  newdate = 02/24/17 
 CENC_VAL = 0.139  newdate = 02/02/17 
 CENC_VAL = 0.117  newdate = 12/23/16 
 CENC_VAL = 0.174  newdate = 11/29/16 
 CENC_VAL = 0.283  newdate = 09/28/16 
 CENC_VAL = 0.199  newdate = 09/23/16 
 CENC_VAL = 0.313  newdate = 08/31/16 
 CENC_VAL = 0.200  newdate = 08/12/16 
 CENC_VAL = 0.113  newdate = 07/06/16 
 CENC_VAL = 0.273  newdate = 07/06/16 
 CENC_VAL = 0.102  newdate = 06/23/16 
 CENC_VAL = 0.115  newdate = 05/26/16 
 CENC_VAL = 0.115  newdate = 04/09/16 
 CENC_VAL = 0.075  newdate = 03/22/16 
 CENC_VAL = 0.120  newdate = 01/22/16 
 CENC_VAL = 0.319  newdate = 08/30/17 
 REPORTING LEVEL = 0.044  newdate = 08/16/17 
 REPORTING LEVEL = 0.044  newdate = 08/16/17 
 REPORTING LEVEL = 0.044  newdate = 08/10/17 
 REPORTING LEVEL = 0.044  newdate = 08/10/17 
 REPORTING LEVEL = 0.044  newdate = 08/01/17 
 REPORTING LEVEL = 0.044  newdate = 08/01/17 
 REPORTING LEVEL = 0.044  newdate = 07/14/17 
 REPORTING LEVEL = 0.044  newdate = 07/14/17 
 REPORTING LEVEL = 0.044  newdate = 02/24/17 
 REPORTING LEVEL = 0.044  newdate = 02/24/17 
 REPORTING LEVEL = 0.044  newdate = 02/02/17 
 REPORTING LEVEL = 0.044  newdate = 02/02/17 
 REPORTING LEVEL = 0.044  newdate = 12/23/16 
 REPORTING LEVEL = 0.044  newdate = 12/23/16 
 REPORTING LEVEL = 0.044  newdate = 11/29/16 
 REPORTING LEVEL = 0.044  newdate = 11/29/16 
 REPORTING LEVEL = 0.044  newdate = 09/28/16 
 REPORTING LEVEL = 0.044  newdate = 09/28/16 
 REPORTING LEVEL = 0.044  newdate = 09/23/16 
 REPORTING LEVEL = 0.044  newdate = 09/23/16 
 REPORTING LEVEL = 0.044  newdate = 08/31/16 
 REPORTING LEVEL = 0.044  newdate = 08/31/16 
 REPORTING LEVEL = 0.044  newdate = 08/12/16 
 REPORTING LEVEL = 0.044  newdate = 08/12/16 
 REPORTING LEVEL = 0.044  newdate = 07/06/16 
 REPORTING LEVEL = 0.044  newdate = 07/06/16 
 REPORTING LEVEL = 0.044  newdate = 07/06/16 
 REPORTING LEVEL = 0.044  newdate = 07/06/16 
 REPORTING LEVEL = 0.044  newdate = 06/23/16 
 REPORTING LEVEL = 0.044  newdate = 06/23/16 
 REPORTING LEVEL = 0.044  newdate = 05/26/16 
 REPORTING LEVEL = 0.044  newdate = 05/26/16 
 REPORTING LEVEL = 0.044  newdate = 04/09/16 
 REPORTING LEVEL = 0.044  newdate = 04/09/16 
 REPORTING LEVEL = 0.044  newdate = 03/22/16 
 REPORTING LEVEL = 0.044  newdate = 03/22/16 
 REPORTING LEVEL = 0.044  newdate = 01/22/16 
 REPORTING LEVEL = 0.044
The SGPlot Procedure

back to table
Organic Blind Sample Program
False Positives & False Negatives
HEXACHLOROCYCLOPENTADIENE
Method: 4437 Testid: 34386GM016
Link to Individual Chart

 newdate = 03/10/17 
 falsepos = 5.47  newdate = 02/24/17 
 falsepos = 5.02  newdate = 01/24/17 
 falsepos = 7.95  newdate = 01/14/17 
 falsepos = 2.59  newdate = 01/03/17 
 falsepos = 3  newdate = 11/02/16 
 falsepos = 3.28  newdate = 10/21/16 
 falsepos = 9.7  newdate = 09/08/16 
 falsepos = 4.7  newdate = 08/11/16 
 falsepos = 4.72  newdate = 07/29/16 
 falsepos = 9.13  newdate = 07/27/16 
 falsepos = 3.07  newdate = 05/21/16 
 falsepos = 6  newdate = 08/30/17 
 CENC_VAL = 5.240  newdate = 08/16/17 
 CENC_VAL = 4.320  newdate = 07/14/17 
 CENC_VAL = 1.840  newdate = 02/24/17 
 CENC_VAL = 2.780  newdate = 02/02/17 
 CENC_VAL = 2.470  newdate = 12/23/16 
 CENC_VAL = 4.150  newdate = 11/29/16 
 CENC_VAL = 5.650  newdate = 09/28/16 
 CENC_VAL = 4.310  newdate = 09/23/16 
 CENC_VAL = 6.650  newdate = 08/31/16 
 CENC_VAL = 4.010  newdate = 08/12/16 
 CENC_VAL = 2.540  newdate = 07/06/16 
 CENC_VAL = 6.600  newdate = 07/06/16 
 CENC_VAL = 2.200  newdate = 06/23/16 
 CENC_VAL = 1.950  newdate = 05/20/16 
 CENC_VAL = 2.350  newdate = 04/09/16 
 CENC_VAL = 1.850  newdate = 03/22/16 
 CENC_VAL = 2.030  newdate = 01/22/16 
 CENC_VAL = 4.670  newdate = 08/30/17 
 REPORTING LEVEL = 1.6  newdate = 08/16/17 
 REPORTING LEVEL = 1.6  newdate = 08/16/17 
 REPORTING LEVEL = 1.6  newdate = 07/14/17 
 REPORTING LEVEL = 1.6  newdate = 07/14/17 
 REPORTING LEVEL = 1.6  newdate = 03/10/17 
 REPORTING LEVEL = 1.6  newdate = 03/10/17 
 REPORTING LEVEL = 1.6  newdate = 02/24/17 
 REPORTING LEVEL = 1.6  newdate = 02/24/17 
 REPORTING LEVEL = 1.6  newdate = 02/24/17 
 REPORTING LEVEL = 1.6  newdate = 02/24/17 
 REPORTING LEVEL = 1.6  newdate = 02/02/17 
 REPORTING LEVEL = 1.6  newdate = 02/02/17 
 REPORTING LEVEL = 1.6  newdate = 01/24/17 
 REPORTING LEVEL = 1.6  newdate = 01/24/17 
 REPORTING LEVEL = 1.6  newdate = 01/14/17 
 REPORTING LEVEL = 1.6  newdate = 01/14/17 
 REPORTING LEVEL = 1.6  newdate = 01/03/17 
 REPORTING LEVEL = 1.6  newdate = 01/03/17 
 REPORTING LEVEL = 1.6  newdate = 12/23/16 
 REPORTING LEVEL = 1.6  newdate = 12/23/16 
 REPORTING LEVEL = 1.6  newdate = 11/29/16 
 REPORTING LEVEL = 1.6  newdate = 11/29/16 
 REPORTING LEVEL = 1.6  newdate = 11/02/16 
 REPORTING LEVEL = 1.6  newdate = 11/02/16 
 REPORTING LEVEL = 1.6  newdate = 10/21/16 
 REPORTING LEVEL = 1.6  newdate = 10/21/16 
 REPORTING LEVEL = 1.6  newdate = 09/28/16 
 REPORTING LEVEL = 1.6  newdate = 09/28/16 
 REPORTING LEVEL = 1.6  newdate = 09/23/16 
 REPORTING LEVEL = 1.6  newdate = 09/23/16 
 REPORTING LEVEL = 1.6  newdate = 09/08/16 
 REPORTING LEVEL = 1.6  newdate = 09/08/16 
 REPORTING LEVEL = 1.6  newdate = 08/31/16 
 REPORTING LEVEL = 1.6  newdate = 08/31/16 
 REPORTING LEVEL = 1.6  newdate = 08/12/16 
 REPORTING LEVEL = 1.6  newdate = 08/12/16 
 REPORTING LEVEL = 1.6  newdate = 08/11/16 
 REPORTING LEVEL = 1.6  newdate = 08/11/16 
 REPORTING LEVEL = 1.6  newdate = 07/29/16 
 REPORTING LEVEL = 1.6  newdate = 07/29/16 
 REPORTING LEVEL = 1.6  newdate = 07/27/16 
 REPORTING LEVEL = 1.6  newdate = 07/27/16 
 REPORTING LEVEL = 1.6  newdate = 07/06/16 
 REPORTING LEVEL = 1.6  newdate = 07/06/16 
 REPORTING LEVEL = 1.6  newdate = 07/06/16 
 REPORTING LEVEL = 1.6  newdate = 07/06/16 
 REPORTING LEVEL = 1.6  newdate = 06/23/16 
 REPORTING LEVEL = 1.6  newdate = 06/23/16 
 REPORTING LEVEL = 1.6  newdate = 05/21/16 
 REPORTING LEVEL = 1.6  newdate = 05/21/16 
 REPORTING LEVEL = 1.6  newdate = 05/20/16 
 REPORTING LEVEL = 1.6  newdate = 05/20/16 
 REPORTING LEVEL = 1.6  newdate = 04/09/16 
 REPORTING LEVEL = 1.6  newdate = 04/09/16 
 REPORTING LEVEL = 1.6  newdate = 03/22/16 
 REPORTING LEVEL = 1.6  newdate = 03/22/16 
 REPORTING LEVEL = 1.6  newdate = 01/22/16 
 REPORTING LEVEL = 1.6
The SGPlot Procedure

False Positive & Negative Listing for HEXACHLOROCYCLOPENTADIENE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Positive 20161400192 Supelco LC20145V: 25 µl & NSI 041516: 25 µl & NSI 041416HVOC: 25 µl 1.6 05/21/16 E 6 0
  20162020127 ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl 1.6 07/27/16 E 3.07 0
  20162100018 Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 1.6 07/29/16 E 9.13 0
  20162150211 Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl 1.6 08/11/16 E 4.72 0
  20162440116 Supelco LC20145V: 25 µl & Abs 060916HVOC: 25 µl 1.6 09/08/16 E 4.7 0
  20162860093 ChemService 5082800: 40 µl & Supelco LC20145V: 40 µl & NSI 041416HVOC: 40 µl 1.6 10/21/16 E 9.7 0
  20162990157 Supelco LC20145V: 15 µl & Abs 060916HVOC: 15 µl & Accu 216041225: 15 µl 1.6 11/02/16 E 3.28 0
  20163630040 Supelco LC20145V: 15 µl & Abs 060916HVOC: 15 µl & NSI 041416HVOC: 15 µl 1.6 01/03/17 E 3 0
  20170040034 Phenova B20160303: 15 µl & Supelco LC20145V: 15 µl 1.6 01/14/17 E 2.59 0
  20170190023 ChemService 5082800: 40 µl & Supelco LC20145V: 40 µl 1.6 01/24/17 E 7.95 0
  20170530013 Supelco LC20145V: 25 µl & NSI 110916: 25 µl 1.6 02/24/17 E 5.02 0
  20170680005 Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & Accu 216041225: 25 µl 1.6 03/10/17 E 5.47 0

Updated 04/25/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
HEXANOL,_2-ETHYL-
Method: 4437 Testid: 77311GM016
Link to Individual Chart

 newdate = 02/02/17 
 falseneg = -0.01  newdate = 01/03/17 
 falseneg = -0.01  newdate = 08/16/17 
 CENC_VAL = 6.100  newdate = 06/24/17 
 CENC_VAL = 7.800  newdate = 06/13/17 
 CENC_VAL = 7.000  newdate = 04/27/17 
 CENC_VAL = 4.400  newdate = 03/24/17 
 CENC_VAL = 5.300  newdate = 03/09/17 
 CENC_VAL = 10.700  newdate = 02/24/17 
 CENC_VAL = 6.000  newdate = 02/02/17 
 CENC_VAL = 10.100  newdate = 12/05/16 
 CENC_VAL = 10.500  newdate = 11/29/16 
 CENC_VAL = 9.900  newdate = 11/18/16 
 CENC_VAL = 4.800  newdate = 11/10/16 
 CENC_VAL = 6.300  newdate = 11/02/16 
 CENC_VAL = 5.200  newdate = 10/07/16 
 CENC_VAL = 5.500  newdate = 09/28/16 
 CENC_VAL = 7.600  newdate = 09/08/16 
 CENC_VAL = 7.300  newdate = 09/08/16 
 CENC_VAL = 7.000  newdate = 08/18/16 
 CENC_VAL = 5.100  newdate = 08/12/16 
 CENC_VAL = 4.600  newdate = 07/29/16 
 CENC_VAL = 10.100  newdate = 07/14/16 
 CENC_VAL = 5.200  newdate = 07/06/16 
 CENC_VAL = 9.200  newdate = 06/29/16 
 CENC_VAL = 9.900  newdate = 06/03/16 
 CENC_VAL = 4.400  newdate = 05/21/16 
 CENC_VAL = 6.700  newdate = 05/20/16 
 CENC_VAL = 4.400  newdate = 04/28/16 
 CENC_VAL = 4.600  newdate = 03/22/16 
 CENC_VAL = 2.800  newdate = 02/12/16 
 CENC_VAL = 2.900  newdate = 08/16/17 
 REPORTING LEVEL = 2  newdate = 06/24/17 
 REPORTING LEVEL = 2  newdate = 06/24/17 
 REPORTING LEVEL = 2  newdate = 06/13/17 
 REPORTING LEVEL = 2  newdate = 06/13/17 
 REPORTING LEVEL = 2  newdate = 04/27/17 
 REPORTING LEVEL = 2  newdate = 04/27/17 
 REPORTING LEVEL = 2  newdate = 03/24/17 
 REPORTING LEVEL = 2  newdate = 03/24/17 
 REPORTING LEVEL = 2  newdate = 03/09/17 
 REPORTING LEVEL = 2  newdate = 03/09/17 
 REPORTING LEVEL = 2  newdate = 02/24/17 
 REPORTING LEVEL = 2  newdate = 02/24/17 
 REPORTING LEVEL = 2  newdate = 02/02/17 
 REPORTING LEVEL = 2  newdate = 02/02/17 
 REPORTING LEVEL = 2  newdate = 02/02/17 
 REPORTING LEVEL = 2  newdate = 02/02/17 
 REPORTING LEVEL = 2  newdate = 01/03/17 
 REPORTING LEVEL = 2  newdate = 01/03/17 
 REPORTING LEVEL = 2  newdate = 12/05/16 
 REPORTING LEVEL = 2  newdate = 12/05/16 
 REPORTING LEVEL = 2  newdate = 11/29/16 
 REPORTING LEVEL = 2  newdate = 11/29/16 
 REPORTING LEVEL = 2  newdate = 11/18/16 
 REPORTING LEVEL = 2  newdate = 11/18/16 
 REPORTING LEVEL = 2  newdate = 11/10/16 
 REPORTING LEVEL = 2  newdate = 11/10/16 
 REPORTING LEVEL = 2  newdate = 11/02/16 
 REPORTING LEVEL = 2  newdate = 11/02/16 
 REPORTING LEVEL = 2  newdate = 10/07/16 
 REPORTING LEVEL = 2  newdate = 10/07/16 
 REPORTING LEVEL = 2  newdate = 09/28/16 
 REPORTING LEVEL = 2  newdate = 09/28/16 
 REPORTING LEVEL = 2  newdate = 09/08/16 
 REPORTING LEVEL = 2  newdate = 09/08/16 
 REPORTING LEVEL = 2  newdate = 09/08/16 
 REPORTING LEVEL = 2  newdate = 09/08/16 
 REPORTING LEVEL = 2  newdate = 08/18/16 
 REPORTING LEVEL = 2  newdate = 08/18/16 
 REPORTING LEVEL = 2  newdate = 08/12/16 
 REPORTING LEVEL = 2  newdate = 08/12/16 
 REPORTING LEVEL = 2  newdate = 07/29/16 
 REPORTING LEVEL = 2  newdate = 07/29/16 
 REPORTING LEVEL = 2  newdate = 07/14/16 
 REPORTING LEVEL = 2  newdate = 07/14/16 
 REPORTING LEVEL = 2  newdate = 07/06/16 
 REPORTING LEVEL = 2  newdate = 07/06/16 
 REPORTING LEVEL = 2  newdate = 06/29/16 
 REPORTING LEVEL = 2  newdate = 06/29/16 
 REPORTING LEVEL = 2  newdate = 06/03/16 
 REPORTING LEVEL = 2  newdate = 06/03/16 
 REPORTING LEVEL = 2  newdate = 05/21/16 
 REPORTING LEVEL = 2  newdate = 05/21/16 
 REPORTING LEVEL = 2  newdate = 05/20/16 
 REPORTING LEVEL = 2  newdate = 05/20/16 
 REPORTING LEVEL = 2  newdate = 04/28/16 
 REPORTING LEVEL = 2  newdate = 04/28/16 
 REPORTING LEVEL = 2  newdate = 03/22/16 
 REPORTING LEVEL = 2  newdate = 03/22/16 
 REPORTING LEVEL = 2  newdate = 02/12/16 
 REPORTING LEVEL = 2  Y = 0
The SGPlot Procedure

False Positive & Negative Listing for HEXANOL,_2-ETHYL-

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20163630040 Supelco LC20145V: 15 µl & Abs 060916HVOC: 15 µl & NSI 041416HVOC: 15 µl 2 01/03/17 < 3.9 5.013
  20170260002 Accu 216041354: 15 µl & NSI 110916: 15 µl & Accu 216041225: 15 µl 2 02/02/17 < 3.8 5.001

Updated 04/25/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
ISOPHORONE
Method: 4437 Testid: 34408GM016
Link to Individual Chart

 newdate = 07/29/16 
 falsepos = 25.1  newdate = 08/30/17 
 CENC_VAL = 6.590  newdate = 08/10/17 
 CENC_VAL = 9.260  newdate = 07/14/17 
 CENC_VAL = 7.830  newdate = 06/01/17 
 CENC_VAL = 17.600  newdate = 04/13/17 
 CENC_VAL = 31.700  newdate = 02/24/17 
 CENC_VAL = 9.600  newdate = 02/02/17 
 CENC_VAL = 8.700  newdate = 12/23/16 
 CENC_VAL = 17.300  newdate = 11/29/16 
 CENC_VAL = 20.000  newdate = 09/28/16 
 CENC_VAL = 15.700  newdate = 09/23/16 
 CENC_VAL = 25.400  newdate = 08/31/16 
 CENC_VAL = 15.100  newdate = 08/12/16 
 CENC_VAL = 9.520  newdate = 07/06/16 
 CENC_VAL = 28.800  newdate = 07/06/16 
 CENC_VAL = 9.040  newdate = 06/23/16 
 CENC_VAL = 4.720  newdate = 05/20/16 
 CENC_VAL = 10.200  newdate = 04/28/16 
 CENC_VAL = 11.800  newdate = 04/09/16 
 CENC_VAL = 6.410  newdate = 02/12/16 
 CENC_VAL = 5.810  newdate = 01/22/16 
 CENC_VAL = 13.900  newdate = 08/30/17 
 REPORTING LEVEL = 5  newdate = 08/10/17 
 REPORTING LEVEL = 5  newdate = 08/10/17 
 REPORTING LEVEL = 5  newdate = 07/14/17 
 REPORTING LEVEL = 5  newdate = 07/14/17 
 REPORTING LEVEL = 5  newdate = 06/01/17 
 REPORTING LEVEL = 5  newdate = 06/01/17 
 REPORTING LEVEL = 5  newdate = 04/13/17 
 REPORTING LEVEL = 5  newdate = 04/13/17 
 REPORTING LEVEL = 5  newdate = 02/24/17 
 REPORTING LEVEL = 5  newdate = 02/24/17 
 REPORTING LEVEL = 5  newdate = 02/02/17 
 REPORTING LEVEL = 5  newdate = 02/02/17 
 REPORTING LEVEL = 5  newdate = 12/23/16 
 REPORTING LEVEL = 5  newdate = 12/23/16 
 REPORTING LEVEL = 5  newdate = 11/29/16 
 REPORTING LEVEL = 5  newdate = 11/29/16 
 REPORTING LEVEL = 5  newdate = 09/28/16 
 REPORTING LEVEL = 5  newdate = 09/28/16 
 REPORTING LEVEL = 5  newdate = 09/23/16 
 REPORTING LEVEL = 5  newdate = 09/23/16 
 REPORTING LEVEL = 5  newdate = 08/31/16 
 REPORTING LEVEL = 5  newdate = 08/31/16 
 REPORTING LEVEL = 5  newdate = 08/12/16 
 REPORTING LEVEL = 5  newdate = 08/12/16 
 REPORTING LEVEL = 5  newdate = 07/29/16 
 REPORTING LEVEL = 5  newdate = 07/29/16 
 REPORTING LEVEL = 5  newdate = 07/06/16 
 REPORTING LEVEL = 5  newdate = 07/06/16 
 REPORTING LEVEL = 5  newdate = 07/06/16 
 REPORTING LEVEL = 5  newdate = 07/06/16 
 REPORTING LEVEL = 5  newdate = 06/23/16 
 REPORTING LEVEL = 5  newdate = 06/23/16 
 REPORTING LEVEL = 5  newdate = 05/20/16 
 REPORTING LEVEL = 5  newdate = 05/20/16 
 REPORTING LEVEL = 5  newdate = 04/28/16 
 REPORTING LEVEL = 5  newdate = 04/28/16 
 REPORTING LEVEL = 5  newdate = 04/09/16 
 REPORTING LEVEL = 5  newdate = 04/09/16 
 REPORTING LEVEL = 5  newdate = 02/12/16 
 REPORTING LEVEL = 5  newdate = 02/12/16 
 REPORTING LEVEL = 5  newdate = 01/22/16 
 REPORTING LEVEL = 5
The SGPlot Procedure

False Positive & Negative Listing for ISOPHORONE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Positive 20162100018 Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 5 07/29/16 E 25.1 0

Updated 04/25/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
ISOPROPYL_ALCOHOL
Method: 4437 Testid: 77015GM016
Link to Individual Chart

 newdate = 02/02/17 
 falsepos = 0.77  newdate = 08/30/17 
 CENC_VAL = 2.470  newdate = 08/16/17 
 CENC_VAL = 3.700  newdate = 08/10/17 
 CENC_VAL = 3.030  newdate = 08/01/17 
 CENC_VAL = 12.300  newdate = 07/14/17 
 CENC_VAL = 1.870  newdate = 02/02/17 
 CENC_VAL = 1.380  newdate = 12/23/16 
 CENC_VAL = 3.190  newdate = 11/29/16 
 CENC_VAL = 3.830  newdate = 09/28/16 
 CENC_VAL = 2.190  newdate = 08/31/16 
 CENC_VAL = 2.430  newdate = 08/12/16 
 CENC_VAL = 1.420  newdate = 07/06/16 
 CENC_VAL = 4.180  newdate = 06/23/16 
 CENC_VAL = 1.040  newdate = 05/20/16 
 CENC_VAL = 2.290  newdate = 04/09/16 
 CENC_VAL = 1.200  newdate = 03/22/16 
 CENC_VAL = 1.250  newdate = 01/22/16 
 CENC_VAL = 2.180  newdate = 08/30/17 
 REPORTING LEVEL = 0.6  newdate = 08/16/17 
 REPORTING LEVEL = 0.6  newdate = 08/16/17 
 REPORTING LEVEL = 0.6  newdate = 08/10/17 
 REPORTING LEVEL = 0.6  newdate = 08/10/17 
 REPORTING LEVEL = 0.6  newdate = 08/01/17 
 REPORTING LEVEL = 0.6  newdate = 08/01/17 
 REPORTING LEVEL = 0.6  newdate = 07/14/17 
 REPORTING LEVEL = 0.6  newdate = 07/14/17 
 REPORTING LEVEL = 0.6  newdate = 02/02/17 
 REPORTING LEVEL = 0.6  newdate = 02/02/17 
 REPORTING LEVEL = 0.6  newdate = 02/02/17 
 REPORTING LEVEL = 0.6  newdate = 02/02/17 
 REPORTING LEVEL = 0.6  newdate = 12/23/16 
 REPORTING LEVEL = 0.6  newdate = 12/23/16 
 REPORTING LEVEL = 0.6  newdate = 11/29/16 
 REPORTING LEVEL = 0.6  newdate = 11/29/16 
 REPORTING LEVEL = 0.6  newdate = 09/28/16 
 REPORTING LEVEL = 0.6  newdate = 09/28/16 
 REPORTING LEVEL = 0.6  newdate = 08/31/16 
 REPORTING LEVEL = 0.6  newdate = 08/31/16 
 REPORTING LEVEL = 0.6  newdate = 08/12/16 
 REPORTING LEVEL = 0.6  newdate = 08/12/16 
 REPORTING LEVEL = 0.6  newdate = 07/06/16 
 REPORTING LEVEL = 0.6  newdate = 07/06/16 
 REPORTING LEVEL = 0.6  newdate = 06/23/16 
 REPORTING LEVEL = 0.6  newdate = 06/23/16 
 REPORTING LEVEL = 0.6  newdate = 05/20/16 
 REPORTING LEVEL = 0.6  newdate = 05/20/16 
 REPORTING LEVEL = 0.6  newdate = 04/09/16 
 REPORTING LEVEL = 0.6  newdate = 04/09/16 
 REPORTING LEVEL = 0.6  newdate = 03/22/16 
 REPORTING LEVEL = 0.6  newdate = 03/22/16 
 REPORTING LEVEL = 0.6  newdate = 01/22/16 
 REPORTING LEVEL = 0.6  Y = 0
The SGPlot Procedure

False Positive & Negative Listing for ISOPROPYL_ALCOHOL

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Positive 20170320043 Abs 060916HVOC: 40 µl & ChemService 5082800: 40 µl & Accu 216041225: 40 µl 0.6 02/02/17 0.77 0

Updated 04/25/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
METHYL_ACETATE
Method: 4437 Testid: 77032GM016
Link to Individual Chart

 newdate = 03/10/17 
 falseneg = -0.01  newdate = 06/23/16 
 falsepos = 0.346  newdate = 08/30/17 
 CENC_VAL = 0.260  newdate = 08/16/17 
 CENC_VAL = 0.459  newdate = 08/10/17 
 CENC_VAL = 0.291  newdate = 07/14/17 
 CENC_VAL = 0.342  newdate = 06/24/17 
 CENC_VAL = 0.627  newdate = 06/17/17 
 CENC_VAL = 0.475  newdate = 06/01/17 
 CENC_VAL = 0.346  newdate = 04/27/17 
 CENC_VAL = 0.275  newdate = 04/13/17 
 CENC_VAL = 0.417  newdate = 03/24/17 
 CENC_VAL = 0.421  newdate = 02/24/17 
 CENC_VAL = 0.401  newdate = 02/02/17 
 CENC_VAL = 0.975  newdate = 02/02/17 
 CENC_VAL = 0.363  newdate = 01/03/17 
 CENC_VAL = 0.260  newdate = 12/23/16 
 CENC_VAL = 0.455  newdate = 11/18/16 
 CENC_VAL = 0.364  newdate = 11/10/16 
 CENC_VAL = 0.678  newdate = 11/02/16 
 CENC_VAL = 0.353  newdate = 10/21/16 
 CENC_VAL = 0.908  newdate = 09/28/16 
 CENC_VAL = 0.675  newdate = 09/08/16 
 CENC_VAL = 0.573  newdate = 08/11/16 
 CENC_VAL = 0.438  newdate = 07/29/16 
 CENC_VAL = 0.823  newdate = 07/27/16 
 CENC_VAL = 0.343  newdate = 07/14/16 
 CENC_VAL = 0.596  newdate = 07/06/16 
 CENC_VAL = 0.693  newdate = 07/06/16 
 CENC_VAL = 0.271  newdate = 06/03/16 
 CENC_VAL = 0.287  newdate = 05/21/16 
 CENC_VAL = 0.547  newdate = 05/20/16 
 CENC_VAL = 0.393  newdate = 04/28/16 
 CENC_VAL = 0.447  newdate = 04/09/16 
 CENC_VAL = 0.214  newdate = 02/12/16 
 CENC_VAL = 0.242  newdate = 01/22/16 
 CENC_VAL = 0.667  newdate = 08/30/17 
 REPORTING LEVEL = 0.14  newdate = 08/16/17 
 REPORTING LEVEL = 0.14  newdate = 08/16/17 
 REPORTING LEVEL = 0.14  newdate = 08/10/17 
 REPORTING LEVEL = 0.14  newdate = 08/10/17 
 REPORTING LEVEL = 0.14  newdate = 07/14/17 
 REPORTING LEVEL = 0.14  newdate = 07/14/17 
 REPORTING LEVEL = 0.14  newdate = 06/24/17 
 REPORTING LEVEL = 0.14  newdate = 06/24/17 
 REPORTING LEVEL = 0.14  newdate = 06/17/17 
 REPORTING LEVEL = 0.14  newdate = 06/17/17 
 REPORTING LEVEL = 0.14  newdate = 06/01/17 
 REPORTING LEVEL = 0.14  newdate = 06/01/17 
 REPORTING LEVEL = 0.14  newdate = 04/27/17 
 REPORTING LEVEL = 0.14  newdate = 04/27/17 
 REPORTING LEVEL = 0.14  newdate = 04/13/17 
 REPORTING LEVEL = 0.14  newdate = 04/13/17 
 REPORTING LEVEL = 0.14  newdate = 03/24/17 
 REPORTING LEVEL = 0.14  newdate = 03/24/17 
 REPORTING LEVEL = 0.14  newdate = 03/10/17 
 REPORTING LEVEL = 0.14  newdate = 03/10/17 
 REPORTING LEVEL = 0.14  newdate = 02/24/17 
 REPORTING LEVEL = 0.14  newdate = 02/24/17 
 REPORTING LEVEL = 0.14  newdate = 02/02/17 
 REPORTING LEVEL = 0.14  newdate = 02/02/17 
 REPORTING LEVEL = 0.14  newdate = 02/02/17 
 REPORTING LEVEL = 0.14  newdate = 02/02/17 
 REPORTING LEVEL = 0.14  newdate = 01/03/17 
 REPORTING LEVEL = 0.14  newdate = 01/03/17 
 REPORTING LEVEL = 0.14  newdate = 12/23/16 
 REPORTING LEVEL = 0.14  newdate = 12/23/16 
 REPORTING LEVEL = 0.14  newdate = 11/18/16 
 REPORTING LEVEL = 0.14  newdate = 11/18/16 
 REPORTING LEVEL = 0.14  newdate = 11/10/16 
 REPORTING LEVEL = 0.14  newdate = 11/10/16 
 REPORTING LEVEL = 0.14  newdate = 11/02/16 
 REPORTING LEVEL = 0.14  newdate = 11/02/16 
 REPORTING LEVEL = 0.14  newdate = 10/21/16 
 REPORTING LEVEL = 0.14  newdate = 10/21/16 
 REPORTING LEVEL = 0.14  newdate = 09/28/16 
 REPORTING LEVEL = 0.14  newdate = 09/28/16 
 REPORTING LEVEL = 0.14  newdate = 09/08/16 
 REPORTING LEVEL = 0.14  newdate = 09/08/16 
 REPORTING LEVEL = 0.14  newdate = 08/11/16 
 REPORTING LEVEL = 0.14  newdate = 08/11/16 
 REPORTING LEVEL = 0.14  newdate = 07/29/16 
 REPORTING LEVEL = 0.14  newdate = 07/29/16 
 REPORTING LEVEL = 0.14  newdate = 07/27/16 
 REPORTING LEVEL = 0.14  newdate = 07/27/16 
 REPORTING LEVEL = 0.14  newdate = 07/14/16 
 REPORTING LEVEL = 0.14  newdate = 07/14/16 
 REPORTING LEVEL = 0.14  newdate = 07/06/16 
 REPORTING LEVEL = 0.14  newdate = 07/06/16 
 REPORTING LEVEL = 0.14  newdate = 07/06/16 
 REPORTING LEVEL = 0.14  newdate = 07/06/16 
 REPORTING LEVEL = 0.14  newdate = 06/23/16 
 REPORTING LEVEL = 0.14  newdate = 06/23/16 
 REPORTING LEVEL = 0.14  newdate = 06/03/16 
 REPORTING LEVEL = 0.14  newdate = 06/03/16 
 REPORTING LEVEL = 0.14  newdate = 05/21/16 
 REPORTING LEVEL = 0.14  newdate = 05/21/16 
 REPORTING LEVEL = 0.14  newdate = 05/20/16 
 REPORTING LEVEL = 0.14  newdate = 05/20/16 
 REPORTING LEVEL = 0.14  newdate = 04/28/16 
 REPORTING LEVEL = 0.14  newdate = 04/28/16 
 REPORTING LEVEL = 0.14  newdate = 04/09/16 
 REPORTING LEVEL = 0.14  newdate = 04/09/16 
 REPORTING LEVEL = 0.14  newdate = 02/12/16 
 REPORTING LEVEL = 0.14  newdate = 02/12/16 
 REPORTING LEVEL = 0.14  newdate = 01/22/16 
 REPORTING LEVEL = 0.14  Y = 0
The SGPlot Procedure

False Positive & Negative Listing for METHYL_ACETATE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20170680005 Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & Accu 216041225: 25 µl 0.14 03/10/17 < 0.14 0.5825
False Positive 20161680364   0.14 06/23/16 0.346 0

Updated 04/25/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
N-PENTANAL
Method: 4437 Testid: 77061GM016
Link to Individual Chart

 newdate = 06/24/17 
 falsepos = 0.212  newdate = 08/30/17 
 CENC_VAL = 0.107  newdate = 08/10/17 
 CENC_VAL = 0.105  newdate = 08/01/17 
 CENC_VAL = 0.118  newdate = 03/24/17 
 CENC_VAL = 0.125  newdate = 03/10/17 
 CENC_VAL = 0.180  newdate = 03/09/17 
 CENC_VAL = 0.293  newdate = 02/24/17 
 CENC_VAL = 0.115  newdate = 01/14/17 
 CENC_VAL = 0.112  newdate = 12/05/16 
 CENC_VAL = 0.314  newdate = 11/10/16 
 CENC_VAL = 0.209  newdate = 09/23/16 
 CENC_VAL = 0.284  newdate = 09/08/16 
 CENC_VAL = 0.193  newdate = 08/11/16 
 CENC_VAL = 0.186  newdate = 07/06/16 
 CENC_VAL = 0.131  newdate = 06/03/16 
 CENC_VAL = 0.109  newdate = 02/12/16 
 CENC_VAL = 0.079  newdate = 01/22/16 
 CENC_VAL = 0.166  newdate = 08/30/17 
 REPORTING LEVEL = 0.054  newdate = 08/10/17 
 REPORTING LEVEL = 0.054  newdate = 08/10/17 
 REPORTING LEVEL = 0.054  newdate = 08/01/17 
 REPORTING LEVEL = 0.054  newdate = 08/01/17 
 REPORTING LEVEL = 0.054  newdate = 06/24/17 
 REPORTING LEVEL = 0.054  newdate = 06/24/17 
 REPORTING LEVEL = 0.054  newdate = 03/24/17 
 REPORTING LEVEL = 0.054  newdate = 03/24/17 
 REPORTING LEVEL = 0.054  newdate = 03/10/17 
 REPORTING LEVEL = 0.054  newdate = 03/10/17 
 REPORTING LEVEL = 0.054  newdate = 03/09/17 
 REPORTING LEVEL = 0.054  newdate = 03/09/17 
 REPORTING LEVEL = 0.054  newdate = 02/24/17 
 REPORTING LEVEL = 0.054  newdate = 02/24/17 
 REPORTING LEVEL = 0.054  newdate = 01/14/17 
 REPORTING LEVEL = 0.054  newdate = 01/14/17 
 REPORTING LEVEL = 0.054  newdate = 12/05/16 
 REPORTING LEVEL = 0.054  newdate = 12/05/16 
 REPORTING LEVEL = 0.054  newdate = 11/10/16 
 REPORTING LEVEL = 0.054  newdate = 11/10/16 
 REPORTING LEVEL = 0.054  newdate = 09/23/16 
 REPORTING LEVEL = 0.054  newdate = 09/23/16 
 REPORTING LEVEL = 0.054  newdate = 09/08/16 
 REPORTING LEVEL = 0.054  newdate = 09/08/16 
 REPORTING LEVEL = 0.054  newdate = 08/11/16 
 REPORTING LEVEL = 0.054  newdate = 08/11/16 
 REPORTING LEVEL = 0.054  newdate = 07/06/16 
 REPORTING LEVEL = 0.054  newdate = 07/06/16 
 REPORTING LEVEL = 0.054  newdate = 06/03/16 
 REPORTING LEVEL = 0.054  newdate = 06/03/16 
 REPORTING LEVEL = 0.054  newdate = 02/12/16 
 REPORTING LEVEL = 0.054  newdate = 02/12/16 
 REPORTING LEVEL = 0.054  newdate = 01/22/16 
 REPORTING LEVEL = 0.054
The SGPlot Procedure

False Positive & Negative Listing for N-PENTANAL

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Positive 20171720144 Supelco LC20145V: 25 µl & Abs 060916HVOC: 25 µl & Accu 216041225: 25 µl 0.054 06/24/17 0.212 0

Updated 04/25/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
NITROBENZENE
Method: 4437 Testid: 34447GM016
Link to Individual Chart

 newdate = 06/29/17 
 falsepos = 1.24  newdate = 08/16/17 
 CENC_VAL = 1.340  newdate = 08/01/17 
 CENC_VAL = 1.390  newdate = 07/14/17 
 CENC_VAL = 1.010  newdate = 06/17/17 
 CENC_VAL = 1.810  newdate = 05/04/17 
 CENC_VAL = 1.530  newdate = 03/24/17 
 CENC_VAL = 1.610  newdate = 03/10/17 
 CENC_VAL = 2.730  newdate = 03/09/17 
 CENC_VAL = 4.300  newdate = 02/24/17 
 CENC_VAL = 1.420  newdate = 02/02/17 
 CENC_VAL = 3.240  newdate = 01/24/17 
 CENC_VAL = 3.530  newdate = 01/14/17 
 CENC_VAL = 1.270  newdate = 12/23/16 
 CENC_VAL = 2.960  newdate = 12/05/16 
 CENC_VAL = 3.660  newdate = 11/18/16 
 CENC_VAL = 1.630  newdate = 11/10/16 
 CENC_VAL = 3.360  newdate = 10/21/16 
 CENC_VAL = 3.960  newdate = 10/07/16 
 CENC_VAL = 1.730  newdate = 09/23/16 
 CENC_VAL = 3.660  newdate = 09/08/16 
 CENC_VAL = 2.610  newdate = 08/31/16 
 CENC_VAL = 2.520  newdate = 08/18/16 
 CENC_VAL = 1.650  newdate = 08/11/16 
 CENC_VAL = 2.150  newdate = 07/27/16 
 CENC_VAL = 1.480  newdate = 07/14/16 
 CENC_VAL = 2.010  newdate = 07/06/16 
 CENC_VAL = 1.280  newdate = 06/29/16 
 CENC_VAL = 4.100  newdate = 06/23/16 
 CENC_VAL = 1.200  newdate = 06/03/16 
 CENC_VAL = 1.360  newdate = 04/28/16 
 CENC_VAL = 1.200  newdate = 04/09/16 
 CENC_VAL = 0.840  newdate = 02/12/16 
 CENC_VAL = 1.010  newdate = 01/22/16 
 CENC_VAL = 2.290  newdate = 08/16/17 
 REPORTING LEVEL = 0.6  newdate = 08/01/17 
 REPORTING LEVEL = 0.6  newdate = 08/01/17 
 REPORTING LEVEL = 0.6  newdate = 07/14/17 
 REPORTING LEVEL = 0.6  newdate = 07/14/17 
 REPORTING LEVEL = 0.6  newdate = 06/29/17 
 REPORTING LEVEL = 0.6  newdate = 06/29/17 
 REPORTING LEVEL = 0.6  newdate = 06/17/17 
 REPORTING LEVEL = 0.6  newdate = 06/17/17 
 REPORTING LEVEL = 0.6  newdate = 05/04/17 
 REPORTING LEVEL = 0.6  newdate = 05/04/17 
 REPORTING LEVEL = 0.6  newdate = 03/24/17 
 REPORTING LEVEL = 0.6  newdate = 03/24/17 
 REPORTING LEVEL = 0.6  newdate = 03/10/17 
 REPORTING LEVEL = 0.6  newdate = 03/10/17 
 REPORTING LEVEL = 0.6  newdate = 03/09/17 
 REPORTING LEVEL = 0.6  newdate = 03/09/17 
 REPORTING LEVEL = 0.6  newdate = 02/24/17 
 REPORTING LEVEL = 0.6  newdate = 02/24/17 
 REPORTING LEVEL = 0.6  newdate = 02/02/17 
 REPORTING LEVEL = 0.6  newdate = 02/02/17 
 REPORTING LEVEL = 0.6  newdate = 01/24/17 
 REPORTING LEVEL = 0.6  newdate = 01/24/17 
 REPORTING LEVEL = 0.6  newdate = 01/14/17 
 REPORTING LEVEL = 0.6  newdate = 01/14/17 
 REPORTING LEVEL = 0.6  newdate = 12/23/16 
 REPORTING LEVEL = 0.6  newdate = 12/23/16 
 REPORTING LEVEL = 0.6  newdate = 12/05/16 
 REPORTING LEVEL = 0.6  newdate = 12/05/16 
 REPORTING LEVEL = 0.6  newdate = 11/18/16 
 REPORTING LEVEL = 0.6  newdate = 11/18/16 
 REPORTING LEVEL = 0.6  newdate = 11/10/16 
 REPORTING LEVEL = 0.6  newdate = 11/10/16 
 REPORTING LEVEL = 0.6  newdate = 10/21/16 
 REPORTING LEVEL = 0.6  newdate = 10/21/16 
 REPORTING LEVEL = 0.6  newdate = 10/07/16 
 REPORTING LEVEL = 0.6  newdate = 10/07/16 
 REPORTING LEVEL = 0.6  newdate = 09/23/16 
 REPORTING LEVEL = 0.6  newdate = 09/23/16 
 REPORTING LEVEL = 0.6  newdate = 09/08/16 
 REPORTING LEVEL = 0.6  newdate = 09/08/16 
 REPORTING LEVEL = 0.6  newdate = 08/31/16 
 REPORTING LEVEL = 0.6  newdate = 08/31/16 
 REPORTING LEVEL = 0.6  newdate = 08/18/16 
 REPORTING LEVEL = 0.6  newdate = 08/18/16 
 REPORTING LEVEL = 0.6  newdate = 08/11/16 
 REPORTING LEVEL = 0.6  newdate = 08/11/16 
 REPORTING LEVEL = 0.6  newdate = 07/27/16 
 REPORTING LEVEL = 0.6  newdate = 07/27/16 
 REPORTING LEVEL = 0.6  newdate = 07/14/16 
 REPORTING LEVEL = 0.6  newdate = 07/14/16 
 REPORTING LEVEL = 0.6  newdate = 07/06/16 
 REPORTING LEVEL = 0.6  newdate = 07/06/16 
 REPORTING LEVEL = 0.6  newdate = 06/29/16 
 REPORTING LEVEL = 0.6  newdate = 06/29/16 
 REPORTING LEVEL = 0.6  newdate = 06/23/16 
 REPORTING LEVEL = 0.6  newdate = 06/23/16 
 REPORTING LEVEL = 0.6  newdate = 06/03/16 
 REPORTING LEVEL = 0.6  newdate = 06/03/16 
 REPORTING LEVEL = 0.6  newdate = 04/28/16 
 REPORTING LEVEL = 0.6  newdate = 04/28/16 
 REPORTING LEVEL = 0.6  newdate = 04/09/16 
 REPORTING LEVEL = 0.6  newdate = 04/09/16 
 REPORTING LEVEL = 0.6  newdate = 02/12/16 
 REPORTING LEVEL = 0.6  newdate = 02/12/16 
 REPORTING LEVEL = 0.6  newdate = 01/22/16 
 REPORTING LEVEL = 0.6
The SGPlot Procedure

False Positive & Negative Listing for NITROBENZENE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Positive 20171720144 Supelco LC20145V: 25 µl & Abs 060916HVOC: 25 µl & Accu 216041225: 25 µl 0.6 06/29/17 E 1.24 0

Updated 04/25/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
TERT-BUTYL_ALCOHOL
Method: 4437 Testid: 77035GM016
Link to Individual Chart

 newdate = 12/23/16 
 falsepos = 0.134  newdate = 08/16/17 
 CENC_VAL = 0.731  newdate = 06/24/17 
 CENC_VAL = 0.992  newdate = 06/13/17 
 CENC_VAL = 1.010  newdate = 04/27/17 
 CENC_VAL = 0.637  newdate = 03/24/17 
 CENC_VAL = 0.568  newdate = 03/09/17 
 CENC_VAL = 1.530  newdate = 02/24/17 
 CENC_VAL = 0.810  newdate = 02/02/17 
 CENC_VAL = 1.640  newdate = 02/02/17 
 CENC_VAL = 0.537  newdate = 01/03/17 
 CENC_VAL = 0.738  newdate = 12/05/16 
 CENC_VAL = 1.580  newdate = 11/29/16 
 CENC_VAL = 1.650  newdate = 11/18/16 
 CENC_VAL = 0.572  newdate = 11/02/16 
 CENC_VAL = 0.573  newdate = 10/07/16 
 CENC_VAL = 0.547  newdate = 09/28/16 
 CENC_VAL = 0.991  newdate = 09/08/16 
 CENC_VAL = 0.978  newdate = 09/08/16 
 CENC_VAL = 0.990  newdate = 08/18/16 
 CENC_VAL = 0.626  newdate = 08/12/16 
 CENC_VAL = 0.613  newdate = 04/09/16 
 CENC_VAL = 0.362  newdate = 03/22/16 
 CENC_VAL = 0.354  newdate = 01/22/16 
 CENC_VAL = 0.847  newdate = 08/16/17 
 REPORTING LEVEL = 0.24  newdate = 06/24/17 
 REPORTING LEVEL = 0.24  newdate = 06/24/17 
 REPORTING LEVEL = 0.24  newdate = 06/13/17 
 REPORTING LEVEL = 0.24  newdate = 06/13/17 
 REPORTING LEVEL = 0.24  newdate = 04/27/17 
 REPORTING LEVEL = 0.24  newdate = 04/27/17 
 REPORTING LEVEL = 0.24  newdate = 03/24/17 
 REPORTING LEVEL = 0.24  newdate = 03/24/17 
 REPORTING LEVEL = 0.24  newdate = 03/09/17 
 REPORTING LEVEL = 0.24  newdate = 03/09/17 
 REPORTING LEVEL = 0.24  newdate = 02/24/17 
 REPORTING LEVEL = 0.24  newdate = 02/24/17 
 REPORTING LEVEL = 0.24  newdate = 02/02/17 
 REPORTING LEVEL = 0.24  newdate = 02/02/17 
 REPORTING LEVEL = 0.24  newdate = 02/02/17 
 REPORTING LEVEL = 0.24  newdate = 02/02/17 
 REPORTING LEVEL = 0.24  newdate = 01/03/17 
 REPORTING LEVEL = 0.24  newdate = 01/03/17 
 REPORTING LEVEL = 0.24  newdate = 12/23/16 
 REPORTING LEVEL = 0.24  newdate = 12/23/16 
 REPORTING LEVEL = 0.24  newdate = 12/05/16 
 REPORTING LEVEL = 0.24  newdate = 12/05/16 
 REPORTING LEVEL = 0.24  newdate = 11/29/16 
 REPORTING LEVEL = 0.24  newdate = 11/29/16 
 REPORTING LEVEL = 0.24  newdate = 11/18/16 
 REPORTING LEVEL = 0.24  newdate = 11/18/16 
 REPORTING LEVEL = 0.24  newdate = 11/02/16 
 REPORTING LEVEL = 0.24  newdate = 11/02/16 
 REPORTING LEVEL = 0.24  newdate = 10/07/16 
 REPORTING LEVEL = 0.24  newdate = 10/07/16 
 REPORTING LEVEL = 0.24  newdate = 09/28/16 
 REPORTING LEVEL = 0.24  newdate = 09/28/16 
 REPORTING LEVEL = 0.24  newdate = 09/08/16 
 REPORTING LEVEL = 0.24  newdate = 09/08/16 
 REPORTING LEVEL = 0.24  newdate = 09/08/16 
 REPORTING LEVEL = 0.24  newdate = 09/08/16 
 REPORTING LEVEL = 0.24  newdate = 08/18/16 
 REPORTING LEVEL = 0.24  newdate = 08/18/16 
 REPORTING LEVEL = 0.24  newdate = 08/12/16 
 REPORTING LEVEL = 0.24  newdate = 08/12/16 
 REPORTING LEVEL = 0.24  newdate = 04/09/16 
 REPORTING LEVEL = 0.24  newdate = 04/09/16 
 REPORTING LEVEL = 0.24  newdate = 03/22/16 
 REPORTING LEVEL = 0.24  newdate = 03/22/16 
 REPORTING LEVEL = 0.24  newdate = 01/22/16 
 REPORTING LEVEL = 0.24  Y = 0
The SGPlot Procedure

False Positive & Negative Listing for TERT-BUTYL_ALCOHOL

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Positive 20163500005 ChemService 5082800: 25 µl & Accu 216041354: 25 µl & NSI 041416HVOC: 25 µl 0.24 12/23/16 0.134 0

Updated 04/25/2018

back to table
Organic Blind Sample Program
False Positives & False Negatives
TERT-BUTYL_METHYL_ETHER_(MTBE)
Method: 4437 Testid: 78032GM016
Link to Individual Chart

 newdate = 08/30/17 
 CENC_VAL = 0.027  newdate = 08/16/17 
 CENC_VAL = 0.040  newdate = 08/10/17 
 CENC_VAL = 0.027  newdate = 08/01/17 
 CENC_VAL = 0.057  newdate = 07/14/17 
 CENC_VAL = 0.029  newdate = 02/02/17 
 CENC_VAL = 0.036  newdate = 12/23/16 
 CENC_VAL = 0.053  newdate = 11/29/16 
 CENC_VAL = 0.079  newdate = 09/28/16 
 CENC_VAL = 0.057  newdate = 08/31/16 
 CENC_VAL = 0.054  newdate = 08/12/16 
 CENC_VAL = 0.029  newdate = 07/06/16 
 CENC_VAL = 0.089  newdate = 06/23/16 
 CENC_VAL = 0.036  newdate = 05/20/16 
 CENC_VAL = 0.037  newdate = 04/28/16 
 CENC_VAL = 0.030  newdate = 03/22/16 
 CENC_VAL = 0.022  newdate = 02/12/16 
 CENC_VAL = 0.017  newdate = 08/30/17 
 REPORTING LEVEL = 0.012  newdate = 08/16/17 
 REPORTING LEVEL = 0.012  newdate = 08/16/17 
 REPORTING LEVEL = 0.012  newdate = 08/10/17 
 REPORTING LEVEL = 0.012  newdate = 08/10/17 
 REPORTING LEVEL = 0.012  newdate = 08/01/17 
 REPORTING LEVEL = 0.012  newdate = 08/01/17 
 REPORTING LEVEL = 0.012  newdate = 07/14/17 
 REPORTING LEVEL = 0.012  newdate = 07/14/17 
 REPORTING LEVEL = 0.012  newdate = 02/02/17 
 REPORTING LEVEL = 0.012  newdate = 02/02/17 
 REPORTING LEVEL = 0.012  newdate = 12/23/16 
 REPORTING LEVEL = 0.012  newdate = 12/23/16 
 REPORTING LEVEL = 0.012  newdate = 11/29/16 
 REPORTING LEVEL = 0.012  newdate = 11/29/16 
 REPORTING LEVEL = 0.012  newdate = 09/28/16 
 REPORTING LEVEL = 0.012  newdate = 09/28/16 
 REPORTING LEVEL = 0.012  newdate = 08/31/16 
 REPORTING LEVEL = 0.012  newdate = 08/31/16 
 REPORTING LEVEL = 0.012  newdate = 08/12/16 
 REPORTING LEVEL = 0.012  newdate = 08/12/16 
 REPORTING LEVEL = 0.012  newdate = 07/06/16 
 REPORTING LEVEL = 0.012  newdate = 07/06/16 
 REPORTING LEVEL = 0.012  newdate = 06/23/16 
 REPORTING LEVEL = 0.012  newdate = 06/23/16 
 REPORTING LEVEL = 0.012  newdate = 05/20/16 
 REPORTING LEVEL = 0.012  newdate = 05/20/16 
 REPORTING LEVEL = 0.012  newdate = 04/28/16 
 REPORTING LEVEL = 0.012  newdate = 04/28/16 
 REPORTING LEVEL = 0.012  newdate = 03/22/16 
 REPORTING LEVEL = 0.012  newdate = 03/22/16 
 REPORTING LEVEL = 0.012  newdate = 02/12/16 
 REPORTING LEVEL = 0.012
The SGPlot Procedure

back to table
Organic Blind Sample Program
False Positives & False Negatives
TRANS-CROTONALDEHYDE
Method: 4437 Testid: 68733GM016
Link to Individual Chart

 newdate = 08/30/17 
 CENC_VAL = 0.740  newdate = 08/16/17 
 CENC_VAL = 2.140  newdate = 08/10/17 
 CENC_VAL = 1.520  newdate = 08/01/17 
 CENC_VAL = 2.240  newdate = 06/29/17 
 CENC_VAL = 2.810  newdate = 06/13/17 
 CENC_VAL = 2.680  newdate = 04/27/17 
 CENC_VAL = 1.320  newdate = 03/24/17 
 CENC_VAL = 1.520  newdate = 03/09/17 
 CENC_VAL = 3.760  newdate = 02/24/17 
 CENC_VAL = 2.430  newdate = 02/02/17 
 CENC_VAL = 3.860  newdate = 02/02/17 
 CENC_VAL = 1.410  newdate = 01/03/17 
 CENC_VAL = 1.460  newdate = 12/05/16 
 CENC_VAL = 3.840  newdate = 11/29/16 
 CENC_VAL = 4.090  newdate = 11/18/16 
 CENC_VAL = 1.410  newdate = 11/02/16 
 CENC_VAL = 1.350  newdate = 10/07/16 
 CENC_VAL = 1.310  newdate = 09/28/16 
 CENC_VAL = 2.100  newdate = 09/08/16 
 CENC_VAL = 1.950  newdate = 09/08/16 
 CENC_VAL = 2.050  newdate = 08/18/16 
 CENC_VAL = 1.220  newdate = 08/12/16 
 CENC_VAL = 1.220  newdate = 04/28/16 
 CENC_VAL = 0.890  newdate = 03/22/16 
 CENC_VAL = 0.684  newdate = 02/12/16 
 CENC_VAL = 0.554  newdate = 08/30/17 
 REPORTING LEVEL = 0.48  newdate = 08/16/17 
 REPORTING LEVEL = 0.48  newdate = 08/16/17 
 REPORTING LEVEL = 0.48  newdate = 08/10/17 
 REPORTING LEVEL = 0.48  newdate = 08/10/17 
 REPORTING LEVEL = 0.48  newdate = 08/01/17 
 REPORTING LEVEL = 0.48  newdate = 08/01/17 
 REPORTING LEVEL = 0.48  newdate = 06/29/17 
 REPORTING LEVEL = 0.48  newdate = 06/29/17 
 REPORTING LEVEL = 0.48  newdate = 06/13/17 
 REPORTING LEVEL = 0.48  newdate = 06/13/17 
 REPORTING LEVEL = 0.48  newdate = 04/27/17 
 REPORTING LEVEL = 0.48  newdate = 04/27/17 
 REPORTING LEVEL = 0.48  newdate = 03/24/17 
 REPORTING LEVEL = 0.48  newdate = 03/24/17 
 REPORTING LEVEL = 0.48  newdate = 03/09/17 
 REPORTING LEVEL = 0.48  newdate = 03/09/17 
 REPORTING LEVEL = 0.48  newdate = 02/24/17 
 REPORTING LEVEL = 0.48  newdate = 02/24/17 
 REPORTING LEVEL = 0.48  newdate = 02/02/17 
 REPORTING LEVEL = 0.48  newdate = 02/02/17 
 REPORTING LEVEL = 0.48  newdate = 02/02/17 
 REPORTING LEVEL = 0.48  newdate = 02/02/17 
 REPORTING LEVEL = 0.48  newdate = 01/03/17 
 REPORTING LEVEL = 0.48  newdate = 01/03/17 
 REPORTING LEVEL = 0.48  newdate = 12/05/16 
 REPORTING LEVEL = 0.48  newdate = 12/05/16 
 REPORTING LEVEL = 0.48  newdate = 11/29/16 
 REPORTING LEVEL = 0.48  newdate = 11/29/16 
 REPORTING LEVEL = 0.48  newdate = 11/18/16 
 REPORTING LEVEL = 0.48  newdate = 11/18/16 
 REPORTING LEVEL = 0.48  newdate = 11/02/16 
 REPORTING LEVEL = 0.48  newdate = 11/02/16 
 REPORTING LEVEL = 0.48  newdate = 10/07/16 
 REPORTING LEVEL = 0.48  newdate = 10/07/16 
 REPORTING LEVEL = 0.48  newdate = 09/28/16 
 REPORTING LEVEL = 0.48  newdate = 09/28/16 
 REPORTING LEVEL = 0.48  newdate = 09/08/16 
 REPORTING LEVEL = 0.48  newdate = 09/08/16 
 REPORTING LEVEL = 0.48  newdate = 09/08/16 
 REPORTING LEVEL = 0.48  newdate = 09/08/16 
 REPORTING LEVEL = 0.48  newdate = 08/18/16 
 REPORTING LEVEL = 0.48  newdate = 08/18/16 
 REPORTING LEVEL = 0.48  newdate = 08/12/16 
 REPORTING LEVEL = 0.48  newdate = 08/12/16 
 REPORTING LEVEL = 0.48  newdate = 04/28/16 
 REPORTING LEVEL = 0.48  newdate = 04/28/16 
 REPORTING LEVEL = 0.48  newdate = 03/22/16 
 REPORTING LEVEL = 0.48  newdate = 03/22/16 
 REPORTING LEVEL = 0.48  newdate = 02/12/16 
 REPORTING LEVEL = 0.48
The SGPlot Procedure